Interferometer-based chemical sensor on chip with enhanced responsivity and low-cost interrogation.

We report experimental results of an interferometric chemical sensor integrated on a silicon chip. The sensor measures refractive index variations of the liquid that contacts exposed spiraled silicon waveguides on one branch of a Mach-Zehnder interferometer. The system requires neither laser tuning nor spectral analysis, but a laser at a fixed wavelength, and a demodulation architecture that includes an internal phase modulator and a real-time processing algorithm based on multitone mixing. Two devices are compared in terms of sensitivity and noise, one at 1550 nm wavelength and TE polarization, and an optimized device at 1310 nm and TM polarization, which shows 3 times higher sensitivity and a limit of detection of 2.24·10-7 RIU.

Distortion-corrected phase demodulation using phase-generated carrier with multitone mixing.

We present a novel phase generated carrier (PGC) demodulation technique for homodyne interferometers which is robust to modulation depth variations and source intensity fluctuations. By digitally mixing the waveform with a multitone synthetic function (a linear combination of harmonics of the modulating signal), distortion can become negligible even in presence of large variations of the modulation depth. The technique only requires two mixers and can also provide the DC component of the phase in real time, without needing any previously recorded data or ellipse-fitting algorithms. We validate the technique with simulated waveforms and with experimental data from a wavelength metering experiment using an integrated unbalanced interferometer on-chip, showing that the technique corrects distortion without increasing the noise with respect to the standard PGC technique.

Camera Calibration with Weighted Direct Linear Transformation and Anisotropic Uncertainties of Image Control Points.

Camera calibration is a crucial step for computer vision in many applications. For example, adequate calibration is required in infrared thermography inside gas turbines for blade temperature measurements, for associating each pixel with the corresponding point on the blade 3D model. The blade has to be used as the calibration frame, but it is always only partially visible, and thus, there are few control points. We propose and test a method that exploits the anisotropic uncertainty of the control points and improves the calibration in conditions where the number of control points is limited. Assuming a bivariate Gaussian 2D distribution of the position error of each control point, we set uncertainty areas of control points' position, which are ellipses (with specific axis lengths and rotations) within which the control points are supposed to be. We use these ellipses to set a weight matrix to be used in a weighted Direct Linear Transformation (wDLT). We present the mathematical formalism for this modified calibration algorithm, and we apply it to calibrate a camera from a picture of a well known object in different situations, comparing its performance to the standard DLT method, showing that the wDLT algorithm provides a more robust and precise solution. We finally discuss the quantitative improvements of the algorithm by varying the modules of random deviations in control points' positions and with partial occlusion of the object.

Dynamic phase extraction in high-SNR DAS based on UWFBGs without phase unwrapping using scalable homodyne demodulation in direct detection.

We demonstrate a Distributed Acoustic Sensor (DAS) based on Ultra-Weak Fiber Bragg Gratings (UWFBGs) using a scalable homodyne demodulation in direct detection. We show that a distributed interferometric system using delay and mixing of backscattering from consecutive identical gratings can be combined with a Phase-Generated Carrier Differentiate and Cross-Multiply (PGC-DCM) demodulation algorithm to perform dynamic measurements with high SNR, employing a simple narrowband laser and a pin photodiode. The proposed homodyne demodulation technique is suitable for real-time monitoring using distributed measurements, as it does not require computationally costly phase unwrapping common in conventional schemes and is robust against detrimental harmonic distortions, while not requiring additional mechanisms to handle division-by-zero operations. The demodulation scheme is also scalable, as it involves symmetric ordinary differentiation and integration operations suitable for processing with FPGA-based or analogue systems which, thanks to readily realizable schemes for implementing fractional order calculus, are also candidates for small-scale integration. We experimentally demonstrate the effectiveness of the technique by monitoring the dynamic response of a generic 2.5 kHz vibration applied to a PZT placed at the end of a sensing fiber comprised of a 1 km array of 200 UWFBGs each with a reflectivity of ~-43 dB written at a spacing of 5 m, with an SNR of ~34.52 dB.

Fiber-Optic Liquid Level Sensing by Temperature Profiling with an FBG Array.

