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Nat Prod Res ; 30(2): 237-40, 2016.
Article in English | MEDLINE | ID: mdl-26118891

ABSTRACT

A head space solid-phase microextraction method combined with gas chromatography-mass spectrometry was developed and optimised to extract and analyse volatile compounds of Melipona beecheii geopropolis. Seventy-three constituents were identified using this technique in the sample of geopropolis collected. The main compounds detected include ß-fenchene (14.53-15.45%), styrene (8.72-9.98%), benzaldehyde (7.44-7.82%) and the most relevant volatile components presents at high level in the geopropolis were terpenoids (58.17%).


Subject(s)
Gas Chromatography-Mass Spectrometry/methods , Propolis/analysis , Solid Phase Microextraction/methods , Volatile Organic Compounds/analysis , Animals , Bees , Benzaldehydes/analysis , Benzaldehydes/chemistry , Bridged Bicyclo Compounds/chemistry , Bridged Bicyclo Compounds/isolation & purification , Camphanes , Mexico , Propolis/chemistry , Styrene/analysis , Styrene/chemistry , Terpenes/analysis , Volatile Organic Compounds/chemistry
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