Analysis of Marginal Adaptation of Porcelain Laminate Veneers Produced by Computer-Aided Design/Computer-Assisted Manufacturing Technology: A Preliminary In Vitro Study.

PURPOSE: To analyze the marginal adaptation of computer-aided design/computer-assisted manufactured (CAD/CAM) porcelain laminate veneers. MATERIALS AND METHODS: A total of 25 three-dimensional (3D) machine-milled laminate veneers were divided into five groups of five each according to fabrication material (E-max; Empress; Lava Ultimate; Suprinity; and Vita Mark II) and cemented in 25 prepared acrylic central incisors. Digital microscopy images (×7.5 magnification) were analyzed for gaps in the mesial/distal surfaces of the prepared tooth and in the cervical, medial, and incisal thirds. RESULTS AND CONCLUSION: All CAD/CAM laminate veneers except for Empress and Suprinity in the middle and incisal thirds showed good results (ie, gaps < 120 µm in the cervical, middle, and incisal thirds).

Assessment of the mechanical properties of glass ionomer cements for orthodontic cementation

OBJECTIVE: To evaluate the mechanical properties of three glass ionomers cements (GICs) used for band cementation in Orthodontics. METHODS: Two conventional glass ionomers (Ketac Cem Easy mix/3M-ESPE and Meron/Voco) and one resin modified glass ionomer (Multi-cure Glass ionomer/3M-Unitek) were selected. For the compressive strength and diametral tensile strength tests, 12 specimens were made of each material. For the microhardness test 15 specimens were made of each material and for the shear bond strength tests 45 bovine permanent incisors were used mounted in a self-cure acrylic resin. Then, band segments with a welded bracket were cemented on the buccal surface of the crowns. For the mechanical tests of compressive and diametral tensile strength and shear bond strength a universal testing machine was used with a crosshead speed of 1,0 mm/min and for the Vickers microhardness analysis tests a Microdurometer was used with 200 g of load during 15 seconds. The results were submitted to statistical analysis through ANOVA complemented by Tukey's test at a significance level of 5%. RESULTS: The results shown that the Multi-Cure Glass Ionomer presented higher diametral tensile strength (p < 0.01) and compressive strength greater than conventional GICs (p = 0.08). Moreover, Ketac Cem showed significant less microhardness (p < 0.01). CONCLUSION: The resin-modified glass ionomer cement showed high mechanical properties, compared to the conventional glass ionomer cements, which had few differences between them.

OBJETIVO: avaliar as propriedades mecânicas de três cimentos de ionômero de vidro (CIVs) utilizados para cimentação de anéis ortodônticos. MÉTODOS: foram utilizados dois CIVs convencionais (Ketac Cem Easy mix/3M-ESPE e Meron/Voco) e um CIV modificado por resina (Multi-Cure Glass ionomer/3M-Unitek). Para os testes de resistência à compressão e tração diametral, foram confeccionados 12 corpos de prova de cada material. Para os testes de microdureza, foram confeccionados 15 corpos de prova de cada material; para os testes de resistência de união ao cisalhamento, foram utilizados 45 dentes bovinos incluídos em resina acrílica, sobre os quais foi cimentada uma lâmina de anel ortodôntico com braquete soldado a ela para a realização dos ensaios. Para os testes de compressão, tração diametral e cisalhamento, foi utilizada uma máquina universal de ensaios a uma velocidade de 1mm/min; para os testes de microdureza Vickers, foi utilizado um microdurômetro com 200g de carga durante 15 segundos. Os resultados foram submetidos à análise estatística ANOVA, complementada pelo teste de Tukey ao nível de significância de 5%. RESULTADOS: os resultados demonstraram que o Multi-Cure Glass Ionomer apresentou resistência à tração diametral significativamente maior (p < 0,01) e maior resistência à compressão (p = 0,08) em relação aos CIVs convencionais. Além disso, o Ketac Cem apresentou microdureza significativamente maior que os demais materiais (p < 0,01). CONCLUSÃO: o CIV modificado por resina apresentou propriedades mecânicas superiores às dos CIVs convencionais, que, por sua vez, apresentaram poucas diferenças entre si.

Influence of ultrasound and diamond burs treatments on microtensile bond strength.

