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Dalton Trans ; 42(44): 15540-3, 2013 Nov 28.
Article in English | MEDLINE | ID: mdl-24056388

ABSTRACT

Technetium disulfide was prepared by reaction between the elements in a sealed tube at 450 °C, by reaction between Tc2(O2CCH3)5 and H2S gas in a flowing system at 450 °C and by reaction between K2TcCl6 and H2S gas in sulfuric acid. The samples were analysed by X-ray absorption fine structure (XAFS) spectroscopy.

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