ABSTRACT
The title and the chemical diagram of the paper by Kang, Li, Zeng, Wang & Wang [Acta Cryst. (2007), E63, o4654] are corrected.[This corrects the article DOI: 10.1107/S1600536807055559.].
ABSTRACT
In the mol-ecule of the title compound, C(11)H(12)BrNO(2), a weak intra-molecular C-Hâ¯Br hydrogen bond results in the formation of a five-membered ring, which adopts an envelope conformation with the H atom displaced by 0.486â Å from the plane of the other ring atoms. In the crystal structure, inter-molecular C-Hâ¯O hydrogen bonds link the mol-ecules.
ABSTRACT
The molecule of the title compound, C(10)H(13)NO(3), is approximately planar. A network of N-Hâ¯O and weak C-Hâ¯O hydrogen bonds helps to consolidate the crystal structure.
ABSTRACT
In the title compound, C(8)H(7)ClFNO, an intra-molecular C-Hâ¯O hydrogen bond forms a six-membered ring. In the crystal structure, mol-ecules are linked by inter-molecular N-Hâ¯O hydrogen bonds, forming infinite chains along the c axis.
ABSTRACT
In the title compound, C(28)H(28)N(4)O(4)S, the dihedral angles between the central thio-phene ring and its pendant oxadiazole rings are 1.2â (3) and 9.8â (3)°. The dihedral angles between the oxadiazole and phenyl rings are 2.9â (3) and 1.8â (3)°. Some short intra-molecular C-Hâ¯O contacts occur.
ABSTRACT
In the mol-ecule of the title compound, C(8)H(11)N(7)S(2), the conformation about the N=N bond is trans and the thia-diazole rings are oriented at a dihedral angle of 2.92â (3)°. In the crystal structure, inter-molecular N-Hâ¯S hydrogen bonds link the mol-ecules into chains. There are π-π contacts between the thia-diazole rings [centroid-to-centroid distances = 3.699â (3) and 3.720â (2)â Å].
ABSTRACT
The asymmetric unit of the title compound, C(9)H(8)N(2)O(2), contains two mol-ecules. In the crystal structure, both mol-ecules form inversion dimers via pairs of O-Hâ¯O hydrogen bonds, and a C-Hâ¯O inter-ation is also seen.