Comprehensive Research of FSW Joints of AZ91 Magnesium Alloy.

For the friction stir welding (FSW) of AZ91 magnesium alloy, low tool rotational speeds and increased tool linear speeds (ratio 3.2) along with a larger diameter shoulder and pin are utilized. The research focused on the influence of welding forces and the characterization of the welds by light microscopy, scanning electron microscopy with an electron backscatter diffraction system (SEM-EBSD), hardness distribution across the joint cross-section, joint tensile strength, and SEM examination of fractured specimens after tensile tests. The micromechanical static tensile tests performed are unique and reveal the material strength distribution within the joint. A numerical model of the temperature distribution and material flow during joining is also presented. The work demonstrates that a good-quality joint can be obtained. A fine microstructure is formed at the weld face, containing larger precipitates of the intermetallic phase, while the weld nugget comprises larger grains. The numerical simulation correlates well with experimental measurements. On the advancing side, the hardness (approx. 60 HV0.1) and strength (approx. 150 MPa) of the weld are lower, which is also related to the lower plasticity of this region of the joint. The strength (approx. 300 MPa) in some micro-areas is significantly higher than that of the overall joint (204 MPa). This is primarily attributable to the macroscopic sample also containing material in the as-cast state, i.e., unwrought. The microprobe therefore includes less potential crack nucleation mechanisms, such as microsegregations and microshrinkage.

The Object Segmentation from the Microstructure of a FSW Dissimilar Weld.

Friction stir welding (FSW) is an environmentally friendly, solid-state welding technique. In this research work, we analyze the microstructure of a new type of FSW weld applying a two- stage framework based on image processing algorithms containing a segmentation step and microstructure analysis of objects occurring in different layers. A dual-speed tool as used to prepare the tested weld. In this paper, we present the segmentation method for recognizing areas containing particles forming bands in the microstructure of a dissimilar weld of aluminum alloys made by FSW technology. A digital analysis was performed on the images obtained using an Olympus GX51 light microscope. The image analysis process consisted of basic segmentation methods in conjunction with domain knowledge and object detection located in different layers of a weld using morphological operations and point transformations. These methods proved to be effective in the analysis of the microstructure images corrupted by noise. The segmentation parts as well as single objects were separated enough to analyze the distribution on different layers of the specimen and the variability of shape and size of the underlying microstructures, which was not possible without computer vision support.

Modification of Mechanical Properties of Aluminum Alloy Rods via Friction-Extrusion Method.

The elaboration of a modified friction-extrusion method aimed at obtaining 2017A aluminum rods of gradient microstructure is described. This was achieved by cutting spiral grooves on the face of the stamp used for alloy extrusion. The experiments were carried out at a constant material feed (~10 mm/min) and a range of tool rotation speeds (80 to 315 rpm). The microstructure observations were carried out using light microscopy (LM) and both scanning and transmission electron microscopy (SEM and TEM). The mechanical properties were assessed through hardness measurements and static tensile tests. The performed investigations show that material simultaneous radial and longitudinal flow, enforced by friction of the rotating tool head and extrusion, results in the formation of two zones of very different microstructures. At the perpendicular section, the outer zone stands out from the core due to circumferential elongation of strings of particles, while in the inner zone the particles are arranged in a more uniform way. Simultaneously, the grain size of the outer zone is refined by two to four times as compared with the inner one. The transfer from the outer zone to the core area is of gradient type. The hardness of the outer zone was found to be ~10% to ~20% higher than that of the core.

Temperature Changes and SEM Effects of Three Different Implants-Abutment Connection during Debridement with Er:YAG Laser: An Ex Vivo Study.

The study aimed to evaluate a temperature increase in, and damage to, titanium implants during flapless laser debridement. The study analyzed 15 implants with various implant-abutment connections: a two-piece implant (n = 4) with a screw abutment (IA-Implant-Abutment) and a one-piece implant with a ball type fixture (BTF, n = 4) or fix type fixture (FTF, n = 4). The implants were placed in porcine mandibles 2 mm over a bone crest to imitate a peri-implantitis. The implants were debrided in contact mode for 60 s with a Er:YAG laser at fluence of 9.95 J/cm2 (G1 group: 50 mJ/30 Hz); 19.89 J/cm2 (G2 group: 100 mJ/30 Hz); 39.79 J/cm2 (G3 group: 200 mJ/30 Hz), or a scaler with a ceramic tip (G4 control group: 4 W/20 Hz). The temperature was measured with thermocouples at implant and abutment levels. The damage in the titanium surface (n = 3, non-irradiated implants from each type) was assessed using SEM (Scanning Electron Microscopy). The temperature increase at the implant level for the laser was higher at IA in contrast with FTF and BTF. (p < 0.05) The temperature change at the abutment level was lower for the scaler in contrast to Er:YAG laser at FTF. (p < 0.0002) Er:YAG laser didn't increase the temperature by 10 °C at 100 mJ/30 Hz and 50 mJ/30 Hz. Based on SEM analysis, cracks occurred on the surface of two-piece implants and were more pronounced. Cracks and the melting of the titanium surface of two-piece implants cleaned with Er:YAG laser at 100 or 200 mJ were observed. The specimens treated with the ultrasonic scaler with a plastic curette showed the remaining dark debris on the titanium surface. We recommend using Er:YAG laser at 50 mJ/30 Hz during flapless implants debridement.

