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1.
Braz J Med Biol Res ; 29(12): 1641-4, 1996 Dec.
Article in English | MEDLINE | ID: mdl-9222425

ABSTRACT

A simple method for the preparation of rabbit antiserum against human von Willebrand factor (vWF) from commercial lyophilized factor VIII concentrate is described. vWF antigen (vWFAg)-like protein was obtained by gel filtration of the concentrate on Sepharose 4B. A combination of measurements of protein content by absorbance at 280 nm, and of vWFAg by electroimmunoassay using a commercial antibody, provided the data needed to select the Sepharose-filtered fractions with the highest concentrations of vWFAg-like protein. The immunization scheme used induced high antibody titers from the 45th to the 126th day after the first immunization. The resulting antiserum showed a performance similar to that of a commercial preparation in terms of vWFAg determination by electroimmunoassay and two-dimensional crossed-immunoelectrophoresis.


Subject(s)
Immune Sera , von Willebrand Factor/analysis , Animals , Humans , Rabbits , von Willebrand Factor/immunology
2.
Rev. bras. pesqui. méd. biol ; Braz. j. med. biol. res;29(12): 1641-4, Dec. 1996. tab, graf
Article in English | LILACS | ID: lil-188447

ABSTRACT

A simple method for the preparation of rabbit antiserum against human von Willebrand factor (vWF) from commercial lyophilized factor VIII concentrate is described. vWF antigen (vWFAg)-like protein was obtained by gel filtration of the concentrate on Sepharose 4BTM. A combination of measurements of protein content by absorbance at 280 nm, and of vWFAg by electroimmunoassay using a commercial antibody, provided the data needed to select the Sepharosefiltered fractions with the highest concentrations of vWFAg-like protein. The immunization scheme used induced high antibody titers from the 45th to the 126th day after the first immunization. The resulting antiserum showed a performance similar to that of a commercial preparation in terms of vWFAg determination by electroimmunoassay and two-dimensional crossed-immunoelectrophoresis.


Subject(s)
Rabbits , Animals , Blood Proteins/analysis , Immune Sera , von Willebrand Factor/immunology , Immunization/methods , Sepharose
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