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1.
Materials (Basel) ; 16(23)2023 Nov 28.
Article in English | MEDLINE | ID: mdl-38068134

ABSTRACT

In guided-wave-based damage-imaging algorithms, damage reconstruction typically involves comparing the signals with and without a defect. However, in many cases, defect-free data may not be available. Therefore, in this study, baseline and baseline-free approaches were used for damage imaging, exploiting not only the amplitude of the signal as the feature but also five additional features, namely, the amplitude of the sparse signal after deconvolution, the amplitude of the coefficients at the excitation frequency from the re-assigned short-time Fourier transform, the time of flight determined from cross-correlation, kurtosis in the time domain, and kurtosis in the frequency domain. For this study, three different plates with different types of defects were considered: a metallic plate with a notch-type artificial defect, a pultruded type of composite plate with an impact defect, and a laminate composite plate with plexiglass serving as an added mass damper artificial defect. The Reconstruction Algorithm for Probabilistic Inspection of Damage (the RAPID algorithm) was used to characterize the defects on the three plates, and the defect parameters were then quantified by creating an ellipse after thresholding.

2.
Sensors (Basel) ; 23(15)2023 Jul 26.
Article in English | MEDLINE | ID: mdl-37571462

ABSTRACT

In this study, a new method for determining the elastic constants of isotropic plates using Lamb wave fundamental modes is presented. This method solves the inverse problem, where the elastic constants (Young's modulus and Poisson's ratio) of the plate were estimated by measuring the phase velocities of the Lamb wave using the Rayleigh-Lamb equations to find the solution and determining the phase velocities of the A0 and S0 modes using a new method. The suitability of the proposed method for determining the elastic constants was evaluated using simulated and experimental signals propagating on an aluminum plate. The theoretical modeling on the aluminum 7075-T6 plate shows that the proposed method allows the determination of the Poisson ratio with a relative error not exceeding 2% and Young's modulus with a relative error not exceeding 0.5%. The experimental measurements of an aluminum plate of known thickness (2 mm) and density (2685 kg/m3) confirmed the suitability of the proposed method for the measurements of elastic constants. In the proposed method, the processing of ultrasonic signals can be performed in real-time, and the values of the elastic constants can be obtained immediately after scanning the required distance.

3.
Sensors (Basel) ; 23(14)2023 Jul 18.
Article in English | MEDLINE | ID: mdl-37514800

ABSTRACT

Pipeline structures are susceptible to corrosion, leading to significant safety, environmental, and economic implications. Existing long range guided wave inspection systems often fail to detect footprints of the concentrated defects, which can lead to leakage. One way to tackle this issue is the utilization of circumferential guided waves that inspect the pipe's cross section. However, achieving the necessary detection resolution typically necessitates the use of high-order modes hindering the inspection data interpretation. This study presents the implementation of an ultrasonic technique capable of detecting and classifying wall thinning and concentrated defects using high-order guided wave modes. The technique is based on a proposed phase velocity mapping approach, which generates a set of isolated wave modes within a specified phase velocity range. By referencing phase velocity maps obtained from defect-free stages of the pipe, it becomes possible to observe changes resulting from the presence of defects and assign those changes to the specific type of damage using artificial neural networks (ANN). The paper outlines the fundamental principles of the proposed phase velocity mapping technique and the ANN models employed for classification tasks that use synthetic data as an input. The presented results are meticulously verified using samples with artificial defects and appropriate numerical models. Through numerical modeling, experimental verification, and analysis using ANN, the proposed method demonstrates promising outcomes in defect detection and classification, providing a more comprehensive assessment of wall thinning and concentrated defects. The model achieved an average prediction accuracy of 92% for localized defects, 99% for defect-free cases, and 98% for uniform defects.

4.
Sensors (Basel) ; 23(4)2023 Feb 07.
Article in English | MEDLINE | ID: mdl-36850463

ABSTRACT

Usually for non-destructive testing at high temperatures, ultrasonic transducers made of PZT and silver electrodes are used, but this could lead to damage to or malfunction of the ultrasonic transducer due to poor adhesion between PZT and silver. Soldering is one of the most common types of bonding used for individual parts of ultrasonic transducers (protector, backing, matching layer, etc.), but silver should be protected using additional metal layers (copper) due to its solubility in solder. A mathematical modelling could help to predict if an ultrasonic transducer was manufactured well and if it could operate up to 225 °C. The observed von Mises stresses were very high and concentrated in metal layers (silver and copper), which could lead to disbonding under long-term cyclic temperature loads. This paper presents a multilayer ultrasonic transducer (PZT, silver electrodes, copper layers, backing), which was heated evenly from room temperature to 225 °C and then cooled down. In the B-scan, it was observed that the amplitude of the reflected signal from the bottom of the sample decreased with an increase in temperature. However, after six heating-cooling cycles, the results repeated themselves and no signs of fatigue were noticed. This ultrasonic transducer was well manufactured and could be used for non-destructive testing when the environment temperature changes in cycles up to 225 °C.

