ABSTRACT
In recent times, nanomaterials (NMs) have gained significant attention for their unique properties and wide-ranging applications. This increased interest has driven research aimed at developing more efficient synthetic approaches in the fields of material science. Moreover, today's increasing demand for materials underscores the need for innovative technologies that can effectively scale up production to meet these growing needs. Hence, this review is primarily delve deeply into the template-assisted method i.e., an advance bottom-up approach for NMs synthesis. Furthermore, this review emphasizes to explore the advancements in soft template-based synthetic strategies for nanostructured materials as it provides high control on morphology and size. Therefore, this review specifically organized around on providing an in-depth discussion of the liquid/liquid interface-assisted soft template method, applications, and the factors affecting liquid/liquid interface for NMs synthesis. These key points are instrumental in driving advancements, highlighting the ongoing need for further enhancement and refinement of smart technologies. Finally, we conclude the review by describing the challenges and future perspectives of the liquid/liquid-assisted approach for NMs designing.