OBJECTIVE: To compare surface treatments with CVDentUS ultrasound tips (UT) and KGSorensen diamond burs (DB) on etched (e) and non-etched (n/e) dentin. The microtensile bond strength (µTBS) was measured and fractography was assessed by scanning electron microscope (SEM). MATERIALS AND METHODS: Sixteen molars were divided into four groups of four teeth each according to treatment (DB-n/e; DB-e; UT-n/e; UT-e). The teeth were restored, sectioned into samples for µTBS (n=40) and tested on a EMIC DL-2000 universal machine (0.5 mm/min) and analyzed by SEM for fracture classification. STATISTICAL ANALYSIS: For analysis of the data on µTBS, the two-way ANOVA, using treatment and acid etching as fixed factor, and the Tukey test were used (α=0.05). To failures classification in cohesive in dentin (CD); cohesive in composite resin (CC); cohesive interfacial on base or top of hybrid layer (CBT); cohesive in adhesive (CA); mixed (M); interfacial on smear layer (S) the Fisher's exact test (α=0.05) was performed. RESULTS: The mean values of µTBS (in MPa) in the different groups were as follows: UT-e: 45.31 ± 8.16; DB-e: 34.04 ± 9.29; UT-n/e: 15.17 ± 3.71; and DB-n/e: 9.86 ± 3.80. On analysis of the SEM micrographs, the DB-n/e group showed total obstruction of dentinal tubules; the UT-n/e group showed partial desobstruction of dentinal tubules and irregular surface; the DB-e group showed complete desobstruction of dentinal tubules; and the UT-e group showed complete desobstruction of dentinal tubules and irregular surface. CONCLUSION: The combination of ultrasound treatment and acid etching provides high values of µTBS. An association exists between CA/CC failures and the UT method, CBT failure and the DB method, CBT/CC failures and etching, S failure and non-etching.

Cytotoxicity of esthetic, metallic, and nickel-free orthodontic brackets: cellular behavior and viability.

INTRODUCTION: In this study, we evaluated the cellular viability of various esthetic, metallic, and nickel-free orthodontic brackets. METHODS: The sample was divided into 11 groups (n = 8): cellular control, negative control, positive control, metallic, polycarbonate, 2 types of monocrystalline ceramic, 3 types of nickel free, and polycrystalline ceramic brackets. Cell culture (NIH/3T3-mice fibroblasts) was added to the plates of 96 wells containing the specimens and incubated in 5% carbon dioxide at 37°C for 24 hours. Cytotoxicity was analyzed qualitatively and quantitatively. Cell growth was analyzed with an inverted light microscope, photomicrographs were obtained, and the results were recorded as response rates based on modifications of the parameters of Stanford according to the size of diffusion halo of toxic substances. Cell viability was analyzed (MTT assay); a microplate reader recorded the cell viability through the mitochondrial activity in a length of 570 nm. The values were statistically analyzed. RESULTS: All tested brackets had higher cytotoxicity values than did the negative control (P <0.05), with the exception Rematitan and Equilibrium (both, Dentaurum, Ispringen, Germany) (P >0.05), suggesting low toxicity effects. The values showed that only polycarbonate brackets were similar (P >0.05) to the positive control, suggesting high toxicity. CONCLUSIONS: The brackets demonstrated different ranges of cytotoxicity; nickel-free brackets had better biocompatibility than the others. On the other hand, polycarbonate brackets were made of a highly cytotoxic material for the cells analyzed.

Evaluation of inorganic particles of composite resins with nanofiller content.

The purposes of this study were evaluate by energy dispersed X-ray (EDS) and scanning electron microscopy (SEM) the inorganic particles of three nanofilled composite resins, comparing particles sizes, shape and composition, and the filler weight content by thermogravimetric analyzes (TGA). Three composite resins classified as nanofilled were selected to this study: Esthet-X; Grandio; Filtek Supreme XT. The shade was standardized (A2) for enamel (E) or dentin (D). Ten samples with 20 mg (±10 mg) of each composite resin were submitted to thermogravimetric analyzes (TGA) in order to record the filler weight content (wt%). The amount of inorganic phase ranged from 75.75 to 87 wt%, to Esthet-X (D) and Grandio (D), respectively. The filler composition was analyzed by energy dispersed X-ray (EDS), and the size and shape were evaluated by scanning electron microscopy (SEM). The filler average size (µm) obtained by SEM were: Esthet-X (E) 1.16; Esthet-X (D) 1.39; Filtek Supreme XT (E) 0.6 (nanocluster); Filtek Supreme XT (D) 1.14 (nanocluster); Grandio (E) 2.05 and Grandio (D) 3.1. Silica (SiO2), Ba and Al were observed through EDS. The shape of Esthet-X and Grandio fillers showed similar characteristics with high quantity of irregular inorganic particles and heterogeneous filler. However, Filtek Supreme XT showed spherical and regular particles with homogeneous distribution and sizes. Based in the analysis of nanofilled composites inorganic phase, inconsistencies of weight content, composition, shape and size can be stated between the literature and manufacturer's instructions.

