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1.
Materials (Basel) ; 16(24)2023 Dec 05.
Article in English | MEDLINE | ID: mdl-38138663

ABSTRACT

In this paper, the mechanical properties of various zones of the welded joints of a heat-resistant steel 15Kh1M1F in different states (in the initial state, after an operation on the main steam piping of a thermal power plant (TPP) for 23 years) were determined, and the fracture surfaces were analyzed using scanning electron microscopy (SEM) images. The effect of hydrogen electrolytic charging on mechanical behavior and fracture mechanism was also studied. The long-term operation of welds resulted in a higher degradation degree of the weld metal compared to the base one, indicated by the deterioration of mechanical properties: decrease in hardness, strength characteristics, and reduction in area, which was accompanied by an atypical increase in elongation at fracture. All studied zones of the operated welded joints were characterized by higher hydrogen content, 2.5-3 times higher than that in the initial state. Additional hydrogen charging of the weld joint metal led to a decrease in the strength and ductility characteristics, more significantly for the operated weld compared with the non-operated one. This justified the possibility of using short-term tests of hydrogenated WM in the air to assess the degree of its damage during operation on a steam piping.

2.
Materials (Basel) ; 15(16)2022 Aug 19.
Article in English | MEDLINE | ID: mdl-36013858

ABSTRACT

The main regularities in the impact of varying intensity impact-oscillatory loading on the variation of the mechanical and structural properties of the VT23 high-strength two-phase transverse-rolled sheet titanium alloy have been found. The intensity of the impulse introduction of energy into the alloy under the dynamic non-equilibrium process (DNP) was estimated by εimp (the increment of dynamic strain). The pulse intensity was found to change the shape of the static strain diagram with further tensioning, as compared to the initial state. This indicates the effect from the structure self-organization inherent in the VT23 titanium alloy upon the DNP. After the DNP (εimp = 1.44%), with further static deformation, the tensile diagram revealed yield sites up to 6.5% long. In most cases, the DNP was found to have a negative effect on the variation of the mechanical properties of the VT23 titanium alloy, especially if the latter was rolled in the transverse direction. The optimal DNP intensity is εimp~1.5%. In this case, the DNP can be used as an effective plasticization technology for the VT23 titanium alloy (regardless of the rolling direction) in the stamping of high-strength titanium alloys. Changes in the mechanical and structural condition of the VT23 titanium alloy subjected to the DNP were confirmed by the fractographic investigation of specimen fractures.

3.
Materials (Basel) ; 16(1)2022 Dec 27.
Article in English | MEDLINE | ID: mdl-36614587

ABSTRACT

The impact of the initial phase composition of alloys was evaluated, in particular, the content of Cu, Mn, and Mg in aluminum alloys D16ChATW, 2024-T351 and aluminum alloy T, which in its physical and mechanical characteristics is close to alloy 6013. The impact was evaluated on the effects manifested by yield sites that occur on aluminum alloys that were subject to the dynamic non-equilibrium processes (DNPs) at the expense of impact-oscillatory loading of different intensities under conditions of static tensioning, The one-time DNP, to which the investigated aluminum alloys were subjected at the pre-set levels of elastic strain followed by static tensioning, was found to cause yield sites formation. This is due to self-organization of the alloy structure, which contributes to alloy plasticization. The initial phase alloys composition impact on the yield sites, which occurs when impulse energy of a different intensity is applied to the alloys, was analyzed. The specimens from the aluminum alloys undergoing DNPs of the same level were compared. This made it possible to conclude that alloys D16ChATW and 2024-T351, which have a higher content of Cu, Mn, and Mg, have longer yield sites upon subsequent static tensioning. On the basis of the experimental results, in particular, physical studies, the authors derived a physical and mathematical model of the yield sites that appear after DNPs.

