Magic-Angle-Spinning NMR Magnet Development: Field Analysis and Prototypes.

We are currently working on a program to complete a 1.5 T/75 mm RT bore magic-angle-spinning nuclear magnetic resonance magnet. The magic-angle-spinning magnet comprises a z-axis 0.866-T solenoid and an x-axis 1.225-T dipole, each to be wound with NbTi wire and operated at 4.2 K in persistent mode. A combination of the fields creates a 1.5-T field pointed at 54.74 degrees (magic angle) from the rotation (z) axis. In the first year of this 3-year program, we have completed magnetic analysis and design of both coils. Also, using a winding machine of our own design and fabrication, we have wound several prototype dipole coils with NbTi wire. As part of this development, we have repeatedly made successful persistent NbTi-NbTi joints with this multifilamentary NbTi wire.

No-Insulation Coil Under Time-Varying Condition: Magnetic Coupling With External Coil.

This paper presents experimental and analytical studies on the time-varying behavior of an NI (no-insulation) high-temperature superconductor pancake coil, alone or magnetically coupled to an external coil. An NI coil and another insulated coil (as an external), both of identical winding i.d. and number of turns, were fabricated. Another external coil used in this study was a 300-mm/5-T low-temperature superconductor magnet. An equivalent circuit model is proposed to simulate the NI coil, and the external coil, under time-varying conditions. Good agreement between experiment and simulation shows that the proposed equivalent circuit model is valid to characterize the time-varying electromagnetic behavior of an NI coil, alone or magnetically coupled to an external coil.

Bulk and Plate Annulus Stacks for Compact NMR Magnets: Trapped Field Characteristics and Active Shimming Performance.

We have constructed two "annulus" magnets, YP2800 and YB10; each consists of 2800 YBCO thin square "plate annuli" (YP2800) and 10 YBCO thick "bulk annuli" (YB10). Their trapped field characteristics, spatial and temporal, were investigated and compared, experimentally and analytically. Two sets of field-cooling tests were performed at 77 K: (1) maximum trapped field tests, where a 2-T background field was applied to investigate the maximum trapped field capability of the two magnets; and (2) reduced trapped field tests, where spatial homogeneity improvement of the two magnets was investigated after field cooling with a reduced background field. Also, a Z1 copper shim coil was designed, constructed, and operated, alone and with YP2800 and YB10. When it was operated with the annulus magnets at 77 K, a significant attenuation of the shim coil strength was observed due to the screening currents induced within the annulus magnets.

Field performance of a prototype compact YBCO "annulus" magnet for micro-NMR spectroscopy.

A prototype compact annulus YBCO magnet (YP1070) for micro-NMR spectroscopy was constructed and tested at 77 K and 4.2 K. This paper, for the first time, presents comparison of the 77-K and 4.2-K test results of our annulus magnet. With a 26-mm cold bore, YP1070 was comprised of a stack of 1070 thin YBCO plates, 80-µm thick and either 40-mm or 46-mm square. After 1070 YBCO plates were stacked ''optimally'' in 214 groups of 5-plate modules, YP1070 was ''field-cooled'' at 77 K after being immersed in a bath of liquid nitrogen (LN2) with background fields of 0.3 and 1 T and also at 4.2 K in a bath of liquid helium (LHe) with background fields of 2.8 and 5 T. In each test, three key NMR magnet field-performance parameters-trapped field strength, spatial field homogeneity, and temporal stability-were measured. At 4.2 K, a maximum peak trapped field of 4.0 T, equivalent to 170 MHz 1H NMR frequency, was achieved with a field homogeneity, within a |z| < 2.5 mm axial space, of ~3000 ppm. YP1070 achieved its best field homogeneity of 182 ppm, though at a reduced trapped field of 2.75 T (117 MHz). The peak trapped fields at 4.2 K were generally ~10 times larger than those at 77 K, in direct proportion to ~10-fold enhancement in superconducting current-carrying capacity of YBCO from 77 to 4.2 K. Temporal stabilities of ~110 and ~17,500 ppm/h measured at 77 K, with trapped fields respectively of 0.3 and 1 T, show that temporal stability deteriorates with trapped field strength. Also, temporal enhancement of trapped fields at 4.2 K was observed and reported here for the first time.

