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1.
J Adhes Dent ; 16(5): 435-40, 2014 Oct.
Article in English | MEDLINE | ID: mdl-25264549

ABSTRACT

PURPOSE: To compare manual and sonic adhesive application modes in terms of the permeability and microtensile bond strength of a self-etching adhesive applied in the one-step or two-step protocol. MATERIALS AND METHODS: Self-etching All Bond SE (Bisco) was applied as a one- or a two-step adhesive under manual or sonic vibration modes on flat occlusal dentin surfaces of 64 human molars. Half of the teeth were used to measure the hydraulic conductance of dentin at 200 cm H2O hydrostatic pressure for 5 min immediately after the adhesive application. In the other half, composite buildups (Opallis) were constructed incrementally to create resin-dentin sticks with a cross-sectional area of 0.8 mm² to be tested in tension (0.5 mm/min) immediately after restoration placement. Data were analyzed using a two-way ANOVA and Tukey's test (α = 0.05). RESULTS: The fluid conductance of dentin was significantly reduced by the sonic vibration mode for both adhesives, but no effect on the bond strength values was observed for either adhesive. CONCLUSION: The sonic application mode at an oscillating frequency of 170 Hz can reduce the fluid conductance of the one- and two-step All Bond SE adhesive when applied on dentin.


Subject(s)
Dental Bonding , Dentin Permeability/physiology , Dentin-Bonding Agents/chemistry , Dentin/ultrastructure , Sonication/methods , Acid Etching, Dental/methods , Composite Resins/chemistry , Dental Materials/chemistry , Dental Stress Analysis/instrumentation , Dentinal Fluid/physiology , Humans , Hydrostatic Pressure , Methacrylates/chemistry , Phosphoric Acids/chemistry , Sonication/instrumentation , Stress, Mechanical , Surface Properties , Tensile Strength , Time Factors , Vibration
2.
J Endod ; 40(8): 1201-5, 2014 Aug.
Article in English | MEDLINE | ID: mdl-25069933

ABSTRACT

INTRODUCTION: Luting posts inside the root canal is still a challenge because of the difficulty of bonding adhesive materials in the apical third of roots. This study evaluated the effect of the application mode of 3 simplified etch-and-rinse adhesives on the push-out bond strength (PBS), nanoleakage (NL), and in situ degree of conversion (DC) of fiber posts in the root canal. METHODS: The roots of human premolars were endodontically prepared and divided into 6 groups according to the combination of the main factors: adhesive (Ambar, FGM, Joinville, SC, Brazil; Adper Single Bond 2, 3MESPE, St Paul, MN; and XP Bond+self-cure activator, DeTrey Dentsply, Konstanz, Germany) and application mode (manual or sonic). The posts were cemented and the PBS tested at 0.5 mm/min. The NL was evaluated by scanning electron microscopy after the immersion of specimens in 50% silver nitrate. Micro-Raman spectroscopy was used to measure the in situ DC. Root third was also considered in the statistical evaluation. Data were analyzed by 3-way repeated measures analysis of variance and Tukey tests (5%). RESULTS: Under sonic application, the PBS and the in situ DC increased, whereas NL decreased significantly for all groups in the middle and apical thirds (P < .05). CONCLUSIONS: The application of simplified adhesives by sonic mode in the root canal is a feasible tool to increase the fiber post bond to root canals.


Subject(s)
Dental Bonding/methods , Dental Pulp Cavity/ultrastructure , Dentin-Bonding Agents/chemistry , Post and Core Technique/instrumentation , Resin Cements/chemistry , Sonication/methods , Bisphenol A-Glycidyl Methacrylate/chemistry , Cementation/methods , Dental Cements/chemistry , Dental Leakage/classification , Dental Stress Analysis/instrumentation , Humans , Materials Testing , Methacrylates/chemistry , Microscopy, Electron, Scanning , Polyethylene Glycols/chemistry , Polymerization , Polymethacrylic Acids/chemistry , Random Allocation , Root Canal Preparation/methods , Silver Staining/methods , Spectrum Analysis, Raman , Stress, Mechanical , Tooth Apex/ultrastructure , Tooth, Nonvital/pathology
3.
Oper Dent ; 33(1): 79-88, 2008.
Article in English | MEDLINE | ID: mdl-18335737

