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Solid State Nucl Magn Reson ; 23(1-2): 50-61, 2003.
Article in English | MEDLINE | ID: mdl-12633831

ABSTRACT

An economic approach for implementing X-[1H,19F] double-decoupling MAS NMR experiments with a conventional X-[1H] dual-channel CP MAS probe is demonstrated. The parameters characterising the isolated 29Si-19F spin pair in an organosilicon compound R(3)SiF (R = 9-anthryl) are determined. In addition, we discuss the optimum choice of experimental parameters for determining all 29Si-19F spin-pair parameters from straightforward 29Si MAS NMR spectra with only 1H decoupling applied during acquisition.


Subject(s)
Fluorine/chemistry , Hydrogen/chemistry , Magnetic Resonance Spectroscopy/methods , Protons , Silicon/chemistry , Crystallography/methods , Isotopes , Reproducibility of Results , Sensitivity and Specificity
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