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Diversely substituted sugar-linked alpha,beta-unsaturated gamma-lactones from sugar-derived Baylis-Hillman adducts via a RCM.
Krishna, Palakodety Radha; Narsingam, M.
J Comb Chem ; 9(1): 62-9, 2007.
Article in English | MEDLINE | ID: mdl-17206833

ABSTRACT

A versatile protocol for the production of sugar-linked alpha,beta-unsaturated gamma-lactones with stereochemical and functional group diversity is described starting from sugar-derived Baylis-Hillman adducts via ring-closing metathesis.


Subject(s)
Alkenes/chemical synthesis , Carbohydrates/chemical synthesis , Lactones/chemical synthesis , Alkenes/chemistry , Carbohydrates/chemistry , Combinatorial Chemistry Techniques/methods , Lactones/chemistry , Magnetic Resonance Spectroscopy , Molecular Structure , Optical Rotation , Spectrometry, Mass, Electrospray Ionization , Spectrophotometry, Infrared , Stereoisomerism
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