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Inorg Chem ; 56(20): 12362-12368, 2017 Oct 16.
Article in English | MEDLINE | ID: mdl-28967746

ABSTRACT

Bismuth and antimony were reacted in sulfur/iodine flux mixtures at various temperatures and iodine concentrations to explore the effects of these variables on the synthesis and properties of Bi1-xSbxSI products. The products grow as crystals; microprobe elemental analysis and UV/vis/NIR spectroscopy of the Bi1-xSbxSI solid solutions indicate that substitution is homogeneous within individual crystals but varies up to 15% between crystals within each synthesis batch. Raman spectra show a two-mode behavior upon substitution, indicating covalent bonding within the structure, and TEM/SEM data confirm no presence of nanoclustering or segregation within the crystals.

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