No-Insulation (NI) HTS Inserts for > 1 GHz LTS/HTS NMR Magnets.

A no-insulation (NI) technique has been applied to wind and test a NI HTS (YBCO) double-pancake coil at 4.2 K. Having little detrimental effect on field-current relationship, the absence of turn-to-turn insulation enabled the test coil to survive a quench at a coil current density of 1.58 kA/mm2. The NI HTS coil is compact and self-protecting, two features suitable for large high-field magnets. To investigate beneficial impacts of the NI technique on >1 GHz LTS/HTS NMR magnets, we have designed six new NI HTS inserts for our ongoing 1.3 GHz LTS/HTS NMR magnet, which require less costly LTS background magnets than the original insulated HTS insert. A net result will be a significant reduction in the overall cost of an LTS/HTS NMR magnet, at 1.3 GHz and above.

MgB2 for MRI Magnets: Test Coils and Superconducting Joints Results.

Among key design and operation issues for MgB2 relevant to MRI magnets are: uniformity of current-carrying capacity over long lengths (>2 km) of wire; and reliability of a splicing technique. This paper presents experimental results of current-carrying capacities of a small test coil and joints, both made from MgB2 round wires, multifilament and monofilament (mono), manufactured by Hyper Tech Research, Inc. The test coils were wound with 95-m long unreacted, C (carbon)-doped MgB2 multifilament wire, sintered at 700°C for 90 min. The critical currents were measured in the 4.2 K-15 K and 0 T-5 T ranges. We have modified our original splicing technique, proven successful with unreacted, un-doped MgB2 multifilament wire sintered at 570°C, and applied it to splice both un-doped and C-doped mono wires sintered at 700°C. Most consistently good results were obtained using the un-doped mono wires. Also presented are results of a small joint-coil-PCS assembly of mono wire, operated in persistent mode at 50 A at >10 K.

On the 600 MHz HTS Insert for a 1.3 GHz NMR Magnet.

We update here on the status of one of the main components of a 1.3 GHz NMR magnet currently being developed at the MIT Francis Bitter Magnet Laboratory (FBML): the 600 MHz HTS insert coil. Started in 2000 as a 3-phase program and currently in its final phase (Phase 3A), the HTS insert will first be installed in the bore of a 500 MHz all LTS magnet, generating a field of 25.8 T (1.1 GHz). In Phase 3B, we will place the HTS insert in the bore of a 700 MHz LTS magnet, achieving our ultimate goal of completing a high-resolution 1.3 GHz magnet. The HTS insert, built as a stack of double pancakes (DP), consists of two concentric stack of coils, the inner coil wound with YBCO tape and the outer coil with Bi2223/Ag tape. The series-connected coils, immersed in a bath of liquid helium at atmospheric pressure, will be operated in driven mode. The paper describes detailed aspects of: 1) design and fabrication of both coils, 2) testing of individual DPs at 77 K to characterize the current carrying capabilities and magnetic performance of each DP coil, 3) techniques and elements utilized in the DP-to-DP splice procedure and, 4) splice dissipation.

A Stack of YBCO Annuli, Thin Plate and Bulk, for Micro-NMR Spectroscopy.

A new annulus magnet, the latest in a series of compact magnets being developed for NMR spectroscopy applications at the MIT Francis Bitter Magnet Laboratory, was built and tested in a bath of liquid nitrogen at 77 K. The magnet, YP2800, a stack of 2800 thin YBCO plate annuli, each either 40 - or 46-mm square and 0.08-mm thick with a 26-mm bore, is an upgraded version of the two earlier plate annulus magnets, YP750 (750 plates) and YP1070 (1070). This paper presents construction details and test results of YP2800. Its spatial field homogeneity and temporal stability were measured, analyzed, and compared with those of YP750 and YP1070. Also, four YBCO bulk annuli, each 26-mm i.d., 46-mm o.d., and 5.2-mm thick, were added to YP2800 and their impacts on field strength and homogeneity were investigated experimentally.

No-Insulation (NI) Winding Technique for Premature-Quench-Free NbTi MRI Magnets.

