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1.
Acta Crystallogr Sect E Struct Rep Online ; 68(Pt 8): o2328, 2012 Aug 01.
Article in English | MEDLINE | ID: mdl-22904800

ABSTRACT

In the title compound, C(31)H(40)NO(2)P, the P atom has a distorted tetra-hedral stereochemistry [bond-angle range about P = 103.33 (6)-115.24 (15)°] and has R(P) chirality, which was confirmed crystallographically. The dihedral angles between the P-bonded phenyl ring and the other two phenyl rings are 40.4 (3) and 12.2 (2)°. In the crystal, a C-H⋯O inter-action links mol-ecules into chains which extend along [100].

2.
Acta Crystallogr Sect E Struct Rep Online ; 68(Pt 7): o2220, 2012 Jul 01.
Article in English | MEDLINE | ID: mdl-22798879

ABSTRACT

In the mol-ecule of the title compound, C(22)H(23)NO, there are two chiral atoms (R* for the C atom attached to the OH group and S* for the C atom attached to the phenyl ring). In the crystal, neighbouring mol-ecules are connected into a chain along the b axis by N-H⋯O hydrogen bonds.

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