Contactless and Vibration-Based Damage Detection in Rectangular Cement Beams Using Magnetoelastic Ribbon Sensors.

This study investigated the innovative use of magnetoelastic sensors to detect the formation of single cracks in cement beams under bending vibrations. The detection method involved monitoring changes in the bending mode spectrum when a crack was introduced. The sensors, functioning as strain sensors, were placed on the beams, and their signals were detected non-invasively using a nearby detection coil. The beams were simply supported, and mechanical impulse excitation was applied. The recorded spectra displayed three distinct peaks representing different bending modes. The sensitivity for crack detection was determined to be a 24% change in the sensing signal for every 1% decrease in beam volume due to the crack. Factors influencing the spectra were investigated, including pre-annealing of the sensors, which improved the detection signal. The choice of beam support material was also explored, revealing that steel yielded better results than wood. Overall, the experiments demonstrated that magnetoelastic sensors enabled the detection of small cracks and provided qualitative information about their location.

Magnetoelastic Ribbons as Vibration Sensors for Real-Time Health Monitoring of Rotating Metal Beams.

In the current work, magnetoelastic material ribbons are used as vibration sensors to monitor, in real time and non-destructively, the mechanical health state of rotating beam blades. The magnetoelastic material has the form of a thin ribbon and is composed of Metglas alloy 2826 MB. The study was conducted in two stages. In the first stage, an experiment was performed to test the ability of the ribbon to detect and transmit the vibration behavior of four rotating blades, while the second stage was the same as the first but with minor damages introduced to the blades. As far as the first stage is concerned, the results show that the sensor can detect and transmit with great accuracy the vibratory behavior of the rotating blades, through which important information about the mechanical health state of the blade can be extracted. Specifically, the fast Fourier transform (FFT) spectrum of the recorded signal revealed five dominant peaks in the frequency range 0-3 kHz, corresponding to the first five bending modes of the blades. The identification process was accomplished using ANSYS modal analysis, and the comparison results showed deviation values of less than 1% between ANSYS and the experimental values. In the second stage, two types of damages were introduced to the rotating blades, an edge cut and a hole. The damages were scaled in number from one blade to another, with the first blade having only one side cut while the last blade had two side cuts and two holes. The results, as was expected, show a measurable shifting on the frequency values of the bending modes, thus proving the ability of the proposed magnetoelastic sensors to detect and transmit changes of the mechanical state of rotating blades in real time.

A New Method for the Measurement of the Diffusion Coefficient of Adsorbed Vapors in Thin Zeolite Films, Based on Magnetoelastic Sensors.

In the current work an experimental method is used in order to calculate the diffusivity D (diffusion coefficient) of various vapors in thin zeolite films. The method is based on adsorption data from magnetoelastic sensors on top of which a zeolite layer was synthesized, and the diffusivity is extracted by fitting the data to Fick's laws of diffusion. In particular, the method is demonstrated for two volatile organic compound (VOC) vapors on two different zeolites, the p-Xylene adsorption in Faujasite type zeolite with D=1.89×10-13 m2/s at 120 °C and the propene adsorption in Linde Type A type zeolite with D=5.9×10-14 m2/s at 80 °C, two diffusion coefficients which are extracted experimentally for first time. Our results are within the order of magnitude of other VOC/zeolite values reported in literature.

Accurate Determination of the Q Quality Factor in Magnetoelastic Resonant Platforms for Advanced Biological Detection.

The main parameters of magnetoelastic resonators in the detection of chemical (i.e., salts, gases, etc.) or biological (i.e., bacteria, phages, etc.) agents are the sensitivity S (or external agent change magnitude per Hz change in the resonance frequency) and the quality factor Q of the resonance. We present an extensive study on the experimental determination of the Q factor in such magnetoelastic resonant platforms, using three different strategies: (a) analyzing the real and imaginary components of the susceptibility at resonance; (b) numerical fitting of the modulus of the susceptibility; (c) using an exact mathematical expression for the real part of the susceptibility. Q values obtained by the three methods are analyzed and discussed, aiming to establish the most adequate one to accurately determine the quality factor of the magnetoelastic resonance.

Nanostructured ZnO in a Metglas/ZnO/Hemoglobin Modified Electrode to Detect the Oxidation of the Hemoglobin Simultaneously by Cyclic Voltammetry and Magnetoelastic Resonance.

