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Annealing effect on the microstructure and electrochemical properties of Fe2O3/H-TiNT/FTO thin film.
J Nanosci Nanotechnol
; 13(3): 1863-6, 2013 Mar.
Article
in English
| MEDLINE
| ID: mdl-23755607
ABSTRACT
A layer of titanate nanotubular (H-TiNT) particles between Fe2O3 film and FTO substrate was inserted and heat-treated to improve electrochemical property of Fe2O3 for water splitting. Heat-treatment of the synthesized F2O3/H-TiNT/FTO thin film was found to significantly affect photoelectrochemical properties of the film through electrochemical impedance analysis. The film showed larger oxidation-reduction peaks of I-V characteristics and capacitive properties under UV-Vis light illumination with heat treatment temperatures during transformation of H-TiNT into anatase TiO2 phase. The overall results showed an appropriate heat treatment was a promising way to improve the electrochemical property of the photoanode film.