A nanonewton force sensor using a U-shape tapered microfiber interferometer.

Nanomechanical measurements, especially the detection of weak contact forces, play a vital role in many fields, such as material science, micromanipulation, and mechanobiology. However, it remains a challenging task to realize the measurement of ultraweak force levels as low as nanonewtons with a simple sensing configuration. In this work, an ultrasensitive all-fiber nanonewton force sensor structure based on a single-mode-tapered U-shape multimode-single-mode fiber probe is proposed and experimentally demonstrated with a limit of detection of ~5.4 nanonewtons. The use of the sensor is demonstrated by force measurement on a human hair sample to determine the spring constant of the hair. The results agree well with measurements using an atomic force microscope for the spring constant of the hair. Compared with other force sensors based on optical fiber in the literature, the proposed all-fiber force sensor provides a substantial advancement in the minimum detectable force possible, with the advantages of a simple configuration, ease of fabrication, and low cost.

Sensitivity-enhanced strain sensor based on a shape-modulated multimode fiber.

In this Letter, we demonstrate a sensitivity-enhanced strain sensor based on a shape-modulated multimode fiber (MMF). In contrast to conventional single-mode-multimode-single-mode (SMS) fiber structures, which typically contain a single cylindrical homogeneous MMF section, the shape of the MMF section in this investigation is modulated by lateral offset splicing of multiple MMF segments. Simulation results show that the designed shape-modulated MMF has a higher peak mechanical strain than that of a cylindrical MMF. Experimental results demonstrate that the strain sensitivity achieved by the shaped-modulated MMF-formed SMS fiber structure is as high as -55.63 pm/µÎµ, which is 33 times higher than that for a cylindrical MMF-formed conventional SMS fiber structure at -1.65 pm/µÎµ. This high sensitivity and low-fabrication cost SMS fiber sensor has the potential to be a promising candidate in precise strain measurement applications.

Laser operation at 1.2†µm in Ho3+-doped ZBYA glass fibers.

Powerful 1.2-µm laser operation was produced in Ho3+-doped single-cladding, in-house fabricated ZrF4-BaF2-YF3-AlF3 (ZBYA) glass fibers. The fibers were fabricated based on ZBYA glass with a composition of ZrF4-BaF2-YF3-AlF3. Pumped by an 1150-nm Raman fiber laser, the maximum combined laser output power emitted from both sides of a 0.5-mol% Ho3+-doped ZBYA fiber was 6.7 W, with a slope efficiency of 40.5%. We also observed lasing at 2.9 µm with an output power of 350 mW, which was ascribed to the transition of Ho3+:5I6 → 5I7. The effect of rare earth (RE) doping concentration and the length of the gain fiber were also investigated to determine their effect on laser performance at 1.2 µm and 2.9 µm.

Efficient 2075-nm laser emission from Ho3+-doped fluorotellurite glass in a compact all-fiber structure.

In this Letter, we report an Ho3+-doped fluorotellurite glass all-fiber laser at 2075 nm. The gain fiber is pumped in-band with a 1976-nm fiber laser and connected by fusion splicing. A high-quality fusion splicing point with a loss of < 0.1 dB was obtained by finely adjusting the splicing power and offset. In addition, by optimizing the writing parameters, a third-order fiber Bragg grating (FBG) with a reflectivity of 98% was achieved at 2075 nm using the femtosecond laser direct-writing method. Using the FBG as the laser cavity mirror and a relatively short 28-cm-long home-made Ho3+-doped fluorotellurite fiber as the laser medium, a laser with a maximum unsaturated output power of 7.33 W was obtained, and the corresponding slope efficiency was as high as 93.4%. The first, to the best of our knowledge, demonstration of the fluorotellurite glass all-fiber ∼2.1-µm laser presented in this work may pave the way for a high-power 2.1-µm fiber laser with a compact structure.

A label-free fiber ring laser biosensor for ultrahigh sensitivity detection of Salmonella Typhimurium.