4.
Materials (Basel) ; 14(12)2021 Jun 16.
Article in English | MEDLINE | ID: mdl-34208438

ABSTRACT

This paper deals with the determination of the basic corrosion characteristics of metallic materials used as components in car construction to achieve a lighter vehicle with higher rigidity, a more complex "hybrid" of diverse materials is needed for the car body structure. Due to the different types of material used in the manufacture of components and their interactions, the issue of assessing the impact of bimetallic corrosion is currently relevant. Based on the potential difference at the end of the corrosion test, it was possible to determine the "anode index", which determines the risk of degradation of materials due to bimetallic corrosion. In our case, a hot-galvanized steel sheet/Al alloy EN AW-6060 couple in deicing salt and hot-galvanized steel sheet/steel S355J0 couple in simulated acid rain solution (SARS) has proven to be "safest" and usable even for more aggressive environments. Hot-galvanized steel sheet/Al alloy EN AW-6060 in SARS solution is suitable for slightly aggressive environments. Stainless steel AISI 304/silumin A356 in deicing salt, stainless steel AISI 304/Al alloy EN AW-6060 in deicing salt, and stainless steel AISI 306/Al alloy EN AW-6060 in simulated exhaust gas environment (SEG solution) are not suitable for non-aggressive environments.

5.
Materials (Basel) ; 14(8)2021 Apr 16.
Article in English | MEDLINE | ID: mdl-33923701

ABSTRACT

The process of laser welding of sheets of HSLA (high-strength low-alloy steel), DP600 (dual-phase steel) and TRIP steels was investigated. A weld was successfully made in a double-sided hot-dip galvanized sheet with a thickness of 0.78-0.81 mm using a laser power of 2 kW per pass without any pretreatment of the weld zone. Microstructure studies revealed the presence of martensitic and ferritic phases in the weld zone, which could be associated with a high rate of its cooling. This made it possible to obtain good strength of the weld, while maintaining sufficient ductility. A relationship between the microstructural features and mechanical properties of welds made in the investigated steels has been established. The highest hardness was found in the alloying region of steels due to the formation of martensite. The hardness test results showed a very narrow soft zone in the heat affected zone (HAZ) adjacent to the weld interface, which does not affect the tensile strength of the weld. The ultimate tensile strength of welds for HSLA steel was 340-450 MPa, for DP600 steel: 580-670 MPa, for TRIP steel: ~700 MPa, respectively, exceeding the strength of base steels.

6.
Materials (Basel) ; 13(21)2020 Nov 05.
Article in English | MEDLINE | ID: mdl-33167467

ABSTRACT

A method of computer modeling of a surface relief is proposed, and its efficiency and high accuracy are proven. The method is based on the mathematical model of surface microrelief, using titanium alloy Ti6Al4V subjected to processing with femtosecond pulses as an example. When modeling the examples of microrelief, changes in the shape of segments-cycles of the studied surface processes, which correspond to separate morphological formations, were taken into account. The proposed algorithms were realized in the form of a computer simulation program, which provides for a more accurate description of the geometry of the microrelief segments. It was proven that the new method significantly increases the efficiency of the analysis procedure and processing of signals that characterize self-organized relief formations.

7.
Materials (Basel) ; 13(20)2020 Oct 13.
Article in English | MEDLINE | ID: mdl-33066074

ABSTRACT

The structure and mechanical properties of the 09Mn2Si high-strength low-alloyed steel after the five-stage helical rolling (HR) were studied. It was revealed that the fine-grained structure had been formed in the surface layer ≈ 1 mm deep as a result of severe plastic strains. In the lower layers, the "lamellar" structure had been formed, which consisted of thin elongated ferrite grains oriented in the HR direction. It was shown that the five-stage HR resulted in the increase in the steel fatigue life by more than 3.5 times under cyclic tension. The highest values of the number of cycles before failure were obtained for the samples cut from the bar core. It was demonstrated that the degree of the elastic energy dissipation in the steel samples under loading directly depended on the area of the grain boundaries as well as on the grain shapes. The fine-grained structure possessed the maximum value of the average torsional energy among all the studied samples, which caused the local material structure transformation and the decrease in the elastic energy level. This improved the crack resistance under the cyclic mechanical loading. The effect of the accumulation of the rotational strain modes at the grain boundaries was discovered, which caused the local structure transformation at the boundary zones. In the fine-grained structure, the formation of grain conglomerates was observed, which increased the values of the specific modulus of the moment of force. This could be mutually compensated due to the small sizes of grains. At the same time, the coarse-grained structures were characterized by the presence of the small number of grains with a high level of the moments of forces at their boundaries. They could result in trans-crystalline cracking.

