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Org Lett ; 13(13): 3292-5, 2011 Jul 01.
Article in English | MEDLINE | ID: mdl-21657252

ABSTRACT

Powdery crystals of p-tert-butylthiacalix[4]arene (2) selectively include EtOH from 1:1 mixtures of MeOH-EtOH and EtOH-PrOH, and EtCO(2)H from HCO(2)H-EtCO(2)H. On the other hand, no acid is included from HCO(2)H-MeCO(2)H, even though MeCO(2)H is included from the neat acid. The origins of these phenomena are discussed based on X-ray analysis of inclusion crystals prepared separately by crystallization.


Subject(s)
Alcohols/chemistry , Carboxylic Acids/chemistry , Phenols/chemistry , Crystallography, X-Ray , Models, Molecular , Molecular Structure
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