The rapid detection of low concentrations of Salmonella Typhimurium (S. Typhimurium) is an essential preventive measure for food safety and prevention of foodborne illness. The study presented in this paper addresses this critical issue by proposing a single mode-tapered seven core-single mode (STSS) fiber ring laser (FRL) biosensor for S. Typhimurium detection. The experimental results show that the specific detection time of S. Typhimurium is less than 20 min and the wavelength shift can achieve -0.906 nm for an S. Typhimurium solution (10 cells/mL). Furthermore, at a lower concentration of 1 cell/mL applied to the biosensor, a result of -0.183 nm is observed in 9% of samples (1/11), which indicates that the proposed FRL biosensor has the ability to detect 1 cell/mL of S. Typhimurium. In addition, the detection results in chicken and pickled pork samples present an average deviation of -27% and -23%, respectively, from the measured results in phosphate buffered saline. Taken together, these results show the proposed FRL biosensor may have potential applications in the fields of food safety monitoring, medical diagnostics, etc.

High-sensitivity vector bend sensor based on a fiber directional coupler inscribed by a femtosecond laser.

In this Letter, we demonstrate a high-sensitivity vector bend sensor based on a fiber directional coupler. The fiber directional coupler is composed of two parallel waveguides inscribed within a no-core fiber (NCF) by a femtosecond laser. Since the two written waveguides have closely matched refractive indices and geometries, the transmission spectrum of the fiber directional coupler possesses periodic resonant dips. Such a fiber directional coupler exhibits a good bending-dependent spectral shift response due to its asymmetric structure. Experimental results show that bending sensitivities of -97.11 nm/m-1 and 58.22 nm/m-1 are achieved for the 0° and 180° orientations in the curvature range of 0-0.62 m-1, respectively. In addition, the proposed fiber directional coupler is shown to be insensitive to external humidity changes, thus improving its suitability in high-accuracy bending measurements.

Light transmission mechanisms in a SMF-capillary fiber-SMF structure and its application to bi-directional liquid level measurement.

Capillary fiber (CF) has been extensively investigated in a singlemode fiber (SMF)-CF-SMF (SCS) sensing structure since multiple light guiding mechanisms can be easily excited by simply tuning the air core diameter (cladding diameter) and length of the CF. Understanding the light guiding principles in an SCS structure is essential for improved implementation of a CF based fiber sensor. In this work, light guiding principles in a relatively large air core diameter (≥ 20 µm) and long length of CF (> 1 mm) are investigated theoretically and experimentally. It is found that both multimode interference (MMI) and Anti-Resonant Reflecting Optical Waveguide (ARROW) light guiding mechanisms are excited in the SCS structure in the transmission configuration. However, MMI dips are not observed in the spectrum for the air core diameters of CF smaller than 50 µm in the experiment due to large transmission loss in small air core CFs. Further experimental results demonstrate that a CF with a bigger air core diameter shows a higher sensitivity to curvature, and the highest sensitivity of -16.15 nm/m-1 is achieved when an CF-100 was used. In addition, a SMF-CF-20-CF-30-SMF (SCCS) structure is proposed for high sensitivity bi-direction liquid level measurement for the first time, to the best of our knowledge. Two types of ARROW dips (Dip-20 and Dip-30) are simultaneously excited in transmission, hence both liquid level and liquid flow direction can be detected by tracing the dip strength changes of Dip-20 and Dip-30, respectively.

Construction of multiple anti-resonant light guidance mechanisms in a hollow-core fiber structure for simultaneous measurement of multiple parameters.

The construction of multiple light guidance mechanisms in a hollow-core fiber (HCF) structure is a popular way to realize the simultaneous measurement of multiple parameters. In this work, a partial coating method to excite multiple anti-resonant light guidance mechanisms (ARLGMs) in an HCF structure for the simultaneous measurement of multiple parameters is proposed. As an example, a double ARLGM based on a partially polyimide (PI)-coated HCF structure for the simultaneous measurement of relative humidity (RH) and temperature is demonstrated theoretically and experimentally. The dip (dip II) produced by the PI-coated HCF section shifts linearly with surrounding RH changes with a sensitivity of circa 58.6 ± 0.77 pm/%RH, while the dip (dip I) produced by the bare HCF section (with an air coating layer) is insensitive to RH changes. In addition, both types of dips have linear responses to temperature variations, with similar sensitivities of ∼ 17 pm/°C. Hence, the proposed sensor structure can be used as an RH sensor that is also capable of compensating for local temperature fluctuations. More importantly, the simultaneous measurement of multiple parameters (such as biomarkers) is possible using the proposed method provided the proper sensing materials are partially coated onto the HCF surface.

