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1.
Anal Bioanal Chem ; 405(12): 4225-34, 2013 May.
Article in English | MEDLINE | ID: mdl-23503732

ABSTRACT

Two kinds (20 each) of gamma-irradiated (0, 5, and 10 kGy) tea samples, blended powders and packed in sachets (tea bags), were investigated using photostimulated luminescence (PSL), thermoluminescence (TL), and electron spin resonance spectroscopy (ESR) to identify their irradiation status. PSL-based rapid screening was possible for all the control samples except for one packed and two powdered samples. The irradiated samples presented a good dose-dependent PSL count except two powdered samples with very low PSL sensitivity. TL analysis provided the most reliable results, in which all the irradiated samples were identified using a well-defined high-intensity TL glow curve in a temperature range of 150-250 °C. The TL results were also confirmed by determining the TL ratio (TL1/TL2), which was <0.1 in all the non-irradiated samples and >0.1 in the irradiated ones. ESR spectroscopy was effective for only 3 packed and 6 powdered samples showing the radiation-induced cellulosic and sugar radical signals, respectively.


Subject(s)
Food Irradiation/methods , Free Radicals/analysis , Tea/chemistry , Tea/radiation effects , Electron Spin Resonance Spectroscopy , Gamma Rays , Luminescence , Luminescent Measurements
2.
J Food Prot ; 67(1): 168-71, 2004 Jan.
Article in English | MEDLINE | ID: mdl-14717368

ABSTRACT

The combined effects of organic acids and irradiation on shelf life of pork loins were examined. Fresh pork loins were sprayed with organic acids (lactic, citric, and acetic) at 2%, packaged aerobically, and irradiated with an electron beam at 1, 2, and 3 kGy. During 14 days of storage, total plate count, coliform number, pH, and thiobarbituric acid-reactive substances were measured. Combinations of organic acid and irradiation were more effective in reducing and maintaining low total plate counts and coliform levels during storage than either treatment alone. Higher lipid oxidations were observed in all combination treatments at 1 day of storage than in the irradiation-only group. However, lower lipid oxidations were the result after 14 days of storage when combination treatments were used with irradiations of 2 and 3 kGy. Combined treatments involving lower irradiation doses than those required for irradiation alone could be used to extend the shelf life of pork loins during postirradiation storage without increasing lipid oxidation.


Subject(s)
Food Handling/methods , Food Irradiation , Food Preservation/methods , Meat/microbiology , Acetic Acid/pharmacology , Animals , Citric Acid/pharmacology , Cold Temperature , Colony Count, Microbial , Dose-Response Relationship, Radiation , Hydrogen-Ion Concentration , Lactic Acid/pharmacology , Lipid Metabolism , Swine , Thiobarbituric Acid Reactive Substances/analysis , Time Factors
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