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1.
Appl Radiat Isot ; 178: 109968, 2021 Dec.
Article in English | MEDLINE | ID: mdl-34619627

ABSTRACT

The paper summarizes measurements and the Monte Carlo simulations performed to adapt the high purity germanium (HPGe) detectors of the system to the particular tasks of the decommissioning site. The work carried out for the installation and adaptation in CIEMAT of the prototype 'SuperMum', developed in the framework of the European MetroDecom II project for segregation and declassification of materials is described. The activities related to the validation of the prototype for the specific needs of a real Waste Management Unit are presented. Monte Carlo models of the SuperMum have been developed at CIEMAT and CMI using different codes and adapted to the geometries used (big-bag containers with the material volume of up to 0.5 m3). Uncertainty budget reporting tailored for the possible deviations between Monte Carlo assumptions and real waste have been analyzed. Data for several filling levels and activity distributions have been measured with reference sources and a good agreement has been obtained with calculated values.

2.
Appl Radiat Isot ; 160: 109113, 2020 Jun.
Article in English | MEDLINE | ID: mdl-32174464

ABSTRACT

A defined-solid-angle proportional counter has been designed for the absolute determination of X-ray emission rates between 2 keV and 10 keV. The main features of the counter are described in this work, and spectra of two radionuclides with low-energy X-ray emissions are presented. The activity concentration of an 55Fe solution was determined by measuring the emission rate of three samples and using tabulated emission probabilities. This activity concentration is compared with the value obtained by liquid scintillation counting, and an excellent agreement has been found.

3.
Appl Radiat Isot ; 155: 108921, 2020 Jan.
Article in English | MEDLINE | ID: mdl-31629294

ABSTRACT

An internal consistency test of the calculation of coincidence-summing correction factors FC for volume sources is presented. The test is based on exact equations relating the values of FC calculated for three ideal measurement configurations. The test is applied to a number of 33 sets of FC values sent by 21 teams. Most sets passed the test, but not the results obtained using the quasi-point source approximation; in the latter case the test qualitatively indicated the magnitude of the bias of FC.

4.
Appl Radiat Isot ; 132: 72-78, 2018 Feb.
Article in English | MEDLINE | ID: mdl-29169063

ABSTRACT

Accurate measurements were performed of the photon emission probabilities following the α decay of 235U to 231Th. Sources of highly enriched 235U were characterised in terms of isotopic composition by mass spectrometry and their activities were standardised by means of alpha-particle counting at a low defined solid angle. The standardised sources were subsequently measured by high-resolution γ-ray spectrometry with calibrated high-purity germanium detectors to determine the photon emission probabilities. Four laboratories participated in this work and reported emission probabilities for 33 γ-ray lines. Most of them agree with previously published evaluated data. In addition, new values are proposed for γ-lines which have been measured only once in the past.

5.
Appl Radiat Isot ; 134: 421-425, 2018 Apr.
Article in English | MEDLINE | ID: mdl-29074291

ABSTRACT

The nuclide 89Zr is being tested for the labelling of compounds with long blood circulation times. It decays by beta plus emission (22.8%) and by electron capture (77.2%) to 89Y. Its half-life has been determined by following the decay rate with two measurement systems; an Ionisation Chamber and an HPGe detector. The combination of six results gives a value of T1/2 = 78.333 (38) h, slightly lower than the DDEP recommended value of 78.42 (13) h. This radionuclide has also been standardised by liquid scintillation counting, 4πγ counting and coincidence techniques.

7.
Appl Radiat Isot ; 109: 314-318, 2016 Mar.
Article in English | MEDLINE | ID: mdl-26701659

ABSTRACT

The half-life of the positron-emitter (44)Sc has been determined by following the decay rate with two measurement systems; an Ionisation Chamber and a HPGe detector. The combination of seven results gives a value of T1/2=4.042 (25)h, about 2% higher than the recommended value of T1/2=3.97 (4)h (Browne, 2011) and with a lower uncertainty. This radionuclide has also been standardised by coincidence counting, and liquid scintillation counting techniques. A (44)Ti/(44)Sc generator developed at CIEMAT was used to obtain the (44)Sc solutions used in all measurements.


Subject(s)
Half-Life , Radiation Dosimeters/standards , Radioisotopes/analysis , Radioisotopes/standards , Scandium/analysis , Scandium/standards , Calibration/standards , Equipment Design , Equipment Failure Analysis , Radiation Dosage , Reference Standards , Reproducibility of Results , Sensitivity and Specificity , Spain
8.
Appl Radiat Isot ; 94: 166-174, 2014 Dec.
Article in English | MEDLINE | ID: mdl-25213083

ABSTRACT

One of the issues of the European Research Project MetroMetal is to develop reference materials in order to provide SI-traceable radioactivity monitoring in foundries. For this purpose, a protocol for preparing a set of identical standard slag samples, containing known activity concentrations of (226)Ra, has been developed. This paper describes the preparation of the raw material, the characterisation in terms of its mineralogical, chemical and radiological features, the spiking procedure and the homogeneity testing of the spiked samples.

9.
Appl Radiat Isot ; 81: 255-60, 2013 Nov.
Article in English | MEDLINE | ID: mdl-23582494

ABSTRACT

In 2011 the joint research project Metrology for Radioactive Waste Management (MetroRWM)(1) of the European Metrology Research Programme (EMRP) started with a total duration of three years. Within this project, new metrological resources for the assessment of radioactive waste, including their calibration with new reference materials traceable to national standards will be developed. This paper gives a review on national, European and international strategies as basis for science-based metrological requirements in clearance and acceptance of radioactive waste.


Subject(s)
Guidelines as Topic , Radiation Protection/legislation & jurisprudence , Radiation Protection/standards , Radioactive Waste/legislation & jurisprudence , Radioactive Waste/prevention & control , Waste Management/legislation & jurisprudence , Waste Management/standards , Decontamination/legislation & jurisprudence , Decontamination/standards , Internationality
10.
Appl Radiat Isot ; 66(6-7): 764-8, 2008.
Article in English | MEDLINE | ID: mdl-18359236

ABSTRACT

In an intercomparison exercise, the Monte Carlo codes most commonly used in gamma-ray spectrometry today were compared with each other in order to gauge the differences between them in terms of typical applications. No reference was made to experimental data; instead, the aim was to confront the codes with each other, as they were applied to the calculation of full-energy-peak and total efficiencies. Surprising differences between the results of different codes were revealed.

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