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Magn Reson Chem ; 48(5): 409-15, 2010 May.
Article in English | MEDLINE | ID: mdl-20301093

ABSTRACT

Bioactive cage-like polycyclic compounds have attracted the attention of several research groups because of their unique appearance and their biological activities. Their structures were established on the basis of (1)H NMR and (13)C NMR spectroscopic data. The (1)H and (13)C signal assignments and most homonuclear hydrogen coupling constants were assigned by use of techniques such as 1D (1)H and (13)C NMR and 2D gCOSY, non-edited gHSQC and gHMBC. The gNOESY experiments proved the endo-stereochemistry.


Subject(s)
Magnetic Resonance Spectroscopy/methods , Polycyclic Compounds/chemistry , Carbon Isotopes , Protons
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