5.
Materials (Basel) ; 15(20)2022 Oct 17.
Article in English | MEDLINE | ID: mdl-36295311

ABSTRACT

Contemporary technologies are employing composite plate materials developed by using various innovative materials (nanostructures, mica structures, etc.). Application of higher-order modes could allow better detection and characterization of defects characteristic of planar plastic and composite structures, mainly due to shorter wavelength. However, excitation of higher-order modes meets many problems, especially in the case of the air-coupled technique, and is not sufficiently investigated. This is relevant in the cases of paper, high-density polyethylene (HDPE), membranes, GFRP, GLARE, CFRP and other composite structures. The objective of the paper was investigation of the excitation and reception of higher-order guided Lamb wave modes in plastic and composite plates. Therefore, it is appropriate to develop new non-contact ultrasonic measurement methods based on the excitation and reception of guided waves for the study of such objects. The obtained results clearly demonstrate the possibility to excite and receive efficiently different higher-order guided Lamb wave modes with very different phase velocities. The presented comparison of the experimental results with the simulation results showed a good agreement. The combination of air-coupled excitation and non-contact reception enables a non-destructive evaluation and characterization of moving plastic objects and composite structures.

6.
Materials (Basel) ; 15(13)2022 Jun 28.
Article in English | MEDLINE | ID: mdl-35806675

ABSTRACT

The article is devoted to the investigation of ultrasonic inspection techniques suitable for detecting hydrogen-induced cracking (HIC) and a high-temperature hydrogen attack (HTHA), which are of great importance in petrochemical and refinery industries. Four techniques were investigated: total focusing method (TFM), advanced velocity ratio (AVR) measurement, advanced ultrasonic backscatter technique (AUBT) and time of flight diffraction method using ultra low angle ultrasonic transducers (TULA). The experimental investigation has been carried out on two carbon steel samples cut off from a heat exchanger of an oil refinery and potentially affected by HIC. It was shown that the AVR technique did not reveal any damage and was not effective in the case of the investigated samples due to a thin damage zone with respect to the total thickness of the samples. The AUBT method enabled us to indicate and classify the presence of the hydrogen-induced damage; however, it is complicated to use in practise due to the need perform measurements exactly at the same position using two transducers of different frequencies. The method is more suitable for the verification of damage at a particular position, rather than for scanning. Both other methods-TFM and TULA-enabled us to identify the presence of HIC in large areas of samples. The obtained results have been verified using a metallographic analysis of the section cut from the side of the sample. The results of metallographic examinations have been compared with indications observed using above mentioned techniques and a good correspondence was obtained. It was demonstrated, that the TFM method can detect cracks with dimensions close to 200 µm, while larger cracks of 2 mm were observed very evidently using a 7.5 MHz phased array. Overall, the results suggested that the TULA method is the most suitable method for the primary detection of hydrogen-induced cracking, while the TFM is recommended for the precise assessment of the extent of the detected cracking.

7.
Materials (Basel) ; 15(10)2022 May 11.
Article in English | MEDLINE | ID: mdl-35629494

ABSTRACT

Multilayered carbon fiber-reinforced polymers (CFRP) are increasingly used in aircraft components because of their superior mechanical properties. However, composite materials are vulnerable to impact loads, resulting in delamination-type damage which, if unnoticed, could lead to catastrophic structural failure. The objective of this research was to investigate possibilities to improve damage detection and the localization using signal processing methods. Numerical modeling using the semi-analytical finite element (SAFE) method was performed to obtain guided wave dispersion curves and to perform modal analysis. From the modal analysis, A0 mode for inspection of the composite with delamination type defects was selected. From the numerical simulation, A0 mode interaction with delamination along the longitudinal direction was analyzed and the location of the defect was estimated by measuring the time of flight (ToF) of the signal using Hilbert transform (HT) and continuous wavelet transform (CWT). The CWT has shown better results in estimating the delamination location compared with HT. The depth of delamination was characterized in the frequency domain by comparing the amplitude of the A0 mode. Inverse fast Fourier transform (IFFT) is recommended to reconstruct the reflected and transmitted modes for better damage detection and to reduce the complexity of signal interpretation.

