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Synthesis of quaternary α-perfluoroalkyl lactams via electrophilic perfluoroalkylation.
Katayev, D; Václavík, J; Brüning, F; Commare, B; Togni, A.
Chem Commun (Camb) ; 52(21): 4049-52, 2016 Mar 14.
Article in English | MEDLINE | ID: mdl-26893124

ABSTRACT

Efficient protocols enabling the rapid installation of trifluoromethyl, as well as further functionalized fluoroalkyl groups by an electrophilic perfluoroalkylation of lactam-derived ketene silyl amides (KSAs) using hypervalent iodine reagents 1 and 2 have been developed.


Subject(s)
Hydrocarbons, Fluorinated/chemistry , Hydrocarbons, Fluorinated/chemical synthesis , Iodine/chemistry , Lactams/chemical synthesis , Catalysis , Ethylenes/chemistry , Indicators and Reagents/chemistry , Ketones/chemistry , Lactams/chemistry , Molecular Structure
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