In the present work, a nanostructured ZnO layer was synthesized onto a Metglas magnetoelastic ribbon to immobilize hemoglobin (Hb) on it and study the Hb's electrochemical behavior towards hydrogen peroxide. Hb oxidation by H2O2 was monitored simultaneously by two different techniques: Cyclic Voltammetry (CV) and Magnetoelastic Resonance (MR). The Metglas/ZnO/Hb system was simultaneously used as a working electrode for the CV scans and as a magnetoelastic sensor excited by external coils, which drive it to resonance and interrogate it. The ZnO nanoparticles for the ZnO layer were grown hydrothermally and fully characterized by X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and photoluminescence (PL). Additionally, the ZnO layer's elastic modulus was measured using a new method, which makes use of the Metglas substrate. For the detection experiments, the electrochemical cell was performed with a glass vial, where the three electrodes (working, counter and reference) were immersed into PBS (Phosphate Buffer Solution) solution and small H2O2 drops were added, one at a time. CV scans were taken every 30 s and 5 min after the addition of each drop and meanwhile a magnetoelastic measurement was taken by the external coils. The CV plots reveal direct electrochemical behavior of Hb and display good electrocatalytic response to the reduction of H2O2. The measured catalysis currents increase linearly with the H2O2 concentration in a wide range of 25-350 µM with a correlation coefficient 0.99. The detection limit is 25-50 µM. Moreover, the Metglas/ZnO/Hb electrode displays rapid response (30 s) to H2O2, and exhibits good stability and reproducibility of the measurements. On the other hand, the magnetoelastic measurements show a small linear mass increase versus the H2O2 concentration with a slope of 152 ng/µM, which is probably due to H2O2 adsorption in ZnO during the electrochemical reaction. No such effects were detected during the control experiment when only PBS solution was present for a long time.

Ninety-degree chevron osteotomy for correction of hallux valgus deformity: clinical data and finite element analysis.

Hallux valgus is a very common foot disorder, with its prevalence estimated at 33% in adult shoe-wearing populations. Conservative management is the initial treatment of choice for this condition, but surgery is sometimes needed. The 60(0) angle Chevron osteotomy is an accepted method for correction of mild to moderate hallux valgus in adults less than 60 years old. A modified 90(0) angle Chevron osteotomy has also been described; this modified technique can confer some advantages compared to the 60(0) angle method, and reported results are good. In the current work we present clinical data from a cohort of fifty-one female patients who had surgery for sixty-two hallux valgus deformities. In addition, in order to get a better physical insight and study the mechanical stresses along the two osteotomies, Finite Element Analysis (FEA) was also conducted. FEA indicated enhanced mechanical bonding with the modified 90(0) Chevron osteotomy, because the compressive stresses that keep the two bone parts together are stronger, and the shearing stresses that tend to slide the two bone parts apart are weaker, compared to the typical 60(0) technique. Follow-up data on our patient cohort show good or excellent long-term clinical results with the modified 90(0) angle technique. These results are consistent with the FEA-based hypothesis that a 90(0) Chevron osteotomy confers certain mechanical advantages compared to the typical 60(0) procedure.

Monitoring blood coagulation with magnetoelastic sensors.

The determination of blood coagulation time is an essential part of monitoring therapeutic anticoagulants. Standard methodologies for the measurement of blood clotting time require dedicated personnel and involve blood sampling procedures. A new method based on magnetoelastic sensors has been employed for the monitoring of blood coagulation. The ribbon-like magnetoelastic sensor oscillates at a fundamental frequency, which shifts linearly in response to applied mass loads or a fixed mass load of changing elasticity. The magnetoelastic sensors emit magnetic flux, which can be detected by a remotely located pick-up coil, so that no direct physical connections are required. During blood coagulation, the viscosity of blood changes due to the formation of a soft fibrin clot. In turn, this change in viscosity shifts the characteristic resonance frequency of the magnetoelastic sensor enabling real-time continuous monitoring of this biological event. By monitoring the signal output as a function of time, a distinct blood clotting profile can be seen. The relatively low cost of the magnetoelastic ribbons enables their use as disposable sensors. This, along with the reduced volume of blood required, make the magnetoelastic sensors well suited for at-home and point-of-care testing devices.