8.
Materials (Basel) ; 15(4)2022 Feb 21.
Article in English | MEDLINE | ID: mdl-35208153

ABSTRACT

Fibre-reinforced composite laminates are frequently used in various engineering structures, due to their increased weight-to-stiffness ratio, which allows to fulfil certain regulations of CO2 emissions. Limited inter-laminar strength makes composites prone to formation of various defects, which leads to progressive degradation of residual strength and fatigue life of the structure. Using ultrasonic guided waves is a common technique for assessing the structural integrity of composite laminates. Phase velocity is one of the fundamental characteristics of guided waves and can be used for defect detection, material property estimation, and evaluation of dispersion. In this paper, a phase velocity reconstruction approach, based on the phase-shift method, was proposed, which uses frequency sweep excitation to estimate velocity at specific frequency harmonics. In contrast to the conventional phase spectrum technique, the proposed approach is applicable to the narrowband piezoelectric transducers and suitable for the reconstruction of dispersion curves for direct, converted, and multiple co-existing modes with high accuracy. The proposed technique was validated with finite element simulations and experiments, both on isotropic and anisotropic structures, analysing the direct, converted, and overlapped modes. The results demonstrated that, using the proposed technique, the phase velocity dispersion can be reconstructed at -20 dB level bandwidth of the transducer, with a relative error of ±4%, compared to the theoretical velocity predictions.

9.
Sensors (Basel) ; 21(9)2021 Apr 27.
Article in English | MEDLINE | ID: mdl-33925402

ABSTRACT

Adhesively bonded dissimilar materials have attracted high interest in the aerospace and automotive industries due to their ability to provide superior structural characteristics and reduce the weight for energy savings. This work focuses on the improvement of disbond-type defect detectability using the immersion pulse-echo ultrasonic technique and an advanced post-processing algorithm. Despite the extensive work done for investigation, it is still challenging to locate such defects in dissimilar material joints due to the large differences in the properties of metals and composites as well as the multi-layered structure of the component. The objective of this work is to improve the detectability of defects in adhesively bonded aluminum and carbon fiber-reinforced plastic (CFRP) by the development of an advanced post-processing algorithm. It was determined that an analysis of multiple reflections has a high potential to improve detectability according to results received by inspection simulations and the evaluation of boundary characteristics. The impact of a highly influential parameter such as the sample curvature can be eliminated by the alignment of arrival time of signals reflected from the sample. The processing algorithm for the improvement of disbond detectability was developed based on time alignment followed by selection of the time intervals with a significant amplitude change of the signals reflected from defective and defect-free areas and shows significant improvement of disbond detectability.

10.
Sensors (Basel) ; 21(1)2020 Dec 22.
Article in English | MEDLINE | ID: mdl-33375103

ABSTRACT

According to the statistics, 40% of unplanned disruptions in electricity distribution grids are caused by failure of equipment in high voltage (HV) transformer substations. These damages in most cases are caused by partial discharge (PD) phenomenon which progressively leads to false operation of equipment. The detection and localization of PD at early stage can significantly reduce repair and maintenance expenses of HV assets. In this paper, a non-invasive PD detection and localization solution has been proposed, which uses three ultrasonic sensors arranged in an L shape to detect, identify and localize PD source. The solution uses a fusion of ultrasonic signal processing, machine learning (ML) and deep learning (DL) methods to classify and process PD signals. The research revealed that the support vector machines classifier performed best among two other classifiers in terms of sensitivity and specificity while classifying discharge and surrounding noise signals. The proposed ultrasonic signal processing methods based on binaural principles allowed us to achieve an experimental lateral source positioning error of 0.1 m by using 0.2 m spacing between L shaped sensors. Finally, an approach based on DL was suggested, which allowed us to detect a single PD source in optical images and, in such a way, to provide visual representation of PD location.

