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Molecules ; 15(8): 5369-77, 2010 Aug 05.
Article in English | MEDLINE | ID: mdl-20714302

ABSTRACT

The novel carbon based acid has been synthesized via one-step hydrothermal carbonization of furaldehyde and hydroxyethylsulfonic acid. A highly efficient procedure for the synthesis of fructone has been developed using the novel carbon based acid. The results showed that the catalyst possessed high activity for the reaction, giving a yield of over 95%. The advantages of high activity, stability, reusability and low cost for a simple synthesis procedure and wide applicability to various diols and beta-keto esters make this novel carbon based acid one of the best choices for the reaction.


Subject(s)
Acetoacetates/chemistry , Carbon/chemistry , Chemistry, Organic/methods , Heterocyclic Compounds, 1-Ring/chemical synthesis , Isethionic Acid/chemistry , Ketones/chemical synthesis , Perfume/chemical synthesis , Alcohols/chemistry , Catalysis , Esters/chemistry , Heterocyclic Compounds, 1-Ring/chemistry , Ketones/chemistry , Microscopy, Electron, Scanning , Perfume/chemistry , Solvents/chemistry , Spectrophotometry, Infrared , Time Factors
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