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1.
Materials (Basel) ; 16(12)2023 Jun 13.
Article in English | MEDLINE | ID: mdl-37374549

ABSTRACT

This study presents a comprehensive analysis of different coating materials on the POM substrate. Specifically, it investigated physical vapour deposition (PVD) coatings of aluminium (Al), chromium (Cr), and chromium nitride (CrN) of three various thicknesses. The deposition of Al was accomplished through a three-step process, particularly plasma activation, metallisation of Al by magnetron sputtering, and plasma polymerisation. The deposition of Cr was attained using the magnetron sputtering technique in a single step. For the deposition of CrN, a two-step process was employed. The first step involved the metallisation of Cr using magnetron sputtering, while the second step involved the vapour deposition of CrN, obtained through the reactive metallisation of Cr and nitrogen using magnetron sputtering. The focus of the research was to conduct comprehensive indentation tests to obtain the surface hardness of the analysed multilayer coatings, SEM analyses to examine surface morphology, and thorough adhesion analyses between the POM substrate and the appropriate PVD coating.

2.
Polymers (Basel) ; 15(3)2023 Feb 03.
Article in English | MEDLINE | ID: mdl-36772081

ABSTRACT

A comprehensive experimental investigation of the noise evaluation of coated spur polymer gears made of POM was performed in this study. The three Physical Vapour Deposition (PVD) coatings investigated were aluminium (Al), chromium (Cr), and chromium nitrite (CrN). The gears were tested on an in-house-developed testing machine under a torque of 20 Nm and at a rotational speed of 1000 rpm. The noise measurements were performed with the tested gear pair on the testing device with a sound-proof acoustic foam used for the acoustic sound-proof insulation. The sound signal was analysed in time, frequency, and time-frequency domains and typical phenomena were identified in the signal. Experimental results showed that the noise level was higher for polymer gears with different coatings if compared to the polymer gears without coatings. With sound analysis in the time-frequency domain, precise degradation of the coatings could be noticed. In future studies, it would be appropriate to use a new method for signal analysis, e.g., high-order statistics and hybrid technique.

3.
Polymers (Basel) ; 14(21)2022 Nov 05.
Article in English | MEDLINE | ID: mdl-36365742

ABSTRACT

A comprehensive experimental investigation of the wear behaviour of coated spur polymer gears made of POM is performed in this study. Three different thicknesses of aluminium (Al) coatings were investigated and deposited by the Physical Vapour Deposition (PVD) process. The Al coating was deposited in three steps: By plasma activation, metallisation of the aluminium by the magnetron sputtering process, and plasma polymerisation. The wear of the gears was tested on an in-house developed testing rig for different torques (16, 20, and 24 Nm) and a rotational speed of 1000 rpm. The duration of the experiments was set to 13 h, when the tooth thickness and, consequently, the wear of the tooth flank were recorded. The experimental results showed that the influence of metallisation with aluminium surface coatings on the wear behaviour of the analysed polymer gear is not significantly important. The results also showed that the gears with a thicker aluminium coating showed greater wear than gears with a thinner coating or even without a coating. This is probably due to the fact that the aluminium particles that started to deviate during gear operation represented the abrasive material, which led to the faster wear of the contacting surfaces of the meshing gear flanks.

4.
Polymers (Basel) ; 13(20)2021 Oct 18.
Article in English | MEDLINE | ID: mdl-34685347

ABSTRACT

A comprehensive experimental investigation of the wear behaviour of coated spur polymer gears made of POM is performed in this study. The three physical vapour deposition (PVD) coatings investigated were aluminium (Al), chromium (Cr), and chromium nitrite (CrN). Al was deposited in three process steps: By plasma activation, metallisation of Al by the magnetron sputtering process, and by plasma polymerisation. Cr deposition was performed in only one step, namely, the metallization of Cr by the magnetron sputtering process. The deposition of CrN was carried out in two steps: the first involved the metallization of Cr by the magnetron sputtering process while the second step, vapour deposition, involved the reactive metallisation of Cr with nitrogen, also by the magnetron sputtering process. The gears were tested on an in-house developed testing rig for different torques (16, 20, 24 and 30 Nm) and rotational speed of 1000 rpm. The duration of the experiments was set to 13 h, when the tooth thickness, and, consequently, the wear of the tooth flank was recorded. The experimental results showed that the influence of metallisation with aluminium, chromium, and chromium nitrite surface coatings on the wear behaviour of the analysed polymer gear is not significant. This is probably due to the fact that the analysed coatings were, in all cases, very thin (less than 500 nm), and therefore did not influence the wear resistance significantly. In that respect, an additional testing using thicker coatings should be applied in the further research work.

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