11.
Sensors (Basel) ; 20(8)2020 Apr 17.
Article in English | MEDLINE | ID: mdl-32316474

ABSTRACT

Analytical modelling is an efficient approach to estimate the directivity of a transducer generating guided waves in the research field of ultrasonic non-destructive testing of the large and complex structures due to its short processing time as compared to the numerical modelling and experimental techniques. The wave patterns or the amplitude variations along the region of ultrasonic transducer itself depend on its behavior, excitation frequency, and the type of propagating wave mode. Depending on the wave-pattern of a propagating wave mode, the appropriate value of the amplitude correction factor must be multiplied to the amplitudes of the excitation signal for the accurate evaluation of directivity pattern of the ultrasonic transducers generating guided waves in analytical modelling. The objective of this work is to analyse the wave patterns under the region of macro-fiber composite (MFC) transducer to improve the accuracy of a previously developed analytical model for the prediction of directivity patterns. Firstly, the amplitude correction factor based on the wave patterns under the region of P1-type MFC (MFC-2814) transducer at two different frequencies (80 kHz, 3 periods and 220 kHz, 3 period) glued on 2 mm Al alloy plate has been estimated analytically in the case of an asymmetric (A0) guided Lamb wave. The validation of analytically estimated amplitude correction factor is performed by a proposed experimental method that allows analyzing the behaviour of MFC transducer under its region by gluing MFC on bottom surface and scanning the receiver on the top surface of the sample. Later on, the estimated amplitude correction factor is included in the previously developed 2D analytical model for the improvement in the directivity patterns of the A0 mode. The modified analytical model shows a significant improvement in the directivity pattern of the A0 wave mode in comparison to the results obtained by the previous model without considering the proper wave patterns. The results reveal that errors between the directivity estimated by the present modified 2D analytical model and experimental investigation are reduced by more than 58% in comparison to the previously developed analytical model.

12.
Materials (Basel) ; 12(10)2019 May 21.
Article in English | MEDLINE | ID: mdl-31117182

ABSTRACT

The ultrasonic testing technique using Lamb waves is widely used for the non-destructive testing and evaluation of various structures. For air-coupled excitation and the reception of A0 mode Lamb waves, leaky guided waves are usually exploited. However, at low frequencies (<100 kHz), the velocity of this mode in plastic and composite materials can become slower than the ultrasound velocity in air, and its propagation in films is accompanied only by an evanescent wave in air. To date, the information about the attenuation of the slow A0 mode is very contradictory. Therefore, the objective of this investigation was the measurement of the attenuation of the slow A0 mode in thin plastic films. The measurement of the attenuation of normal displacements of the film caused by a propagating slow A0 mode is discussed. The normal displacements of the film at different distances from the source were measured by a laser interferometer. In order to reduce diffraction errors, the measurement method based on the excitation of cylindrical but not plane waves was proposed. The slow A0 mode was excited in the polyvinylchloride film by a dry contact type ultrasonic transducer made of high-efficiency PMN-32%PT strip-like piezoelectric crystal. It was found that that the attenuation of the slow A0 mode in PVC film at the frequency of 44 kHz is 2 dB/cm. The obtained results can be useful for the development of quality control methods for plastic films.

13.
Ultrasonics ; 95: 13-21, 2019 May.
Article in English | MEDLINE | ID: mdl-30852341

ABSTRACT

Ultrasonic inspection is widely used for non-destructive evaluation of composite adhesive joints. However, there are serious challenges in applying ultrasonic testing on metal to composite hybrid joints, because they are multi-layered, made out of dissimilar materials and relatively thin. The ultrasonic signals reflected by different layers are overlapped, scattered and attenuated. The aim of this research was to develop an ultrasonic inspection technique suitable for defect detection in hybrid metal to composite joints where the metal part has pin arrays, which entangle with the composite part. The immersion pulse echo technique was used to collect data. In order to overcome the problems related to the rough surface and non-parallel layers a novel signal post-processing algorithm for reconstruction of the joint area was developed and validated experimentally. It is shown that using the proposed technique the positions of different defects can be determined.

14.
Sensors (Basel) ; 18(9)2018 Sep 19.
Article in English | MEDLINE | ID: mdl-30235795

ABSTRACT

Ultrasonic non-destructive testing techniques (NDT) based on the application of guided waves are already used for inspection of plate-type structures made of various materials, including composite materials. Air-coupled ultrasonic techniques are used to test such structures by means of guided waves. The objective of this research was development and investigation of air-coupled excitation of a slow A0 Lamb wave mode in thin plastic films by a PMN-32%PT ultrasonic array. It is known that when the velocity of the A0 mode in the film is less than the ultrasound velocity in air no leaky wave is observed in a surrounding air. It opens new possibilities for NDT of composite structures. The influence of the airborne wave may be eliminated by 3D filtering in a wavenumbers-frequency domain. A special filter and corresponding signals processing technique were developed in order to obtain directivity patterns and velocity maps of the waves propagating in all directions. The measured ultrasound velocity values prove that, with the proposed method, it is possible to excite a slow A0 Lamb wave mode and to separate it from other parasitic waves propagating in air. Measurements of the parameters of the slow A0 mode, such as the propagation velocity in the plastic film, may be applied for the material characterization.