Evaluation of mechanical properties on three nanofilled composites.

The purpose of this study was to evaluate the mechanical behavior of three composites with nanoparticles Filtek Z350 XT (3M ESPE), Esthet X (Dentsply), Grandio (Voco) in enamel and body shades (A2) trough nanohardness, elastic modulus, compressive strength test, flexural strength test, diametral tensile strength, flexural modulus, weight filler content and Knoop microhardness. One sample of each material was submitted to nanohardness and elastic modulus. Five values of ten indentations were considered valids inside confidence intereval. Ten samples of each material were submitted to compressive strength, flexural strength and diametral tensile strength test at universal testing machine. The flexural modulus test was calculated based on flexural strength results. Ten samples of each group were submitted to knoop microhardness test. The results were submitted to ANOVA and Tukey statistical tests. The highest inorganic weight filler content for Grandio was registered after the organic mould decomposition. After statistical analysis Grandio showed the highest averages for nanohardness, elastic modulus, flexural modulus and knoop microhardness. For diametral tensile strength Grandio and Filtek Z350 XT obtained the highest averages. The tested composite resins ranged similar medias statistically for compressive strength. For flexural strength Filtek Z350 XT and Esthet X showed the highest averages. The results suggest that the weight filler content, the filler size and shape and the contact surface between nanofillers and organic phase has direct relation with composite resins with nanoparticles mechanical properties. Further studies should be carried out to improve the knowledge of composites with nanoparticles mechanical behavior.

Release of toxic ions from silver solder used in orthodontics: an in-situ evaluation.

INTRODUCTION: The objective of this study was to test the hypothesis that toxic metallic ions in silver solder used in orthodontics are released into saliva. METHODS: The sample included 60 children, 8 to 14 years of age, divided into 2 groups (n = 30 in each group): the control group and the study group (needing maxillary expansion with the hyrax appliance). For analysis of the release of metallic ions, saliva samples from each patient were collected at 6 times in both groups: before placement of the appliance and 10 minutes, 24 hours, and 7, 30, and 60 days after placement. The analysis of saliva was performed by atomic absorption spectrophotometry in a graphite oven to determine the concentrations of cadmium, copper, zinc, and silver ions. Statistical analyses were performed by the mixed model for repeated-measures covariance structure of the symmetrical component type, at P <0.05. RESULTS: The ion concentrations in the control group had low values for cadmium, copper, and zinc (P >0.05); for silver ions, the values did not reach the detection limit. In the study group, all ions showed expressive concentrations at 10 minutes after placement of the appliance (P <0.001), with the highest mean for copper (70.60 µg/L) and the lowest mean for zinc (0.07 µg/L). Comparison between groups revealed significant differences for copper (all periods), zinc (10 minutes, 24 hours, 7 and 30 days), and for cadmium only at 10 minutes. CONCLUSIONS: Great amounts of these ions were released, with the highest concentrations immediately after placement of the appliance.

Can we add chlorhexidine into glass ionomer cements for band cementation?

OBJECTIVE: To test if the addition of chlorhexidine digluconate (CHD) might influence the mechanical properties and antibacterial properties of two different conventional glass ionomer cements (GICs) used for band cementation. MATERIALS AND METHODS: Two commercial brands of conventional GICs were used: Ketac Cem Easymix (3M/ESPE, St Paul, Minn) and Meron (Voco, Cuxhaven, Germany). The cements were manipulated in their original composition and also with 10% and 18% CHD in the liquid to create a total of six groups. Diametral tensile strength, compressive strength, microhardness, shear bond strength, and antibacterial effects in 5, 45, and 65 days against Streptococcus mutans were tested in all groups, and the data were submitted to statistical analyses. RESULTS: There were no significant differences between the groups of the same material in diametral tensile, compressive strength, and shear bond strength (P > .05). There was significant improvement in the microhardness to the Ketac Cem Easymix (P < .001). GICs with the addition of CHD showed significant inhibition of S. mutans growth in comparison with the control groups at the three time points evaluated (P < .001). The addition of 18% CHD resulted in higher bacterial inhibition (P < .001). CONCLUSIONS: The addition of chlorhexidine digluconate to conventional GICs does not negatively modify the mechanical properties and may increase the antibacterial effects around the GICs even for relatively long periods of time.

Surface changes in denture soft liners with and without sealer coating following abrasion with mechanical brushing.

