Retentive strength and marginal discrepancies of a ceramic-reinforced calcium phosphate luting agent: An in vitro pilot study.

STATEMENT OF PROBLEM: Information on the properties of a relatively new luting agent with a unique formulation (ceramic-reinforced calcium phosphate) is limited. PURPOSE: The purpose of this in vitro study was to compare the retentive strengths and marginal discrepancies of a ceramic-reinforced calcium phosphate luting agent (CM) with a self-adhesive resin luting agent (RX) and to determine and compare the mode of failure of dislodged cemented copings. MATERIAL AND METHODS: Forty extracted human molar teeth were prepared to receive zirconia copings. After cementation, the specimens were divided into 4 subgroups (n=10): CM A (axial loading), CM OA (off-axis loading), RX A (axial loading), and RX OA (off-axis loading). For each subgroup, 9 of the specimens received experimental treatment (thermocycling and dynamic loading), and the tenth received no experimental treatment. Eight copings were pulled off in a universal testing machine (MTS Insight; MTS). The ninth specimen was treated experimentally but was not pull tested. The marginal discrepancy and the dentin interface of the specimens that were not pull tested were analyzed with scanning electron microscopy and energy dispersion spectroscopy. The mode of failure of the dislodged copings was also subjectively evaluated. RESULTS: The mean retentive strengths were 5.92 MPa for CM A, 5.81 MPa for CM OA, 5.75 MPa for RX A, and 5.69 MPa for RX OA. The marginal discrepancy recorded for both CM and RX ranged from 30 to 45 µm, (mean, 36 ±4.6 µm). Energy dispersion spectroscopy analysis showed the presence of calcium, phosphorus, silicon, and aluminum for the CM marginal discrepancy and the presence of aluminum in the dentinal tubules adjacent to the CM. Calcium and phosphorus were detected in lesser amounts adjacent to the RX marginal discrepancy. The mode of failure for CM was primarily adhesive to the tooth preparation, and, for RX, the failure mode was predominantly adhesive to the coping. CONCLUSIONS: CM had statistically significantly higher mean retentive strength compared with RX. Subgroups loaded axially had statistically significantly higher retentive strengths compared with those loaded off axis.

Analysis of dimensional changes in the screw and the surface topography at the interface of a titanium screw and a zirconia abutment under cyclic loading: an in vitro study.

PURPOSE: The purpose of this experiment was to analyze the mechanics of the ceramic abutment-implant joint and the dimensional changes in the abutment screws from cyclic loading. MATERIALS AND METHODS: Two groups of experimental assemblies were used, one with zirconia abutments and the other with titanium abutments (n = 10). Each specimen consisted of an implant, an abutment, and a metal crown affixed in an acrylic resin base. The specimens were subjected to cyclic loading of 200 N for 1 million cycles at 10 Hz. After loading, a torque-angle signature analysis was done, the dimensions of the screws were measured, and the implant-abutment interfaces were examined with scanning electron microscopy. RESULTS: There was a statistically significant increase in the total length of the screws: 121 µm in the titanium group versus 88 µm in the zirconia group (P < .004). Microscopic analysis showed collected debris on the zirconia abutment undersurface and the screws. A statistically similar decrease in torque was observed: 18% for zirconia versus 13.5% for titanium. Radiographic microanalysis revealed that the debris collected in the zirconia assemblies was essentially a collection of titanium, vanadium, and aluminum, with traces of zirconium. CONCLUSIONS: While there was a loss of torque in both types of abutments, the stability of the zirconia abutment-implant joint was not affected by the loading. The study provides a better understanding of zirconia abutments, screw designs, and the mechanism holding together the implant-abutment assembly.