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Chem Commun (Camb) ; 54(100): 14148-14151, 2018 Dec 13.
Article in English | MEDLINE | ID: mdl-30506077

ABSTRACT

A radical cascade cyclization of 2-alkynylthioanisoles with α-oxocarboxylic acids with AgNO3 has been described. This reaction provides a novel route to directly access 3-acylbenzothiophenes from simple chemical feedstocks. In particular, the utility of the approach was demonstrated by its application to the synthesis of a polymerization inhibitor and a raloxifene precursor.

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