AIM: To evaluate the surface alterations of soft liners with or without sealer coating following abrasion with mechanical brushing. METHODS: Thirty specimens were made of a methacrylate- (Coe-Soft) and a siloxane-based material (Ufi-Gel SC), and 15 received two coatings of surface sealer. The specimens were submitted to a mechanical brushing-dentifrice assay under 200g of force at 250 cycles/min. Mechanical brushing was simulated for a period of 1 (1250 cycles) and 6 months (5000 cycles). Surface roughness (Ra parameter) was measured, and scanning electron microscopy (SEM) images were obtained. Ra data were analysed by anova for repeated measures and Bonferroni's test (alpha=0.05). RESULTS: Ra increased from baseline to 6 months regardless of sealer coating. At baseline, only Coe-Soft without sealer had a higher Ra than the other groups. After 1 month, the Ra of Coe-Soft with sealer was three-fold higher than the Ra at baseline; the other groups showed no significant increase of Ra. SEM images showed degradation of the soft liners over time, except for the Ufi-Gel SC with sealer, which displayed minimum alteration of surface texture. CONCLUSION: Sealer coating reduced the surface degradation of the tested soft liners, but the protective effect was more pronounced for the siloxane-based material.

Development of glass ionomer cement modified with seashell powder as a scaffold material for bone formation / Desenvolvimento de cimento de ionômero de vidro modificado com pó de conchas como material estrutural para formação óssea

PURPOSE: The present study examined the possibility of modifying the structural properties of glass ionomer cement by adding seashells to form a possible 'scaffold' material for cases of bone formation. METHODS: White and black seashells were ground into a fine, homogeneous powder. To analyze their composition, the seashell samples were submitted to EDX and X-Ray diffraction. The ground seashells were mixed with the glass ionomer cement at either 1, 5 or 10 percent concentrations (in weight). Samples without any seashells were used as the control group. Solutions and GIC samples were analyzed for pH measurement. The structural and superficial analysis of samples was performed by using scanning electron microscopy (SEM). RESULTS: There was no difference in pH values among the tested solutions with different seashell concentrations (1, 5 and 10 percent). In the GIC samples with the shells, the pH values were close to 7.0. The EDX and X-Ray diffraction showed calcium carbonate (CaCO3) peaks for the shell samples. The superficial SEM analysis demonstrated that the samples containing seashells had framework formations in their structures. CONCLUSION: Although there is a need for biocompatibility and cellular cytotoxicity testing in vitro, as well as in vivo evaluation, seashells could be used in glass ionomer cement aiming at the development of a 'scaffold' material for bone grafting or osseointegration.

OBJETIVO: Este estudo examinou a possibilidade de modificar as propriedades estruturais do cimento de ionômero de vidro (CIV) pela adição de conchas para formar um material estrutural, com objetivo de uso em casos de formação óssea. METODOLOGIA: Conchas de cor branca e preta foram transformadas em um pó fino e homogêneo e sua composição foi analisada por EDX e difração por RX. O pó de concha foi misturado a CIV nas concentrações de 1, 5 ou 10 por cento (em peso) para a confecção das amostras. Amostras sem pó de concha foram usadas como grupo controle. Foram realizadas medições de pH de soluções do pó de conchas e das amostras de CIV. A análise estrutural e superficial das amostras foi realizada por microscopia eletrônica de varredura (MEV). RESULTADOS: Não houve diferença de pH entre as soluções testadas com diferentes concentrações de pó de concha (1, 5 ou 10 por cento). Nas amostras de CIV com conchas, os valores de pH foram próximos a 7,0. Os métodos de EDX e difração por RX mostraram picos de carbonato de cálcio (CaCO3) para as amostras com conchas. A análise por MEV demonstrou que as amostras com pó de conchas tinham formações estruturais diferentes do controle. CONCLUSÃO: Embora haja necessidade de testes de biocompatibilidade e citotoxicidade celular, assim como avaliação in vivo, as conchas poderiam ser utilizadas como material de modificação estrutural do cimento de ionômero de vidro em casos de material para enxerto ósseo ou osseointegração.

