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Mater Sci Eng C Mater Biol Appl ; 69: 850-5, 2016 Dec 01.
Article in English | MEDLINE | ID: mdl-27612779

ABSTRACT

This paper presents the synthesis of pure and europium-doped lutetium oxide (Lu2O3) powders prepared by sol-gel method. The influence of europium ion concentration into Lu2O3 nanocrystallites was investigated for first time in an in vitro system using a modified ABTS radical cation decolorization assay to determine the antioxidant activity. The crystalline structure of Lu2O3 and Eu:Lu2O3 powders was elucidated by XRD obtaining cubic phase in all system without secondary products in accordance with FT-IR results. By TEM and Scherrer equation, it was determined that Lu2O3 and Eu:Lu2O3 powders presented nearly spherical particle morphology with crystallites sizes in the range of 8 to 13nm. The antioxidant assays results revealed that europium ion enhance Lu2O3 powders antioxidant properties, showing that 12.5mol% of europium is sufficient to reach its maximum capacity.


Subject(s)
Antioxidants/pharmacology , Europium/chemistry , Lutetium/pharmacology , Nanoparticles/chemistry , Oxides/pharmacology , Phase Transition , Nanoparticles/ultrastructure , Spectroscopy, Fourier Transform Infrared , X-Ray Diffraction
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