In Vitro Examination of the Use of Er:YAG Laser to Retrieve Lithium Disilicate Crowns from Titanium Implant Abutments.

PURPOSE: Removal of cement-retained implant crowns can be difficult and often requires sectioning of the prosthesis by rotary instruments. This study aimed to measure how much time is required in crown removal and the temperature changes when erbium-doped yttrium aluminum garnet (Er:YAG) laser was used to retrieve lithium disilicate crowns from titanium implant abutments luted with composite resin (CR) cement and resin-modified glass ionomer (RMGI). MATERIALS AND METHODS: Forty identical lithium disilicate crowns were fabricated for prefabricated titanium abutments. CR and RMGI cements were used to lute the crowns, 20 specimens for each cement. Specimens were kept in 100% humidity for 48 hours. Er:YAG laser was then used to facilitate the crown retrieval. The retrieval time was recorded. The temperature changes at the abutment level for each type of cement were recorded during irradiation of 10 specimens for each type of cement from 1 to 10 minutes. Data were analyzed using t-test (ɑ = 0.01) and paired t-test (ɑ = 0.05). The surfaces of the crown and the abutment were further examined using scanning electron microscopy (SEM). RESULTS: The average times of crown removal from titanium abutments were 196.5 seconds for CR and 97.5 seconds for RMGI groups with statistical significance (p < 0.001). The temperatures measured from 1 to 10 minutes of irradiation ranged from 18° to 20.8° for CR and 18° to 23° for RMGI at the abutment surface, and 22.1° to 24.6° for CR and 22° to 24.8° for RMGI at the crown surface. No statistical differences were observed between temperature changes at the abutment or the crown for each cement (p = 0.63); however, there was a statistically significant difference between the temperatures at the abutment and crown for both cements (p < 0.001). SEM examination showed no visible damage caused by treatment with Er:YAG laser. CONCLUSIONS: It is faster to remove lithium disilicate crowns from titanium implant abutments when luted with RMGI compared to CR cement. The temperature rise was higher in the crown compared to the abutment. The type of cement had no effects on temperature changes. Heat generated from Er:YAG irradiation does not appear to be high enough to have any adverse effect on implant osseointegration.

Er:YAG Laser for Metal and Ceramic Bracket Debonding: An In Vitro Study on Intrapulpal Temperature, SEM, and EDS Analysis.

OBJECTIVE: To evaluate the effects of bracket removal using an erbium laser on the pulp temperature and enamel surface. BACKGROUND: Removal of orthodontic brackets with conventional debonding pliers may result in enamel cracks. To avoid damage to the enamel surface and effectively remove metal or ceramic brackets, different types of lasers, such as Nd:YAG, CO2, TM:YAP, diode laser, or Er:YAG, have been introduced for debonding. MATERIALS AND METHODS: A total of 55 brackets (n = 55; 20 metal and 35 ceramic ones) were bonded to 55 caries-free premolars extracted for orthodontic indications. Brackets were irradiated with Er:YAG laser (Morita, Irvine, CA) with a wavelength of 2940 nm at a power of 3.4 W, energy 170 mJ, frequency 20 Hz, pulse duration 300 µs, tip diameter 0.8 mm, air/fluid cooling 3 mL/s, and time of irradiation: 6 sec. Debonding was made by scanning (n = 15; 6 sec irradiation at distance of 2 mm from the bracket with an "S" shape movement) and circular (n = 15; 6 sec irradiation at distance of 1 mm from the bracket) motion technique in ceramic brackets or the circular motion technique in metal brackets (n = 15). The number of 10 nonirradiated teeth with ceramic (n = 5) or metal brackets (n = 5) was used as a control in SEM test and EDS analysis. The damage in tooth enamel surface and the calcium percentage were analyzed by means of scanning electron microscope (JEOL 6610LV, JEOL, Japan) and energy dispersive X-ray spectroscopy (EDS, Oxford, United Kingdom). Temperature changes in the pulp were measured by K-type thermocouple. Evaluation of the Adhesive Remnant Index (ARI) on the enamel surface of each tooth was examined after bracket debonding. RESULTS: The scanning method has caused significantly lower temperature increase (mean: 0.83°C) compared with circular motion technique around the ceramic brackets (mean: 1.78°C; p = 0.0001) or the metal brackets (mean: 1.29°C; p = 0.015). ARI score showed no differences between the study groups (p = 0.57). SEM analysis revealed no cracks on enamel surface after laser-assisted debonding in comparison with the control samples where cracks were found. EDS showed a higher mean percentage of the calcium (30.7-85.8%) for all test groups compared with control samples (mean: 7%; p = 0.0002). The amount of the calcium elements was higher for metal brackets in comparison with ceramic ones (p = 0.0002). CONCLUSIONS: Er:YAG laser-assisted debonding causes a minor increase in the pulp temperature and reduced the risk of enamel damage compared with conventional bracket removal.