Relationship between filler content and selected mechanical properties of six microhybrid composites / Relação entre o conteúdo de carga e propriedades mecânicas de seis resinas compostas microhíbridas

PURPOSE: The purpose of this study was to evaluate the influence of filler weight content on selected mechanical properties of six microhybrid composite resins. METHODS: Compressive strength, elastic modulus, Vickers microhardness (VHN), and weight filler content were evaluated in the following dental composites: Admira (AD), Charisma (CH), InTen-S (IN), Tetric Ceram (TC), Point 4 (P4), and Z250 (Z2). RESULTS: Mean values for compressive strength (MPa) ranged from P4 76.60 to Z2 222.33. The elastic moduli (GPa) ranged from IN 2.56 to Z2 4.59. Microhardness VHN ranged from P4 50.53 to Z2 87.88. Filler weight content (Wt percent) ranged from IN 72.51 to TC 79.56. Significant differences were found between the composites (ANOVA/Tukey's, P<0.05). CONCLUSION: Z2 had the highest compressive strength; Z2 and TC showed the highest elastic modulus, VHN and filler weight content. Weight filler content had a strong influence on mechanical properties (0.78

OBJETIVO: O objetivo deste estudo foi avaliar a influência do conteudo de carga, em peso, de seis resinas compostas microhíbrida sobre determinadas propriedades mecânicas. METODOLOGIA: A resistência à compressão, módulo de elasticidade, microdureza Vickers (VHN) e conteúdo de carga de peso foram avaliados nas seguintes resinas compostas: Admira (AD), Charisma (CH), InTen-S (IN), Tetric Ceram (TC), Point 4 (P4) e Z250 (Z2). RESULTADOS: Os valores médios de resistência à compressão (MPa) variaram de P4 76,60 a Z2 222,33. Os módulos de elasticidade (GPa) variou de IN 2,56 a Z2 4,59. A microdureza VHN variou de P4 50,53 a Z2 87,88. O conteúdo de carga em peso (Wt por cento) variou de IN 72,51 a TC 79,56. Foram encontradas diferenças significativas entre as resinas compostas (ANOVA/Tukey's, P<0,05). CONCLUSÃO: A resina Z2 teve a maior resistência à compressão; Z2 e TC apresentaram maiores módulo de elasticidade, VHN e conteúdo de carga em peso. O conteúdo de carga em peso teve uma forte influência nas propriedades mecânicas avaliadas (0,78

Análise in vitro do alívio interno de coroas totais após a utilização de espaçadores para troqueis / In vitro analysis of the internal relief of full crowns after the use of die spacers

OBJETIVO: Avaliar o alívio interno de coroas totais após a utilização de espaçadores para troqueis. MÉTODOS: Foram confeccionadas 20 coroas metálicas, em níquel-cromo, divididas em quatro grupos de cinco coroas de acordo com o número de camadas de espaçador empregadas. Cada coroa foi submetida à medição do espaço interno, formado entre as suas paredes internas e a parede externa do troquel mestre metálico. Para a medição, uma silicona de adição ultraleve foi injetada no interior das coroas. As amostras assim obtidas foram seccionadas ao meio no sentido ocluso-cervical de modo a obter duas metades, as quais foram escaneadas em alta resolução juntamente com um paquímetro. As imagens obtidas foram levadas ao software Image Tool 3.0 para medição do alívio interno obtido em dois pontos equidistantes em cada uma das paredes axiais e na parede oclusal. Os valores médios obtidos em micrômetros (µm) para condição de alívio nas diferentes paredes foram submetidos à análise estatística através da análise de variância, teste de Tukey e teste t de Student. RESULTADOS: À medida que se aumenta o número de camadas de espaçador aumenta também o alívio interno obtido. O Grupo 4 demonstrou uma espessura elevada na parede oclusal, a qual foi equivalente ao Grupo 2 e explicada pelo não escoamento do material para moldagem no interior da coroa. CONCLUSÃO: A aplicação de espaçadores para troqueis antes da ceroplastia permite ao operador obter fundições com alívio interno controlado, como condição para obter espaço suficiente para o agente cimentante.

OBJECTIVE: This research evaluated the internal relief in full crowns after the use of die spacers. METHODS: Twenty nickel-chromium crowns were made and divided into four groups of five crowns each, according to the number of die spacer layers used .The space between the inside walls and outside walls of the metal master die of each crown was measured. The measurement was done by injecting a very light-bodied addition silicone inside the crowns. The resulting samples were cut in half along the occlusal cervical plane and the halves were scanned in high resolution together with a slide caliper. The resulting images were transferred to the Image Tool 3.0 software for measuring the internal relief obtained from two equidistant points on each axial wall and on the occlusal wall. The relief means in micrometers in the different walls were statistically analyzed by analysis of variance, Tukey test and Student's t-test. RESULTS: As the number of spacer layers increases, so does internal relief. The occlusal wall of Group 4 was very thick, equivalent to that of Group 2, which is explained by the impression material not flowing inside the crown. CONCLUSION: The application of die spacers before waxing allows the operator to obtain casts with controlled internal reliefs, making room for the cement.

Effect of conditioner on microtensile bond strength of self-adhesive resin cements to dentin.