Two-watt mid-infrared laser emission in robust fluorozirconate fibers.

To the best of our knowledge, we report here the first demonstration of 2.9 µm laser emission from in-house fabricated Ho3+/Pr3+ co-doped ZBYA glass fiber. The fiber was fabricated based on the ZBYA glass with compositions of ZrF4-BaF2-YF3-AlF3-PbF2-HoF3-PrF3. Under the pump of a 1150 nm Raman fiber laser, the maximum unsaturated output power of 2.16 W was obtained in a 15 cm long gain fiber with a slope efficiency of 24%. The influence of rare-earth doping concentration on laser performance was also investigated. The result indicates that ZBYA glass fibers have potential for using as a fluorozirconate glass gain fiber for mid-infrared fiber lasers.

Ultra-compact in-core-parallel-written FBG and Mach-Zehnder interferometer for simultaneous measurement of strain and temperature.

An ultra-compact in-core-parallel-written fiber Bragg grating (FBG) and Mach-Zehnder interferometer (MZI) for simultaneous measurement of strain and temperature is described. The FBG and MZI are written spatially parallel in the same section of fiber core using a femtosecond laser, forming an ultra-compact device, which is different from the previously developed axial cascade of different structures. Due to the weak coupling between the FBG and the MZI, their individual extinction ratios are traded off by optimizing their writing position and separation, and extinction ratios of 5.9 dB for the FBG and 10 dB for the MZI are achieved. Experimental results show that the FBG and MZI have different sensitivities for strain and temperature, allowing this device to measure strain and temperature simultaneously. In addition, since both the FBG and MZI are written in the fiber core, this ultra-compact device is proven to be impervious to ambient humidity, making it a promising candidate for accurate industrial strain and temperature measurements.

Praseodymium mid-infrared emission in AlF3-based glass sensitized by ytterbium.

Broadband emission was obtained over 2.6 to 4.1 µm (Pr3+: 1G4→3F4, 3F3) in AlF3-based glass samples doped with different concentrations of praseodymium and 1 mol% ytterbium using a 976 nm laser pump. An efficient energy transfer process from Yb3+: 2F5/2 to Pr3+: 1G4 was analyzed through emission spectra and fluorescence lifetime values. The absorption and emission cross-sections were calculated by Füchtbauer-Ladenburg and McCumber theories and a positive gain can be obtained when P>0.3. To the best of the authors' knowledge, this work represents the first report of broadband mid-infrared emission of Pr3+ in an AlF3-based glass. The results show that praseodymium doped AlF3-based glass sensitized by ytterbium could be a promising candidate for fiber lasers operating in mid-infrared region.

Strain-, curvature- and twist-independent temperature sensor based on a small air core hollow core fiber structure.

Cross-sensitivity (crosstalk) to multiple parameters is a serious but common issue for most sensors and can significantly decrease the usefulness and detection accuracy of sensors. In this work, a high sensitivity temperature sensor based on a small air core (10 µm) hollow core fiber (SACHCF) structure is proposed. Co-excitation of both anti-resonant reflecting optical waveguide (ARROW) and Mach-Zehnder interferometer (MZI) guiding mechanisms in transmission are demonstrated. It is found that the strain sensitivity of the proposed SACHCF structure is decreased over one order of magnitude when a double phase condition (destructive condition of MZI and resonant condition of ARROW) is satisfied. In addition, due to its compact size and a symmetrical configuration, the SACHCF structure shows ultra-low sensitivity to curvature and twist. Experimentally, a high temperature sensitivity of 31.6 pm/°C, an ultra-low strain sensitivity of -0.01pm/µÎµ, a curvature sensitivity of 18.25 pm/m-1, and a twist sensitivity of -22.55 pm/(rad/m) were demonstrated. The corresponding temperature cross sensitivities to strain, curvature and twist are calculated to be -0.00032 °C/µÎµ, 0.58 °C/m-1 and 0.71 °C/(rad/m), respectively. The above cross sensitivities are one to two orders of magnitude lower than that of previously reported optical fiber temperature sensors. The proposed sensor shows a great potential to be used as a temperature sensor in practical applications where influence of multiple environmental parameters cannot be eliminated.