We describe a fiber-optic system to measure the liquid level inside a container. The technique is based on the extraction of the temperature profile of the fiber by using a fiber Bragg grating (FBG) array. When the temperatures of the liquid and the gas are different, the liquid level can be estimated. We present a physical model of the system and the experimental results and we compare different algorithms to extract the liquid level from the temperature profile. We also show how air convection influences the temperature profile and the level of estimation accuracy. We finally show dynamic response measurements which are used to obtain the response time of the sensor. Turbomachinery monitoring is proposed as one possible application of the device.

Dynamic phase extraction in a modulated double-pulse ϕ-OTDR sensor using a stable homodyne demodulation in direct detection.

We propose and experimentally demonstrate a stable homodyne phase demodulation technique in a ϕ-OTDR using a double-pulse probe and a simple direct detection receiver. The technique uses selective phase modulation of one of a pair of pulses to generate a carrier for dynamic phase changes and involves an enhanced phase demodulation scheme suitable for distributed sensing by being robust against light intensity fluctuations, independent of the modulation depth, and convenient for analogue signal processing. The capability of the technique to quantify distributed dynamic phase change due to a generic external impact is experimentally demonstrated by measuring the phase change induced by a nonlinear actuator generating a 2 kHz perturbation at a distance of 1.5 km on a standard singlemode fiber with an SNR of ~24 dB. The demodulated nonlinear response is shown to have a spectrum consistent with one obtained using an FBG sensor and a commercial reading unit.

Hybrid distributed acoustic and temperature sensor using a commercial off-the-shelf DFB laser and direct detection.

We demonstrate a hybrid distributed acoustic and temperature sensor (DATS) using a commercial off-the-shelf (COTS) distributed feedback (DFB) laser, a single-mode optical fiber, and a common receiver block. We show that the spectral and frequency noise characteristics of the laser, combined with a suitable modulation scheme, ensure the inter-pulse incoherence and intra-pulse coherence conditions required for exploiting the fast denoising benefits of cyclic Simplex pulse coding in the hybrid measurement. The proposed technique enables simultaneous, distributed measurement of vibrations and temperature, with key industrial applications in structural health monitoring and industrial process control systems. The sensor is able to clearly identify a 500 Hz vibration at 5 km distance along a standard single-mode fiber and simultaneously measure the temperature profile along the same fiber with a temperature resolution of less than 0.5°C with 5 m spatial resolution.

Whispering gallery mode laser based on antitumor drug-dye complex gain medium.

Optofluidic lasers have emerged as a new research field over the past few years. Most frequently they use conventional dye molecules as the gain medium. In this Letter, we demonstrate a laser emission produced by the coupling of the evanescent whispering gallery modes that resonate in a cylindrical microresonator to a newly developed gain medium. This medium is formed by attachment of a 7-nitrobenzo [c] [1,2,5]-oxadiazol-4-yl fluorescent tag to tamoxifen, the most widely used drug in the treatment of breast cancer. The antitumor character of the gain medium paves the way to novel biophotonic applications.

Linear and nonlinear optical properties of carbon nanotube-coated single-mode optical fiber gratings.

Single-wall carbon nanotube deposition on the cladding of optical fibers has been carried out to fabricate an all-fiber nonlinear device. Two different nanotube deposition techniques were studied. The first consisted of repeatedly immersing the optical fiber into a nanotube supension, increasing the thickness of the coating in each step. The second deposition involved wrapping a thin film of nanotubes around the optical fiber. For both cases, interaction of transmitted light through the fiber core with the external coating was assisted by the cladding mode resonances of a tilted fiber Bragg grating. Ultrafast nonlinear effects of the nanotube-coated fiber were measured by means of a pump-probe pulses experiment.

Optical and structural features of silicon-rich hydrogenated amorphous silicon nitride thin films.