8.
Materials (Basel) ; 12(17)2019 Aug 25.
Article in English | MEDLINE | ID: mdl-31450651

ABSTRACT

It was shown previously that cyclic loading can be used to extend the fatigue life of sheet plastic materials subjected to the preliminary impact-oscillatory loading. This type of loading causes dynamic non-equilibrium processes (DNP) in materials, which lead to the formation of dissipative structures in materials and on their surface. The density of these dissipative structures is less than that of the base metal. In this paper, the results of investigations into the relief and hardness of surface layers modified by impact-oscillatory loading are analyzed on the example of five structural materials. The signs of a regular, orderly system of microextrusions formed on flat surfaces of all materials due to DNP are considered along with the alignment of roughness parameters Rz and Ra of relief profiles. The effect of impact-oscillatory loading is one of the main causes that lead to the extension of the fatigue life of materials.

9.
Materials (Basel) ; 12(13)2019 Jun 26.
Article in English | MEDLINE | ID: mdl-31247954

ABSTRACT

The authors developed a method for the automated detection and calculation of quantitative parameters of dimples of ductile fracture on the digital images of fracture surfaces obtained at different scales. The processing algorithm of fractographic images was proposed, which allowed high quality recognition of the shape and size of dimples to be achieved, taking into account the morphological features of their digital images. The developed method for identifying dimples of various physical and morphological characteristics was tested on the VT23M alloy. The test results showed that the method meets the quality requirements for the automated diagnostics of fracture mechanisms of titanium alloys.

10.
Materials (Basel) ; 12(3)2019 Feb 05.
Article in English | MEDLINE | ID: mdl-30764509

ABSTRACT

Regularities of steel structure degradation of the "Novopskov-Aksay-Mozdok" gas main pipelines (Nevinnomysskaya CS) as well as the "Gorky-Center" pipelines (Gavrilovskaya CS) were studied. The revealed peculiarities of their degradation after long-term operation are suggested to be treated as a particular case of the damage accumulation classification (scheme) proposed by prof. H.M. Nykyforchyn. It is shown that the fracture surface consists of sections of ductile separation and localized zones of micro-spalling. The presence of the latter testifies to the hydrogen-induced embrittlement effect. However, the steels under investigation possess sufficiently high levels of the mechanical properties required for their further safe exploitation, both in terms of durability and cracking resistance.

11.
Materials (Basel) ; 11(12)2018 Dec 05.
Article in English | MEDLINE | ID: mdl-30563063

ABSTRACT

The research of fractographic images of metals is an important method that allows obtaining valuable information about the physical and mechanical properties of a metallic specimen, determining the causes of its fracture, and developing models for optimizing its properties. One of the main lines of research in this case is studying the characteristics of the dimples of viscous detachment, which are formed on the metal surface in the process of its fracture. This paper proposes a method for detecting dimples of viscous detachment on a fractographic image, which is based on using a convolutional neural network. Compared to classical image processing algorithms, the use of the neural network significantly reduces the number of parameters to be adjusted manually. In addition, when being trained, the neural network can reveal a lot more characteristic features that affect the quality of recognition in a positive way. This makes the method more versatile and accurate. We investigated 17 models of convolutional neural networks with different structures and selected the optimal variant in terms of accuracy and speed. The proposed neural network classifies image pixels into two categories: "dimple" and "edge". A transition from a probabilistic result at the output of the neural network to an unambiguously clear classification is proposed. The results obtained using the neural network were compared to the results obtained using a previously developed algorithm based on a set of filters. It has been found that the results are very similar (more than 90% similarity), but the neural network reveals the necessary features more accurately than the previous method.

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