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1.
Materials (Basel) ; 15(24)2022 Dec 13.
Article in English | MEDLINE | ID: mdl-36556719

ABSTRACT

The freeform capability additive manufacturing (AM) technique and the magnetic efficiency of Fe-6.5Si steel have the potential for the development of electromechanical component designs with thin body sections. Moreover, the directional anisotropy of the material, which is formed during growth, improves the magnetic and electrical properties of Fe-6.5 wt%Si. We obtained the range of optimal technological modes of Laser Power Bed Fusion process (volume energy density (VED) of 100−140 J/mm3, scanning speed of 750−500 mm/s) to produce the samples from Fe-6.5 wt%Si powder, but even at the best of them cracks may appear. The optical microscopy and SEM with EDX analysis of the laser-fabricated structures are applied for investigation of this phenomena. We detected a carbon content at the boundaries of the cracks. This suggests that one of the reasons for the crack formation is the presence of Fe3C in the area of the ordered α'FeSi (B2)+Fe3Si(D03) phases. Quantitative analysis based on crack initiation criteria (CIC) showed that the safe level of internal stresses in terms of the CIC criteria in the area of discontinuities is exceeded by almost 190%. Local precipitates of carbides in the area of cracks are explained by the heterogeneity and high dynamics of temperature fields, as well as the transfer of substances due to Marangoni convection, which, as a result, contributes to a significant segregation of elements and the formation of precipitate phases.

2.
Materials (Basel) ; 15(20)2022 Oct 11.
Article in English | MEDLINE | ID: mdl-36295128

ABSTRACT

This paper addresses the study of the complex effect of alloying elements (magnesium, manganese, copper and zirconium) on changes in magnesium-rich aluminum alloy composition, fine and coarse particle size and number, recrystallization characteristics and mechanical properties. The data obtained made it possible to analyze change in the chemical composition, sizes of intermetallic compounds and dispersoids depending on alloying elements content. The effect of the chemical composition on the driving force and the number of recrystallization nuclei was studied. It was established that the addition of alloying elements leads to grain refinement, including through the activation of a particle-stimulated nucleation mechanism. As a result, with Mg increase from 4 to 5%, addition of 0.5% Mn and 0.5% Cu, the grain size decreased from 72 to 15 µm. Grain refinement occurred due to an increase in the number of particle-stimulated nuclei, the number of which at minimal alloying rose from 3.47 × 1011 to 81.2 × 1011 with the maximum concentration of Mg, Mn, Cu additives. The retarding force of recrystallization, which in the original alloy was 1.57 × 10-3 N/m2, increased to 5.49 × 10-3 N/m2 at maximum alloying. The influence of copper was especially noticeable, the introduction of 0.5% increasing the retarding force of recrystallization by 2.39 × 10-3 N/m2. This is due to the fact that copper has the most significant effect on the size and number of intermetallic particles. It was established that strength increase without ductility change occurs when magnesium, manganese and copper content increases.

3.
Materials (Basel) ; 15(3)2022 Jan 21.
Article in English | MEDLINE | ID: mdl-35160767

ABSTRACT

Functional Graded Structures and Functional Graded parts, made using dissimilar materials, are designed to provide specific properties to the final product. One of the most promising methods for manufacturing 3D Functional Graded objects is 3D laser cladding and/or direct energy deposition. However, the construction of graded and especially layered graded structures in the process of joining materials with different thermophysical properties under certain conditions is accompanied by the formation of cracks along the phase boundaries, which are a consequence of residual stresses and/or chemical segregations. The conditions for phase consolidation are macroscopic balancing of residual stresses in the region of the interface. In a broader sense, in the field of the interface, it is necessary to consider the thermodynamic equilibrium of the phases in connection with mechanical equilibrium. In this regard, the article proposed criteria for the thermodynamic affinity of phases in the area of the Functional Graded Structures interface, including the coefficients of thermal expansion and isobaric and isochoric heat capacities of the phases. Examples of cracking and the use of the obtained criteria are provided.

4.
Springerplus ; 5: 378, 2016.
Article in English | MEDLINE | ID: mdl-27066385

ABSTRACT

An efficient method for calculating the evolution of internal variables in an expanding hollow cylinder of rigid/plastic material is proposed. The conventional constitutive equations for rigid plastic, hardening material are supplemented with quite an arbitrary set of evolution laws for internal variables assuming that the material is incompressible. No restriction is imposed on the hardening law. The problem is solved in Lagrangian coordinates. This significantly facilitates a numerical treatment of the problem. In particular, the initial/boundary value problem is reduced to a system of equations in characteristic coordinates. A finite difference scheme is used for solving these equations. An illustrative example is presented assuming that the internal variables are the equivalent plastic strain and a damage parameter.

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