OBJECTIVE: Evaluate, in vitro, the microtensile bond strength (µTBS) of RelyX ARC conventional resin cement and RelyX Unicem and Maxcem self-adhesive resin cements to dentin, and the influence of polyacrylic acid pretreatment on the µTBS. MATERIAL AND METHODS: Flat dentin surfaces were obtained in 15 third molars which were randomly divided into 5 groups: Group 1 - RelyX ARC (control); Group 2 - RelyX Unicem; Group 3 - Maxcem Elite; Group 4 - 22.5% polyacrylic acid and RelyX Unicem; Group 5 - 22.5% polyacrylic acid and Maxcem Elite. A block of composite resin was built over the resin cements. The samples were sectioned to obtain beams, and 20 specimens for each group were submitted to µTBS on a universal testing machine. Failure modes were analyzed by scanning electron microscopy. RESULTS: According to ANOVA and Tukey test, the highest µTBS mean (MPa) was obtained with RelyX ARC (21.38), which did not differ statistically from Maxcem Elite with polyacrylic acid pretreatment (19.22) and RelyX Unicem with polyacrylic acid pretreatment (17.75) (p>0.05). The latter two groups did not differ statistically from RelyX Unicem (16.98) (p>0.05). The lowest mean was obtained for Maxcem Elite (6.43), which differed statistically from the other groups (p<0.05). All failures were adhesive for Maxcem Elite without polyacrylic acid pretreatment, and mixed failures were predominant in the other groups. CONCLUSIONS: RelyX ARC achieved higher µTBS to dentin in comparison to the self-adhesive resin cements. Polyacrylic acid pretreatment was effective in improving the µTBS of Maxcem Elite, but did not influence the µTBS for RelyX Unicem.

Influência de variáveis metodológicas na resistência de união ao cisalhamento / The influence of the methodological variables on the shear bond strength

OBJETIVO: avaliar a influência de diferentes variáveis metodológicas sobre a resistência de união ao cisalhamento em estudos in vitro. MÉTODOS: foram utilizados 105 incisivos permanentes bovinos, seccionados ao nível do colo dentário. A porção coronária foi inclusa em tubos de PVC, com resina acrílica autopolimerizável, e com face vestibular voltada para cima. Todos os corpos de prova foram preparados para a colagem com profilaxia e condicionamento ácido na região central das coroas, onde foram posicionados braquetes Morelli® de incisivos centrais superiores, com resina Concise® Ortodôntico (3M/Unitek). Foram determinados três grupos de acordo com a variável estudada: (Grupo 1) - meio de armazenamento dos dentes, previamente à inclusão e à colagem, com solução de timol 0,1 por cento (a), água destilada (b) e congelamento (c); (Grupo 2) - velocidade da célula de carga da máquina de ensaio de 0,5 (a), 1,0 (b) e 2,0mm/min (c) e (Grupo 3) - diferentes marcas comerciais de ácidos fosfóricos a 37 por cento, 3M/Unitek (a), AcidGel (b) e Attack Tek (c). Os corpos de prova foram submetidos ao ensaio mecânico de resistência ao cisalhamento através da máquina Emic DL2000®. Os dados foram analisados estatisticamente por meio do Teste t Student para amostras independentes. RESULTADOS: os resultados demonstraram que no Grupo 1 o subgrupo de congelamento apresentou maiores valores em relação aos outros dois subgrupos, porém sem diferença estatisticamente significativa (p > 0,05). No Grupo 2, a força no momento da ruptura foi menor à medida que era aumentada a velocidade da célula de carga, porém sem diferença significativa entre os subgrupos. No Grupo 3, o ácido da 3M/Unitek apresentou a maior média em MPa, no entanto, também sem diferença significativa entre os subgrupos. CONCLUSÕES: conclui-se, portanto, que as variáveis analisadas neste trabalho não apresentaram influência suficiente para determinação de diferenças estatisticamente significativas...

AIM: Evaluate the influence of several methodological variables on the shear bond strength of in vitro studies. METHODS: 105 bovine incisors were sectioned at the cervical level. The coronary portion was included in PVC rings, fulfilled with auto polymerized acrylic resin, with its labial faces turned to the top. All the samples were prepared for bonding, cleaned and acid etched on the central area of the crowns. In this area, central incisors' MorelliÕ brackets were bonded with ConciseÕ (3M/Unitek). Three testing groups were established, according to the studied variable: Group 1 - storage previous to bonding (a-Thymol 0,1 percent; b- distilled water; c- freezing); Group 2 - crosshead speed of the universal testing machine (a- 0,5mm/min; b- 1,0mm/min; c- 2,00mm/min) and Group 3 - commercial brand of 37 percent phosphoric acid (a- 3M/Unitek; b- Acid Gel; c- Attack Tek). The shear bond strength test was performed at the Emic DL2000Õ universal testing machine. Data was analyzed through the Student's t test for independent samples. RESULTS: In Group 1, the freezing group showed the higher values of shear bond strength when compared to the others, although no statistical difference was observed (p>0,05). For Group 2, the higher the crosshead speed, the lower the shear bond strength, with no statistical difference. In Group 3, the 3M/Unitek brand showed the highest average of shear bond strength in MPa, but also no statistical difference was shown. CONCLUSIONS: The variable analyzed in this research had not presented enough influence to determine significant differences between the results.