15.
J Med Ultrason (2001) ; 45(4): 545-553, 2018 Oct.
Article in English | MEDLINE | ID: mdl-29536280

ABSTRACT

PURPOSE: For long time, blood clot retraction was measured only by thromboelastographic or platelet contractile force measurement techniques. The purpose of the present study was development of a novel ultrasonic method based on simultaneous monitoring of variations in the ultrasound velocity and the frequency spectrum of the signal propagating in clotting blood and its application for automatic evaluation of blood clotting parameters. METHODS: Simultaneous measurement of ultrasound velocity and variations in the frequency spectrum of wideband ultrasonic signals in clotting blood samples was performed. All measurements were performed in pulse-echo mode. Standard clinical data were obtained using routine clinical laboratory methods. RESULTS: The amplitudes of ultrasonic signals during native blood coagulation varied up to ten times for different frequencies. The measurement results of the start and duration of blood clot retraction differed between patient samples: different components of the blood coagulation system had significant impact on the blood clot retraction process. CONCLUSIONS: Our results showed that during blood clotting, the ultrasound velocity and variations in frequency spectrum should be used simultaneously to determine the beginning and duration of blood clot retraction. Our results also showed that blood clot retraction is controlled by the activity of factor XIII.


Subject(s)
Blood Coagulation Tests/methods , Blood Coagulation , Ultrasonography/methods , Adult , Blood Coagulation/genetics , Blood Coagulation/physiology , Blood Coagulation Tests/instrumentation , Equipment Design , Female , Humans , Male , Ultrasonic Waves , Ultrasonography/instrumentation
16.
Sensors (Basel) ; 18(4)2018 Mar 26.
Article in English | MEDLINE | ID: mdl-29587472

ABSTRACT

In this paper, a novel 2D analytical model based on the Huygens's principle of wave propagation is proposed in order to predict the directivity patterns of contact type ultrasonic transducers in the generation of guided waves (GWs). The developed model is able to estimate the directivity patterns at any distance, at any excitation frequency and for any configuration and shape of the transducers with prior information of phase dispersive characteristics of the guided wave modes and the behavior of transducer. This, in turn, facilitates to choose the appropriate transducer or arrays of transducers, suitable guided wave modes and excitation frequency for the nondestructive testing (NDT) and structural health monitoring (SHM) applications. The model is demonstrated for P1-type macro-fiber composite (MFC) transducer glued on a 2 mm thick aluminum (Al) alloy plate. The directivity patterns of MFC transducer in the generation of fundamental guided Lamb modes (the S0 and A0) and shear horizontal mode (the SH0) are successfully obtained at 80 kHz, 5-period excitation signal. The results are verified using 3D finite element (FE) modelling and experimental investigation. The results obtained using the proposed model shows the good agreement with those obtained using numerical simulations and experimental analysis. The calculation time using the analytical model was significantly shorter as compared to the time spent in experimental analysis and FE numerical modelling.

17.
Sensors (Basel) ; 17(8)2017 Aug 08.
Article in English | MEDLINE | ID: mdl-28786924

ABSTRACT

Ultrasonic guided wave (UGW)-based condition monitoring has shown great promise in detecting, localizing, and characterizing damage in complex systems. However, the application of guided waves for damage detection is challenging due to the existence of multiple modes and dispersion. This results in distorted wave packets with limited resolution and the interference of multiple reflected modes. To develop reliable inspection systems, either the transducers have to be optimized to generate a desired single mode of guided waves with known dispersive properties, or the frequency responses of all modes present in the structure must be known to predict wave interaction. Currently, there is a lack of methods to predict the response spectrum of guided wave modes, especially in cases when multiple modes are being excited simultaneously. Such methods are of vital importance for further understanding wave propagation within the structures as well as wave-damage interaction. In this study, a novel method to predict the response spectrum of guided wave modes was proposed based on Fourier analysis of the particle velocity distribution on the excitation area. The method proposed in this study estimates an excitability function based on the spatial dimensions of the transducer, type of vibration, and dispersive properties of the medium. As a result, the response amplitude as a function of frequency for each guided wave mode present in the structure can be separately obtained. The method was validated with numerical simulations on the aluminum and glass fiber composite samples. The key findings showed that it can be applied to estimate the response spectrum of a guided wave mode on any type of material (either isotropic structures, or multi layered anisotropic composites) and under any type of excitation if the phase velocity dispersion curve and the particle velocity distribution of the wave source was known initially. Thus, the proposed method may be a beneficial tool to explain and predict the response spectrum of guided waves throughout the development of any structural health monitoring system.