ABSTRACT

This study examined the early and long-term microtensile bond strengths (MTBS) and interfacial enamel gap formation (IGW) of two-step self-etch systems to unground and ground enamel. Resin composite (Filtek Z250) buildups were bonded to proximal enamel surfaces (unground, bur-cut or SiC-treated enamel) of third molars after the application of four self-etch adhesives: a mild (Clearfil SE Bond [SE]), two moderate (Optibond Solo Plus Self-Etch Primer [SO] and AdheSE [AD]) and a strong adhesive (Tyrian Self Priming Etchant + One Step Plus [TY]) and two etch-and-rinse adhesive systems (Single Bond [SB] and Scotchbond Multi-Purpose Plus [SBMP]). Ten tooth halves were assigned for each adhesive. After storage in water (24 hours/37 degrees C), the bonded specimens were sectioned into beams (0.9 mm2) and subjected to microTBS (0.5 mm/minute) or interfacial gap width measurement (stereomicroscope at 400x) either immediately (IM) or after 12 months (12M) of water storage. The data were analyzed by three-way repeated measures ANOVA and Tukey's test (alpha=0.05). No gap formation was observed in any experimental condition. The microTBS in the Si-C paper and diamond bur groups were similar and greater than the unground group only for the moderate self-etch systems (SO and AD). No reductions in bond strength values were observed after 12 months of water storage, regardless of the adhesive evaluated.


Subject(s)
Acid Etching, Dental/methods , Dental Bonding , Dental Marginal Adaptation , Resin Cements , Analysis of Variance , Dental Enamel , Dental Stress Analysis , Drug Storage , Humans , Molar , Statistics, Nonparametric , Surface Properties , Tensile Strength , Water
4.
J Dent ; 36(4): 249-55, 2008 Apr.
Article in English | MEDLINE | ID: mdl-18308450

ABSTRACT

OBJECTIVES: The aim of this study was to compare the fracture strength of three techniques used to re-attach tooth fragments in sound and endodontically treated fractured teeth with or without fiber post placement. MATERIAL AND METHODS: Ninety human lower incisors were randomly divided into three groups of 30 teeth each. In group A teeth were not subjected to endodontic treatment; while teeth from groups B and C were endodontically treated and the pulp chamber restored with a composite resin. All teeth were fractured by an axial load applied to the buccal area in order to obtain tooth fragments. Teeth from each group were then divided into three subgroups, according to the re-attachment technique: bonded-only, buccal-chamfer and circumferential chamfer. Before the re-attachment procedures, fiber posts were placed in teeth from group C using dual cure resin luting cement (Duo-Link). All teeth (groups A-C) had the fragments re-attached using a same dual cure resin luting cement. In the bonded-only group, no additional preparation was made. After re-attachment of the fragment, teeth from groups buccal and circumferential chamfer groups had a 1.0 mm depth chamfer placed in the fracture line either on buccal surface or along the buccal and lingual surfaces, respectively. Increments of microhybid composite resin (Tetric Ceram) were used in subgroups buccal chamfer and circumferential chamfer to restore the chamfer. The specimens were loaded until fracture in the same pre-determined area. The force required to detach each fragment was recorded and the data was subjected to a three-way analysis of variance where factors Group and Re-attachment technique are independent measures and Time of fracture is a repeated measure factor (first and second) and Tukey's test (alpha=0.05). RESULTS: The main factors Re-attachment technique (p=0.04) and Time of fracture (p=0.02) were statistically significant. The buccal and circumferential chamfer techniques were statistically similar (p>0.05) and superior to the bonded-only group (p<0.05). The first time of fracture was statistically superior to second time of fracture (p<0.001). CONCLUSIONS: The use of fiber post is not necessary for the reinforcement of the tooth structure in re-attachment of endodontically treated teeth. When bonding a fractured fragment, the buccal or circumferential re-attachment techniques should be preferable in comparison with the simple re-attachment without any additional preparation. None of the techniques used for re-attachment restored the fracture strength of the intact teeth.


Subject(s)
Dental Bonding/methods , Dental Restoration, Permanent/methods , Post and Core Technique , Tooth Crown/injuries , Tooth Fractures/therapy , Composite Resins , Dental Stress Analysis , Humans , Resin Cements , Tooth, Nonvital
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