Marginal fit analysis of premachined and castable UCLA abutments.

This study evaluated the fit between implants and premachined and castable UCLA abutments. All plastic specimens were cast using the conventional technique in accordance with the manufacturer's instructions. Five specimens of each experimental group were measured for vertical and horizontal gaps by scanning electronic microscopy (Phillips XL 30 model, Holland). Gold UCLA (vertical gap: 2.15 microm, horizontal gap: 11.30 microm) and castable rotational UCLA (vertical gap: 14.91 microm, horizontal gap: 59.41 microm) groups showed the lowest and highest mean values, respectively (Neodent, Curitiba, Parana, Brazil). In general, the castable UCLA abutments showed poorer marginal fit than the premachined abutments.

Stress distribution of an internal connection implant prostheses set: a 3D finite element analysis.

OBJECTIVE: This study evaluated the stress distribution by loads, under a internal connection implant system with two sort of abutment screws and prosthetic crown models at ten observation points. MATERIALS AND METHOD: The analysis were made in two models with internal butt joint, and with gold and titanium screw, respectively. The load was 382N with 90 masculine to the occlusal surface and 15 masculine to the implant axis at 4 and 6 mm from the implant center. RESULTS: In both models, a large amount of stress was located around the implant neck and little stress was concentrated along the abutment screw. CONCLUSION: The simulations made suggest that the internal connection protects the abutment screw from the accumulated stresses; however, it exposes the implant walls to these stresses.

Marginal fit analysis of premachined and castable UCLA abutments

This study evaluated the fit between implants and premachined and castable UCLA abutments. All plastic specimens were cast using the conventional technique in accordance with the manufacturer's instructions. Five specimens of each experimental group were measured for vertical and horizontal gaps by scanning electronic microscopy (Phillips XL 30 model, Holland). Gold UCLA (vertical gap: 2.15 μm, horizontal gap: 11.30 μm) and castable rotational UCLA (vertical gap: 14.91 μm, horizontal gap: 59.41 μm) groups showed the lowest and highest mean values, respectively (Neodent, Curitiba, Parana, Brazil). In general, the castable UCLA abutments showed poorer marginal fit than the premachined abutments.

Esse estudo avaliou a adaptacao entre implantes pilares UCLA usinados e fundidos. Todos os corpos de prova de plastico foram fundidos usando tecnica de fundicao convencional de acordo com o fabricante. Cinco corpos de prova foram avaliados em relacao a desadaptacao vertical e horizontal utilizando um Microscopio Eletronico de Varredura. Os grupos UCLA Ouro (desadaptacao vertical: 2.15 μm, horizontal : 11.30 μm) e UCLA rotacional fundido (desadaptacao vertical: 14.91 μm, horizontal: 59.41 μm) mostraram as medias mais baixas e mais altas, respectivamente. De uma maneira geral, os pilares UCLA fundidos mostraram adaptacao menor do que os pilares UCLA usinados.

Cytotoxicity of silver solder employed in orthodontics.

OBJECTIVE: To test the null hypothesis that the silver soldering employed in orthodontics is not cytotoxic for fibroblasts. MATERIALS AND METHODS: This in vitro study was performed using a culture of mice fibroblasts (lineage NIH/3T3), divided into four groups (n = 10 each): control, negative control (stainless steel archwire), positive control (amalgam disks), and test group (silver soldering). After cell culture in complete Dulbecco modified eagle medium and achievement of confluence in 80%, the suspension was added to the plates of 24 wells containing the specimens and incubated in an oven at 37 degrees C for 24 hours. The plates were analyzed on an inverted light microscope, photomicrographs were obtained, and the results were recorded as response rates based on modifications of the parameters of Stanford according to the size of the diffusion halo of the toxic substance and quantity of cell lysis. RESULTS: The results revealed a maximum response rate for the silver soldering group, as well as severe inhibition of cell proliferation and growth, more round cells with mostly darkened and granular aspects, suggesting lysis with cell death. A similar response was seen in the positive control group. CONCLUSION: The hypothesis is rejected. The silver soldering used in orthodontics represents a highly cytotoxic material for the cells analyzed.

