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J Microsc ; 237(1): 89-95, 2010 Jan.
Article in English | MEDLINE | ID: mdl-20055922

ABSTRACT

A three-dimensional (3D) internal structure observation system based on serial sectioning was developed from an ultrasonic elliptical vibration cutting device and an optical microscope combined with a high-precision positioning device. For bearing steel samples, the cutting device created mirrored surfaces suitable for optical metallography, even for long-cutting distances during serial sectioning of these ferrous materials. Serial sectioning progressed automatically by means of numerical control. The system was used to observe inclusions in steel materials on a scale of several tens of micrometers. Three specimens containing inclusions were prepared from bearing steels. These inclusions could be detected as two-dimensional (2D) sectional images with resolution better than 1 mum. A three-dimensional (3D) model of each inclusion was reconstructed from the 2D serial images. The microscopic 3D models had sharp edges and complicated surfaces.


Subject(s)
Imaging, Three-Dimensional/methods , Microtomy , Steel/analysis , Materials Testing/instrumentation , Materials Testing/methods , Microtomy/instrumentation , Microtomy/methods , Sensitivity and Specificity , Ultrasonics , Vibration
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