High-sensitivity temperature sensor based on anti-resonance in high-index polymer-coated optical fiber interferometers.

Compared to the multimode interference (MMI) effect, the anti-resonance (AR) effect does not rely on the multimode property of the optical waveguide. This Letter shows that fiber bending can suppress the MMI and can break the superposition of AR spectra of multiple modes in a high-index polymer-coated optical fiber interferometer based on a single-mode fiber-polymer-coated no-core fiber-single-mode fiber hetero-structure. This results in the dominance of the AR spectrum of an individual mode and consequently in periodic sharp transmission dips. As a result of this phenomenon and large thermo-optical and thermal expansion coefficients of the polymer, a compact, high-sensitivity and linear response temperature sensor with the sensitivity as high as -3.784nm/∘C has been demonstrated experimentally.

Negative Curvature Hollow Core Fiber Based All-Fiber Interferometer and Its Sensing Applications to Temperature and Strain.

Negative curvature hollow core fiber (NCHCF) is a promising candidate for sensing applications; however, research on NCHCF based fiber sensors starts only in the recent two years. In this work, an all-fiber interferometer based on an NCHCF structure is proposed for the first time. The interferometer was fabricated by simple fusion splicing of a short section of an NCHCF between two singlemode fibers (SMFs). Both simulation and experimental results show that multiple modes and modal interferences are excited within the NCHCF structure. Periodic transmission dips with high spectral extinction ratio (up to 30 dB) and wide free spectral range (FSR) are produced, which is mainly introduced by the modes coupling between HE11 and HE12. A small portion of light guiding by means of Anti-resonant reflecting optical waveguide (ARROW) mechanism is also observed. The transmission dips, resulting from multimode interferences (MMI) and ARROW effect have a big difference in sensitivities to strain and temperature, thus making it possible to monitor these two parameters with a single sensor head by using a characteristic matrix approach. In addition, the proposed sensor structure is experimentally proven to have a good reproducibility.

Intense mid-infrared emission at 3.9 µm in Ho3+-doped ZBYA glasses for potential use as a fiber laser.

Intense mid-infrared emission at 3.9 µm in Ho3+-doped ZBYA glasses with direct upper laser level (Ho3+:5I5) pumping at a wavelength of 888 nm is reported for the first time, to the best of our knowledge. Spectroscopic parameters were determined using the Judd-Ofelt theory and the measured absorption spectrum. The maximum emission cross section of the Ho3+-doped ZBYA glass is estimated to be 2.7×10-21cm2 at 3906 nm. Additionally, fluorescence spectra and lifetimes of ZBYA glasses with different Ho3+ ion doping concentrations were measured. The results provide theoretical and experimental basis for better selection of rare-earth-doped matrix glasses to achieve a fluorescence output centered on a wavelength of 3.9 µm.

Anti-resonance, inhibited coupling and mode transition in depressed core fibers.

The depressed core fiber (DCF), consisting of a low-index solid core, a high-index cladding and air surrounding, is in effect a bridge between the conventional step-index fiber and the tube-type hollow-core fiber from the point of view of the index profile. In this paper the dispersion diagram of a DCF is obtained by solving the full-vector eigenvalue equations and analyzed using the theory of anti-resonant and the inhibited coupling mechanisms. While light propagation in tube-type hollow-core fibers is commonly described by the symmetric planar waveguide model, here we propose an asymmetric planar waveguide for the DCFs in an anti-resonant reflecting optical waveguide (ARROW) model. It is found that the anti-resonant core modes in the DCFs have real effective indices, compared to the anti-resonant core modes with complex effective indices in the tube-type hollow-core fibers. The anti-resonant core modes in the DCFs exhibit similar qualitative and quantitative behavior as the core modes in the conventional step-index fibers. The full-vector analytical results for the simple-structure DCFs can contribute to a better understanding of the anti-resonant and inhibited coupling guidance mechanisms in other complex inversed index fibers.

Miniature Fabry-Perot interferometer based on a movable microsphere reflector.