This paper describes and discusses a No-Insulation (NI) winding technique that, based on experiment results of two test NbTi coils, promises to significantly improve stability and ease protection of high performance magnets; if applied to those used in marketplace MRI magnets, it may eradicate premature quenches that still afflict these magnets, though much less frequently than in the past. The key idea is that a single turn in an NI winding can, upon a quench, share the copper stabilizers of neighboring turns through turn-to-turn contacts. To demonstrate the main features of the NI technique, two test coils (Φ30 mm) were wound with insulated (INS) and no-insulation (NI) NbTi wires, respectively. The results presented in this paper include: 1) charge-discharge test results and field analyses showing that the NI field performance is essentially identical to that of the INS coil except a charging delay; and 2) charging test results where coil voltages were measured during critical current tests to imply that the NI coil is charged more stably than its INS counterpart.

A 1.3-GHz LTS/HTS NMR Magnet-A Progress Report.

In this paper we present details of a 600 MHz HTS insert (H600) double pancake (DP) windings. It will first be operated in the bore of a 500 MHz LTS magnet, achieving a frequency of 1.1 GHz. Upon completion of H600, we will embark on the final phase (Phase 3B) of a 3-Phase program began in 2000: completion of a high resolution 1.3 GHz LTS/HTS magnet. In Phase 3B, the H600 will be coupled to a 700 MHz LTS magnet to achieve the ultimate frequency of 1.3 GHz. The HTS insert is composed of two concentric stacks of double pancakes, one wound with high strength BSCCO-2223 tape, the other with YBCO coated conductor. Details include conductor and coil parameters, winding procedure, DPs mechanical support and integration to the background 500 MHz LTS magnet. Test results of individual DPs in LN2 are also presented.

Field Performance of an Optimized Stack of YBCO Square "Annuli" for a Compact NMR Magnet.

The spatial field homogeneity and time stability of a trapped field generated by a stack of YBCO square plates with a center hole (square "annuli") was investigated. By optimizing stacking of magnetized square annuli, we aim to construct a compact NMR magnet. The stacked magnet consists of 750 thin YBCO plates, each 40-mm square and 80- µm thick with a 25-mm bore, and has a Ø10 mm room-temperature access for NMR measurement. To improve spatial field homogeneity of the 750-plate stack (YP750) a three-step optimization was performed: 1) statistical selection of best plates from supply plates; 2) field homogeneity measurement of multi-plate modules; and 3) optimal assembly of the modules to maximize field homogeneity. In this paper, we present analytical and experimental results of field homogeneity and temporal stability at 77 K, performed on YP750 and those of a hybrid stack, YPB750, in which two YBCO bulk annuli, each Ø46 mm and 16-mm thick with a 25-mm bore, are added to YP750, one at the top and the other at the bottom.

Active Protection of an MgB(2) Test Coil.

This paper presents results of a study, experimental and computational, of a detect-and-activate-the-heater protection technique applied to a magnesium diboride (MgB(2)) test coil operated in semi-persistent mode. The test coil with a winding ID of 25 cm and wound with ~500-m long reacted MgB(2) wire was operated at 4.2 K immersed in a bath of liquid helium. In this active technique, upon the initiation of a "hot spot" of a length ~10 cm, induced by a "quench heater," a "protection heater" (PH) of ~600-cm long planted within the test coil is activated. The normal zone created by the PH is large enough to absorb the test coil's entire initial stored energy and still keeps the peak temperature within the winding below ~260 K.

HTS Pancake Coils Without Turn-to-Turn Insulation.

This paper reports a study of HTS pancake coils without turn-to-turn insulation. Three no-insulation (NI) pancake coils were wound: each single and double pancake coil of Bi2223 conductor and one single pancake of ReBCO conductor. An equivalent electrical circuit for modeling NI coils was verified by two sets of test: 1) charge-discharge; and 2) sudden discharge. Also, an overcurrent test in which a current exceeding a coil's critical current by 2.3 times was performed, and analysed, to demonstrate that in terms of stability NI HTS coils outperform their counterparts. The new NI winding offers HTS coils enhanced performance in three key parameters: overall current density; thermal stability; and mechanical integrity.