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2.
Nat Commun ; 13(1): 5119, 2022 Aug 31.
Article in English | MEDLINE | ID: mdl-36045129

ABSTRACT

Ice accretion causes problems in vital industries and has been addressed over the past decades with either passive or active de-icing systems. This work presents a smart, hybrid (passive and active) de-icing system through the combination of a low interfacial toughness coating, printed circuit board heaters, and an ice-detecting microwave sensor. The coating's interfacial toughness with ice is found to be temperature dependent and can be modulated using the embedded heaters. Accordingly, de-icing is realized without melting the interface. The synergistic combination of the low interfacial toughness coating and periodic heaters results in a greater de-icing power density than a full-coverage heater system. The hybrid de-icing system also shows durability towards repeated icing/de-icing, mechanical abrasion, outdoor exposure, and chemical contamination. A non-contact planar microwave resonator sensor is additionally designed and implemented to precisely detect the presence or absence of water or ice on the surface while operating beneath the coating, further enhancing the system's energy efficiency. Scalability of the smart coating is demonstrated using large (up to 1 m) iced interfaces. Overall, the smart hybrid system designed here offers a paradigm shift in de-icing that can efficiently render a surface ice-free without the need for energetically expensive interface melting.

3.
Sci Rep ; 11(1): 13707, 2021 Jul 01.
Article in English | MEDLINE | ID: mdl-34211060

ABSTRACT

A patch antenna sensor with T-shaped slots operating at 2.378 GHz was developed and investigated for wireless ice and frost detection applications. Detection was performed by monitoring the resonant amplitude and resonant frequency of the transmission coefficient between the antenna sensor and a wide band receiver. This sensor was capable of distinguishing between frost, ice, and water with total shifts in resonant frequency of 32 MHz and 36 MHz in the presence of frost and ice, respectively, when compared to the bare sensor. Additionally, the antenna was sensitive to both ice thickness and the surface area covered in ice displaying resonant frequency shifts of 2 MHz and 8 MHz respectively between 80 and 160 µL of ice. By fitting an exponential function to the recorded data, the freezing rate was also extracted. The analysis within this work distinguishes the antenna sensor as a highly accurate and robust method for wireless ice accretion detection and monitoring. This technology has applications in a variety of industries including the energy sector for detection of ice on wind turbines and power lines.

4.
ACS Appl Mater Interfaces ; 12(49): 55483-55492, 2020 Dec 09.
Article in English | MEDLINE | ID: mdl-33241686

ABSTRACT

Ice accumulation on aircraft is known to negatively impact the aerodynamic and mechanical operation, sometimes resulting in catastrophic failure. Recently, microwave resonators have gained interest as durable and reliable frost and ice detectors. Here, a microwave resonator sensor with built-in heating capability patterned into the ground plane was designed, fabricated, and tested to investigate real-time ice and frost growth. Sensing was performed on surfaces with anti-icing coatings to quantitatively analyze the effectiveness of these materials. The sensor was also tested to determine its ability to evaluate different deicing methods. The sensor itself was a split-ring resonator (SRR) operating at 5.82 GHz, which could effectively distinguish between water and ice by detecting changes in the dielectric properties on or around its surface. This application was particularly suited for an SRR due to the extreme difference between the relative permittivity of water (ε = 90) and ice (ε = 3.2) at 5 GHz and 0 °C. The results from this sensor can be used to determine the holdover time of various coatings to resist ice formation. This study validates the use of SRRs as ice detection sensors for applications where ice and frost are of great interest, such as on aircraft, roads, or walkways.

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