ABSTRACT
OBJECTIVES: The aim of this study was to investigate the role of deep cryogenic treatment (DCT) on the cyclic fatigue resistance and cutting efficiency of martensitic shape memory (SM) nickel-titanium (NiTi) rotary endodontic instruments. MATERIALS AND METHODS: Seventy-five HyFlex(®) CM instruments were randomly divided into three groups of 25 each and subjected to different DCT (-185° C) conditions based on soaking time: DCT 24 group: 24 h, DCT 6 group: 6 h, and control group. Each group was randomly subdivided for evaluation of cyclic fatigue resistance in custom-made artificial canals (n = 15) and cutting efficiency in plexiglass simulators (n = 10). The cyclic fatigue resistance was measured by calculating the number of cycles to failure (NCF) and cutting efficiency was measured using the loss of weight method. RESULTS: Increase in NCF of instruments in DCT 24 group was highly significant (P < 0.01; Tukey's honest significant difference). There was no difference in weight loss of plexiglass simulators in all the groups (P > 0.05; one-way analysis of variance). In conclusion, deep dry cryogenic treatment with 24 h soaking time significantly increases the cyclic fatigue resistance without affecting the cutting efficiency of SM NiTi endodontic instruments. MATERIALS AND METHODS: Seventy-five HyFlex(®) CM instruments were randomly divided into three groups of 25 each and subjected to different DCT (-185° C) conditions based on soaking time: DCT 24 group: 24 h, DCT 6 group: 6 h, and control group. Each group was randomly subdivided for evaluation of cyclic fatigue resistance in custom-made artificial canals (n = 15) and cutting efficiency in plexiglass simulators (n = 10). The cyclic fatigue resistance was measured by calculating the number of cycles to failure (NCF) and cutting efficiency was measured using the loss of weight method. RESULTS: Increase in NCF of instruments in DCT 24 group was highly significant (P < 0.01; Tukey's honest significant difference). There was no difference in weight loss of plexiglass simulators in all the groups (P > 0.05; one-way analysis of variance). In conclusion, deep dry cryogenic treatment with 24 h soaking time significantly increases the cyclic fatigue resistance without affecting the cutting efficiency of SM NiTi endodontic instruments.
ABSTRACT
CONTEXT: Recent introduction of shape memory (SM) nickel-titanium (NiTi) alloy into endodontics is a major breakthrough. Although the flexibility of these instruments was enhanced, fracture of rotary endodontic instruments during instrumentation is an important challenge for the operator. Implementation of supplementary manufacturing methods that would improve the fatigue life of the instrument is desirable. AIM: The purpose of this study was to investigate the role of dry cryogenic treatment (CT) conditions on the microstructure of martensitic SM NiTi alloy. MATERIALS AND METHODS: Experiments were conducted on Ni-51 wt% Ti-49 wt% SM alloy. Five cylindrical specimens and five sheet specimens were subjected to different CT conditions: Deep CT (DCT) 24 group: -185°C; 24 h, DCT 6 group: -185°C; 6 h, shallow CT (SCT) 24 group: -80°C, 24 h, SCT 6 group: -80°C, 6 h and control group. Microstructure of surface was observed on cylindrical specimens with an optical microscope and scanning electron microscope at different magnifications. Subsurface structure was analyzed on sheet specimens using X-ray diffraction (XRD). RESULTS: Microstructures of all SM NiTi specimens had equiaxed grains (approximately 25 µm) with well-defined boundaries and precipitates. XRD patterns of cryogenically treated specimens revealed accentuation of austenite and martensite peaks. The volume of martensite and its crystallite size was relatively more in DCT 24 specimen. CONCLUSIONS: DCT with 24 h soaking period increases the martensite content of the SM NiTi alloy without altering the grain size.
ABSTRACT
OBJECTIVES: The aim of this study is to investigate the role of dry cryogenic treatment (CT) temperature and time on the Vickers hardness and wear resistance of new martensitic shape memory (SM) nickel-titanium (NiTi) alloy. The null hypothesis tested was that there is no difference in Vickers hardness and wear resistance between SM NiTi alloys following CT under two soaking temperatures and times. MATERIALS AND METHODS: The composition and the phase transformation behavior of the alloy were examined by X-ray energy dispersive spectroscopy and differential scanning calorimetry, respectively. Fifteen cylindrical specimens and 50 sheet specimens were subjected to different CT conditions: Deep cryogenic treatment (DCT) 24 group: -185°C, 24 h; DCT six group: -185°C, 6 h; shallow cryogenic treatment (SCT) 24 group: -80°C, 24 h; SCT six group: -80°C, 6 h; and control group. Wear resistance was assessed from weight loss before and after reciprocatory wet sliding wear. RESULTS: The as-received SM NiTi alloy contained 50.8 wt% nickel and possessed austenite finish temperature (Af) of 45.76°C. Reduction in Vickers hardness of specimens in DCT 24 group was highly significant (P < 0.01; Tukey's honest significant difference [HSD]). The weight loss was significantly higher in DCT 24 group (P < 0.05; Tukey's HSD). CONCLUSION: Deep dry CT with 24 h soaking period significantly reduces the hardness and wear resistance of SM NiTi alloy.
