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Solvent free, microwave assisted conversion of aldehydes into nitriles and oximes in the presence of NH2OH x HCl and TiO2.
Hoelz, Lucas Villas-Boas; Gonçalves, Biank Tomaz; Barros, José Celestino; da Silva, Joaquim Fernando Mendes.
Molecules ; 15(1): 94-9, 2009 Dec 29.
Article in English | MEDLINE | ID: mdl-20110874

ABSTRACT

Aromatic aldehydes bearing electron-donating groups are easily converted into their respective nitriles using NH(2)OH.HCl and TiO(2) under microwave irradiation, while those bearing an electron-withdrawing group give the corresponding oximes.


Subject(s)
Aldehydes/chemistry , Hydrochloric Acid/chemistry , Hydroxides/chemistry , Microwaves , Nitriles/chemistry , Oximes/chemistry , Titanium/chemistry , Ammonium Hydroxide , Benzaldehydes/chemistry , Chromatography, Gas , Mass Spectrometry , Solvents/chemistry , Time Factors
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