A systematic study of fabrication and effect of post-deposition processing on the optical and structural features of silicon-rich hydrogenated amorphous silicon nitride thin films deposited by Hg-sensitized Photo-Chemical Vapour Deposition technique is presented. Both deposition parameters and post-deposition thermal treatment resulted into substantial change in the refractive index associated with the densification of the film. Our studies reveal that the presence of hydrogen and its out-diffusion upon thermal treatment play a crucial role in the overall structural evolution, specially the stabilization of individual phases such as Si and Si3N4. We further report the room-temperature photoluminescence from as-deposited films, which is due to formation of silicon nanostructures in crystalline and amorphous forms. These studies are of great interest from the prospective of commercially viable Si-based technology.

Reduction of the amplified spontaneous emission threshold in semiconducting polymer waveguides on porous silica.

Hybrid organic-inorganic monomode waveguides of conjugated polymers on porous silicon (PS) substrates have been fabricated. Different low refractive index PS substrates, varying from 1.46 down to 1.18 have been studied. Amplified spontaneous emission (ASE) has been observed for all the samples and the ASE threshold has been monitored as a function of the PS refractive index. A decrease in the ASE threshold is detected when the PS refractive index decreases. These results have been analysed in the frame of a four level waveguide amplifier model and the theoretical predictions are in agreement with the experimental data.

Loosening the DNA wrapping around single-walled carbon nanotubes by increasing the strand length.

In this study, we discuss the influence of DNA strand length on DNA wrapping of single-walled carbon nanotubes under high-shear sonication and find that different strand length results in changed DNA-nanotube interaction, which is sensitively probed by the upshift extent of the Raman radial breathing mode bands of nanotubes due to DNA wrapping. The difference in the interaction between nanotubes and DNA strands of various length results in apparently different degrees of wrapping compactness, revealed by atomic force microscopy observations, and nanotube selectivity in wrapping, indicated by both Raman and photoluminescence spectroscopy results. The above findings can be utilized to precisely control the nanotube diameter distribution and modulate the physicochemical properties of the nanotube wrapped by DNA without any direct functionalization of nanotubes. This finding is of considerable interest from both theoretical and practical standpoints.

Porous silicon-based rugate filters.

We report an experimental study of porous silicon-based rugate filters. We performed filter apodization, following a half-apodization approach, which successfully attenuated the sidelobes at both sides of the photonic stop band. We achieved successful reduction of interference ripples through the insertion of index-matching layers on the first and last interfaces. An apodized dielectric mirror and a rugate filter are compared: Appreciable differences in the harmonic presence and stop-band performance were observed and are commented on. Bandwidth control when index contrast is modified is also demonstrated. Finally, the possibility of combining different rugate filter designs to attain more complex responses is demonstrated by the achievement of a multi-stop-band filter. Numerical calculations for design optimization and comparison with experimental data are reported too.

Zener tunneling of light waves in an optical superlattice.

We report on the observation of Zener tunneling of light waves in spectral and time-resolved transmission measurements, performed on an optical superlattice made of porous silicon. The structure was designed to have two photonic minibands, spaced by a narrow frequency gap. A gradient in the refractive index was introduced to create two optical Wannier-Stark ladders and, at a critical value of the optical gradient, tunneling between energy bands was observed in the form of an enhanced transmission peak and a characteristic time dependence of the transmission.

Light transport through the band-edge states of Fibonacci quasicrystals.

The propagation of light in nonperiodic quasicrystals is studied by ultrashort pulse interferometry. Samples consist of multilayer dielectric structures of the Fibonacci type and are realized from porous silicon. We observe mode beating and strong pulse stretching in the light transport through these systems, and a strongly suppressed group velocity for frequencies close to a Fibonacci band gap. A theoretical description based on transfer matrix theory allows us to interpret the results in terms of Fibonacci band-edge resonances.

Optical analogue of electronic Bloch oscillations.

We report on the observation of Bloch oscillations in light transport through periodic dielectric systems. By introducing a linear refractive index gradient along the propagation direction the optical equivalent of a Wannier-Stark ladder was obtained. Bloch oscillations were observed as time-resolved oscillations in transmission, in direct analogy to electronic Bloch oscillations in conducting crystals where the Wannier-Stark ladder is obtained via an external electric field. The observed oscillatory behavior is in excellent agreement with transfer matrix calculations.