1.
Rev Sci Instrum
; 79(8): 084103, 2008 Aug.
Article
in English
| MEDLINE
| ID: mdl-19044364
ABSTRACT
This paper reports a simple and efficient gas burette system that allows automated determination of evolved gas volume in real time using only temperature and pressure measurements. The system is reliable and has been used successfully to study the hydrogen release kinetics of ammonia borane thermolysis. The system is especially suitable for bench scale studies involving small batches and potentially rapid reaction kinetics.