Fracture strength of endodontically treated molars transfixed horizontally by a fiber glass post.

PURPOSE: To assess the effect of a horizontally transfixed fiber glass post placed between buccal and palatal surfaces, on the fracture strength of endodontically treated molar teeth with MOD cavities, either restored with resin-based composite, or not. METHODS: 75 sound maxillary human third molars were extracted, embedded in acrylic resin blocks and randomly assigned to five groups (n=15). Group A (sound teeth), (control) and Groups B, C, D and E, which were subjected to the following procedures after endodontic treatment: GB--(MOD+Endo), GC--(MOD+Endo+Post), GD--MOD and composite restoration (MOD+Endo+CR), GE--(MOD+Endo+Post+CR). The specimens were stored in distilled water at 37 degrees C for 24 hours. Later, a compressive force was applied by means of a universal testing machine at 1 mm/minute speed, parallel to the long axis of the teeth until fracture occurred. RESULTS: The means of the results (N) followed by the same letter represent no statistical difference by ANOVA and Tukey (P<0.05): GA = 4289.8 (+/- 1128.9)a, GB = 549.6 (+/- 120.7)b, GC = 1474.8 (+/- 338.1)c, GD = 1224.7 (+/- 236.0)c, GE = 2645.4 (+/- 675.1)d. In the analysis of qualitative variables, there was a tendency to cusp fracture in all groups except for Group C. The fiber glass post transfixed horizontally in a MOD cavity significantly increased the fracture resistance of the teeth restored with resin composite.

Influence of chisel width on shear bond strength of composite to enamel / Influência da largura do cinzel sobre a resistência ao cisalhamento da união esmalte/resina composta

Purpose: To evaluate the effect of chisel width on shear bond strength of composite to dental enamel. Methods: Sixty crowns of bovine incisors were embedded in acrylic resin, and their enamel surfaces were flattened and etched with 35% phosphoric acid. Single Bond (3M/ESPE) adhesive system and Z-250 (3M/ESPE) composite were used to build a cylindrical-shaped restoration perpendicular to the conditioned enamel flat surface. Specimens were divided into four groups and subjected to the shear bond strength testing using a chisel-shaped shearing blade with a 0.5, 1.0, 2.0, or 3.0 mm-width blunt edge in a universal testing machine at crosshead speed of 0.5 mm/min. Data on shear bond strength were analyzed by ANOVA and Duncan's test (á=0.05). Results: Shear bond strength means for the experimental groups were: 0.5 mm - 19.66 MPa; 1 mm - 18.78 MPa; 2 mm - 16.77 MPa; 3 mm - 16.06 MPa. Bond strength was significantly different between the groups tested with chisels of 0.5 and 3 mm-width (P=0.045) showing an inverse relationship between shear bond strength and chisel width. Conclusion: The results suggest that shear bond strength varies as a function of chisel width.

Objetivo: Avaliar a influência de diferentes larguras de cinzel sobre a resistência de união ao cisalhamento na interface esmalte dental/resina composta. Metodologia: As coroas de 60 dentes incisivos bovinos foram incluídas em resina acrílica e as superfícies vestibulares de esmalte foram planificadas e condicionadas com ácido fosfórico a 35 %. O sistema adesivo Single Bond (3M/ESPE) e de resina composta Z-250 (3M/ESPE) foram utilizados para fabricar restaurações cilíndricas de resina composta perpendiculares à superfície plana do esmalte condicionado. Para o teste de cisalhamento, os espécimes foram submetidos ao ensaio mecânico com cinzéis de 0,5 mm, 1,0 mm, 2,0 mm ou 3,0 mm de largura da parte ativa romba, em uma máquina de ensaio universal à velocidade de 0,5 mm/min. Os dados obtidos foram analisados por análise de variância e teste de Duncan ao nível de significância de 5 %. Resultados: As médias de resistência de união ao cisalhamento dos grupos testados foram: 0,5 mm - 19,66 MPa; 1,0 mm -18,78 MPa; 2,0 mm - 16,77 MPa; 3,0 mm - 16,06 MPa. Houve diferença estatisticamente significativa entre os grupos de 0,5 e 3,0 mm (P=0,045), com uma relação inversa entre resistência de união ao cisalhamento e largura do cinzel. Conclusão: Os resultados sugerem que a resistência de união ao cisalhamento sofre influência da largura do cinzel utilizado no ensaio.