18.
Microscopy (Oxf) ; 65(5): 429-437, 2016 10.
Article in English | MEDLINE | ID: mdl-27489311

ABSTRACT

Scanning acoustic microscopy (SAM) is used as a routine non-destructive test tool for different diagnostic examinations: detection of defects such as microcracks, delamination, disbonding, inclusions, subsurface features in materials such as pores and cracks. SAM can be operated in a wide frequency range from Megahertz to Gigahertz. SAM measurement spatial resolution is diffraction limited by the wavelength of the acoustic wave in particular medium and also depends on individual transducers geometry. Actual SAM spatial resolution can be determined by measuring calibrated lithographically formed microstructures in high acoustic impedance materials. Numerical acoustic signal simulation method, based on the diffraction approach, was employed for the selection of the calibration block pattern geometry and linear dimensions of the elements. Universal calibration block for SAM operating in a 20-230 MHz frequency range was micromachined in high acoustic impedance ceramic substrates. Differently spaced (from 18 to 185 µm) lines of the same width and different widths (from 17 to 113 µm) but similar spacing lines were imposed in alumina ceramics employing one step lithography process, i.e. femtosecond laser ablation. Proposed SAM calibration pattern linear dimensions were characterized employing optical and scanning electron microscopy. Finally the samples were measured with SAM employing different frequency transducers and results were compared with the numerical simulations. It was obtained that resolution of SAM operating with 230 MHz transducer is not worse than 40 µm.

19.
Materials (Basel) ; 9(6)2016 Jun 06.
Article in English | MEDLINE | ID: mdl-28773574

ABSTRACT

Multi-wire ropes are widely used as load-carrying constructional elements in bridges, cranes, elevators, etc. Structural integrity of such ropes can be inspected by using non-destructive ultrasonic techniques. The objective of this work was to investigate propagation of ultrasonic guided waves (UGW) along composite multi-wire ropes in the cases of various types of acoustic contacts between neighboring wires and the plastic core. The modes of UGW propagating along the multi-wire ropes were identified using modelling, the dispersion curves were calculated using analytical and semi-analytical finite element (SAFE) techniques. In order to investigate the effects of UGW propagation, the two types of the acoustic contact between neighboring wires were simulated using the 3D finite element method (FE) as well. The key question of investigation was estimation of the actual boundary conditions between neighboring wires (solid or slip) and the real depth of penetration of UGW into the overall cross-section of the rope. Therefore, in order to verify the results of FE modelling, the guided wave penetration into strands of multi-wire rope was investigated experimentally. The performed modelling and experimental investigation enabled us to select optimal parameters of UGW to be used for non-destructive testing.

20.
Sensors (Basel) ; 15(8): 19393-415, 2015 Aug 07.
Article in English | MEDLINE | ID: mdl-26262619

ABSTRACT

An ultrasonic technique, invariant to temperature changes, for a density measurement of different liquids under in situ extreme conditions is presented. The influence of geometry and material parameters of the measurement system (transducer, waveguide, matching layer) on measurement accuracy and reliability is analyzed theoretically along with experimental results. The proposed method is based on measurement of the amplitude of the ultrasonic wave, reflected from the interface of the solid/liquid medium under investigation. In order to enhance sensitivity, the use of a quarter wavelength acoustic matching layer is proposed. Therefore, the sensitivity of the measurement system increases significantly. Density measurements quite often must be performed in extreme conditions at high temperature (up to 220 °C) and high pressure. In this case, metal waveguides between piezoelectric transducer and the measured liquid are used in order to protect the conventional transducer from the influence of high temperature and to avoid depolarization. The presented ultrasonic density measurement technique is suitable for density measurement in different materials, including liquids and polymer melts in extreme conditions. A new calibration algorithm was proposed. The metrological evaluation of the measurement method was performed. The expanded measurement uncertainty Uρ = 7.4 × 10(-3) g/cm(3) (1%).

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