Transient rhyolite melt extraction to produce a shallow granitic pluton.

Rhyolitic melt that fuels explosive eruptions often originates in the upper crust via extraction from crystal-rich sources, implying an evolutionary link between volcanism and residual plutonism. However, the time scales over which these systems evolve are mainly understood through erupted deposits, limiting confirmation of this connection. Exhumed plutons that preserve a record of high-silica melt segregation provide a critical subvolcanic perspective on rhyolite generation, permitting comparison between time scales of long-term assembly and transient melt extraction events. Here, U-Pb zircon petrochronology and 40Ar/39Ar thermochronology constrain silicic melt segregation and residual cumulate formation in a ~7 to 6 Ma, shallow (3 to 7 km depth) Andean pluton. Thermo-petrological simulations linked to a zircon saturation model map spatiotemporal melt flux distributions. Our findings suggest that ~50 km3 of rhyolitic melt was extracted in ~130 ka, transient pluton assembly that indicates the thermal viability of advanced magma differentiation in the upper crust.

100 Ma sweat bee nests: Early and rapid co-diversification of crown bees and flowering plants.

100 Ma sweat bee nests reported herein are the oldest evidence of crown bees. A new phylogeny for short-tongued bees, calibrated with these nests dated with 40Ar/39Ar, attests for the first time for a late Albian rapid diversification of bees along with angiosperms. Such hypothesis lacked paleontological support until this study. The new ichnospecies Cellicalichnus krausei, which was found along with wasp trace fossils and new beetle trace fossils in the Castillo Formation of Patagonia, represents typical Halictini nests composed of sessile cells that are attached to main tunnels. According to geological, paleosol, paleobotanical, and ichnological data, bees, and angiosperms cohabited in an inland and dry environment comparable to an open dry woodland or savanna, under warm-temperate and semiarid-subhumid climate, in the Southern Hemisphere by the Albian.

Synchronizing volcanic, sedimentary, and ice core records of Earth's last magnetic polarity reversal.

Reversal of Earth's magnetic field polarity every 105 to 106 years is among the most far-reaching, yet enigmatic, geophysical phenomena. The short duration of reversals make precise temporal records of past magnetic field behavior paramount to understanding the processes that produce them. We correlate new 40Ar/39Ar dates from transitionally magnetized lava flows to astronomically dated sediment and ice records to map the evolution of Earth's last reversal. The final 180° polarity reversal at ~773 ka culminates a complex process beginning at ~795 ka with weakening of the field, succeeded by increased field intensity manifested in sediments and ice, and then by an excursion and weakening of intensity at ~784 ka that heralds a >10 ka period wherein sediments record highly variable directions. The 22 ka evolution of this reversal suggested by our findings is mirrored by a numerical geodynamo simulation that may capture much of the naturally observed reversal process.

A new tephrochronology for early diverse stone tool technologies and long-distance raw material transport in the Middle to Late Pleistocene Kapthurin Formation, East Africa.

The Middle to Late Pleistocene (780-10 ka) of East Africa records evidence of significant behavioral change, early fossils of Homo sapiens, and the dispersals of our species across and out of Africa. Studying human evolution in this time period thus requires an extensive and precise chronology relating behavioral evidence from archaeological sequences to aspects of hominin biology and evidence of past environments from fossils and geological sequences. Tephrochronology provides the chronostratigraphic resolution to achieve this through correlation and dating of volcanic ashes. The tephrochronology of the Kapthurin Formation presented here, based on tephra correlations and 40Ar/39Ar dates, provides new ages between 395.6 ± 3.5 ka and 465.3 ± 1.0 ka for nine sites showing diverse blade and Levallois methods of core reduction. These are >110 kyr older than previously known in East Africa. New 40Ar/39Ar dates provide a refined age of 222.5 ± 0.6 ka for early evidence of long-distance (166 km) obsidian transport at the Sibilo School Road Site. A tephra correlation between the Baringo and Victoria basins also provides a new date of ∼100 ka for the Middle Stone Age site of Keraswanin. By providing new and older dates for 11 sites containing several important aspects of hominin behavior and extending the chronology of the Kapthurin Formation forward by ∼130,000 years, the tephrochronology presented here contributes one of the longest and most refined chronostratigraphic frameworks of Middle through Late Pleistocene East Africa. This tephrochronology thus provides the foundation to understand the process of modern human behavioral evolution as it relates to biological and paleoenvironmental circumstances.

