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Virtually epimerization-free synthesis of peptide-alpha-thioesters.
Hogenauer, Tyrone J; Wang, Qianli; Sanki, Aditya K; Gammon, Amy J; Chu, Cherie H L; Kaneshiro, Clyde M; Kajihara, Yasuhiro; Michael, Katja.
Org Biomol Chem ; 5(5): 759-62, 2007 Mar 07.
Article in English | MEDLINE | ID: mdl-17315060

ABSTRACT

Under slightly basic or neutral reaction conditions peptide-alpha-thioesters are photochemically synthesized from peptide-alpha-nitroindoline precursors, either in solution, or by direct photorelease from a solid support.


Subject(s)
Peptides/chemical synthesis , Sulfhydryl Compounds/chemical synthesis , Amino Acids/chemistry , Chromatography, High Pressure Liquid , Esters , Fluorenes/chemistry , Indoles/chemistry , Molecular Structure , Peptides/chemistry , Photochemistry , Sulfhydryl Compounds/chemistry
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