We propose and demonstrate a miniature Fabry-Perot interferometer (FPI) based on a movable microsphere reflector. The movable microsphere acts as a good reflector, with the reflections occurring at the spliced single-mode fiber/hollow-core fiber interface and the surface of a microsphere, resulting in two-beam interference. The silica microsphere is formed at the tip of a half-tapered optical fiber, and its diameter can be reduced to miniaturize the FPI. The movable microsphere interferometer exhibits a highly linear response to external displacement change, and a high displacement sensitivity of 11.9 pm/nm with a nanoscale resolution of 1.7 nm is achieved. Wide-range displacement can also be measured by monitoring the changes in the free spectral range of the reflection spectrum. Therefore, this miniaturized FPI may find use in applications in nano-displacement measurement fields, and the concept of a movable microsphere reflector is of great significance for the miniaturization of micro-photonic devices.

Ultrasensitive biosensor based on magnetic microspheres enhanced microfiber interferometer.

A critical barrier for the successful development of fiber sensors for bio-chemical processes is their limitedly improved sensitivity, restricted by the sensor structural design. To solve this, in this paper, a novel concept was proposed using functionalised modified magnetic microspheres (MMSs) to "amplify" the effect of target bio-chemical analytes to significantly improve the fiber sensor's sensitivity, which has been demonstrated using human chorionic gonadotropin (hCG) as an example. Two types of antibody hCG, (ß and α, both can specifically bind with hCG), were adhered on the surface of fibre sensor and MMSs respectively. Both hCG and MMSs will be specifically captured by the fibre sensor, where MMSs act as an "amplifier" to improve the sensor sensitivity. Experimentally immunomagnetic detection limit of 0.0001 mIU/mL has been achieved, which is the highest reported so far. This newly developed methodology opens a new direction for sensitivity improvement and could be further explored to applications require ultrahigh sensitivity detections such as earlier medical diagnostics.

Strain independent twist sensor based on uneven platinum coated hollow core fiber structure.

Optical fiber based twist sensors usually suffer from high cross sensitivity to strain. Here we report a strain independent twist sensor based on an uneven platinum coated hollow core fiber (HCF) structure. The sensor is fabricated by splicing a section of ~4.5-mm long HCF between two standard single mode fibers, followed by a sputter-coating of a very thin layer of platinum on both sides of the HCF surface. Experimental results demonstrate that twist angles can be measured by monitoring the strength change of transmission spectral dip. The sensor's cross sensitivity to strain is investigated before and after coating with platinum. It is found that by coating a platinum layer of ~9 nm on the HCF surface, the sensor's cross sensitivity to strain is significantly decreased with over two orders of magnitude less than that of the uncoated sensor sample. The lowest strain sensitivity of ~2.32×10-5 dB/𝜇𝛆 has been experimentally achieved, which is to the best of our knowledge, the lowest cross sensitivity to strain reported to date for optical fiber sensors based on intensity modulation. In addition, the proposed sensor is capable of simultaneous measurement of strain and twist angle by monitoring the wavelength shift and dip strength variation of a single spectral dip. In the experiment, strain and twist angle sensitivities of 0.61 pm/𝜇𝛆 and 0.10 dB/° have been achieved. Moreover, the proposed sensor offers advantages of ease of fabrication, miniature size, and a good repeatability of measurement.

Nanosecond passively Q-switched fibre laser using a NiS2 based saturable absorber.

Q-switched pulse laser generation is successfully demonstrated in both Erbium-doped fibre laser (EDFL) and Thulium-doped fibre laser (TDFL) cavities by employing Nickel disulfide (NiS2) as a saturable absorber (SA). Q-switched pulse laser operation at 1.55 µm and 2.0 µm is obtained at low pump power levels of 37 mW and 48 mW, respectively. For the EDFL, stable passively Q-switched laser output at a wavelength of 1561.86 nm is achieved, with a minimum pulse duration of 237 ns and a repetition rate of 243.9 kHz. For the TDFL, the centre wavelength of the laser output is 1915.5 nm, with a minimum pulse duration of 505 ns and a repetition rate of 214.68 kHz. NiS2 is used as SA for Q-switched laser generation over a broadband wavelength for the first time.