Incremental heating of Bishop Tuff sanidine reveals preeruptive radiogenic Ar and rapid remobilization from cold storage.

Accurate and precise ages of large silicic eruptions are critical to calibrating the geologic timescale and gauging the tempo of changes in climate, biologic evolution, and magmatic processes throughout Earth history. The conventional approach to dating these eruptive products using the 40Ar/39Ar method is to fuse dozens of individual feldspar crystals. However, dispersion of fusion dates is common and interpretation is complicated by increasingly precise data obtained via multicollector mass spectrometry. Incremental heating of 49 individual Bishop Tuff (BT) sanidine crystals produces 40Ar/39Ar dates with reduced dispersion, yet we find a 16-ky range of plateau dates that is not attributable to excess Ar. We interpret this dispersion to reflect cooling of the magma reservoir margins below ∼475 °C, accumulation of radiogenic Ar, and rapid preeruption remobilization. Accordingly, these data elucidate the recycling of subsolidus material into voluminous rhyolite magma reservoirs and the effect of preeruptive magmatic processes on the 40Ar/39Ar system. The youngest sanidine dates, likely the most representative of the BT eruption age, yield a weighted mean of 764.8 ± 0.3/0.6 ka (2σ analytical/full uncertainty) indicating eruption only ∼7 ky following the Matuyama-Brunhes magnetic polarity reversal. Single-crystal incremental heating provides leverage with which to interpret complex populations of 40Ar/39Ar sanidine and U-Pb zircon dates and a substantially improved capability to resolve the timing and causal relationship of events in the geologic record.

40Ar/39Ar dating of Glacial Termination VI: constraints on the duration of Marine Isotopic Stage 13.

We present four new 40Ar/39Ar ages of tephra layers from an aggradational succession (Valle Giulia Formation) near the mouth of the Tiber Valley in Rome that was deposited in response to sea-level rise during Marine Isotopic Stage (MIS) 13. These new ages, integrated with seven previously determined ages, provide the only extant independent, radioisotopic age constraint on glacial termination VI and on the duration of MIS 13 sea-level rise. The new geochronologic constraints suggest a long duration for the period of sea-level rise (533 ± 2 through 498 ± 2 ka) encompassing two consecutive positive peaks of the δ18O curve (substages 13.3 and 13.1). Consistently, the litho-stratigraphic features of the sedimentary record account for two aggradational phases separated by an intervening erosional phase. Moreover, the ages obtained for this study give us the opportunity to compare the timing of the sea-level fluctuations inferred from the stratigraphic record and that provided by the astrochronologic calibration of the Oxygen isotopic curves, and to assess the calibrations of 40Ar/39Ar standards. Results of this comparison indicate that the best match is for an age of 1.186 Ma for the Alder Creek Rhyolite sanidine and 28.201 Ma for the Fish Canyon Tuff sanidine.

Structural and temporal requirements for geomagnetic field reversal deduced from lava flows.

Reversals of the Earth's magnetic field reflect changes in the geodynamo--flow within the outer core--that generates the field. Constraining core processes or mantle properties that induce or modulate reversals requires knowing the timing and morphology of field changes that precede and accompany these reversals. But the short duration of transitional field states and fragmentary nature of even the best palaeomagnetic records make it difficult to provide a timeline for the reversal process. 40Ar/39Ar dating of lavas on Tahiti, long thought to record the primary part of the most recent 'Matuyama-Brunhes' reversal, gives an age of 795 +/- 7 kyr, indistinguishable from that of lavas in Chile and La Palma that record a transition in the Earth's magnetic field, but older than the accepted age for the reversal. Only the 'transitional' lavas on Maui and one from La Palma (dated at 776 +/- 2 kyr), agree with the astronomical age for the reversal. Here we propose that the older lavas record the onset of a geodynamo process, which only on occasion would result in polarity change. This initial instability, associated with the first of two decreases in field intensity, began approximately 18 kyr before the actual polarity switch. These data support the claim that complete reversals require a significant period for magnetic flux to escape from the solid inner core and sufficiently weaken its stabilizing effect.