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1.
ACS Omega ; 8(38): 34698-34709, 2023 Sep 26.
Article in English | MEDLINE | ID: mdl-37780025

ABSTRACT

The paper analyzes the dynamic behavior during the preparation of cemented backfill slurry by combining the structural performance analysis of the double-shaft mixer and the Euler multiphase flow field computational fluid dynamics model. Considering the interaction between phases and gas phase disturbances, the transient kinetic parameters and the interaction between gas and liquid phases were introduced. According to the modified lift model, the user-defined function of the net lateral lift coefficient and the turbulence energy equation was adjusted. Taking the parameters of flow field velocity, gas phase mixing, uniformity, and turbulent energy dissipation as the evaluation indexes of the mixing effect, the double-shaft mixer at a rotation velocity of 45 rpm and with a blade installation angle of 25° is the optimal design in this study. Experimental tests were carried out and confirmed that the refined two-fluid model of interphase interaction can provide a basis for the performance evaluation of material mixing equipment.

2.
Materials (Basel) ; 16(13)2023 Jul 01.
Article in English | MEDLINE | ID: mdl-37445087

ABSTRACT

Nuclear magnetic resonance can only quantitatively obtain porosity and pore size distribution, but as a conventional microstructure observation technology, scanning electron microscope (SEM) can select different magnifications to observe the microstructure of backfill materials. However, the processing of SEM images is not deep enough. In this paper, Image-Pro Plus 6.0 software was used to extract the data from SEM images, and the parameters of the area, and the perimeter, aspect ratio and roundness of the pores in the SEM images were obtained. The fractal characteristics of the pores in the SEM image were obtained by using the slit island method fractal theory. The concretization and quantification analysis of the pores' complexity were achieved. A functional relationship model for the strength and pore parameters was constructed; thus, the influence law of pore characteristics on strength was quantitatively analyzed. The conclusions included: (1) Pore parameters indicate that most pores in backfill are irregular, and only a few pores are regular-however, the whole structure has good fractal characteristics (R2 > 0.96). (2) The fractal dimension of pores is directly proportional to the roundness, the aspect ratio, and the pore content of pores-which indicates that the complexity of pores is related to both pore shape and pore content. (3) The strength had a linear inverse relationship with the roundness, aspect ratio, pore content, and fractal dimension-which indicates that all characteristics of pores have a certain influence on the strength.

3.
R Soc Open Sci ; 6(6): 190389, 2019 Jun.
Article in English | MEDLINE | ID: mdl-31312499

ABSTRACT

The characteristics of the porous structure of backfill are directly related to the macro parameters of the flowability of the filling slurry and the mechanical features of the backfill, which are fundamental to the study of multiscale mechanics of backfill. Based on the geometry and fractal theory, scanning electron microscopy images of backfill were analysed by image analysis methods such as OTSU and box counting. The fractal dimension of the pore structure was calculated. By quantitatively characterizing the pore structure, the trans-scale relationships between the fractal dimension of the pore structure and the macro parameters of the filling slurry were established in terms of equilibrium shear stress (ESS) and equilibrium apparent viscosity (EAV). In addition, the correlations between the fractal dimension and macro parameters of backfill were obtained in terms of uniaxial compressive strength (UCS), water content (WC) and porosity. The influence of the microstructure on the macro parameters was discussed. The results show the following: (i) the fractal dimension of the backfill pore structure can characterize the complexity of the structure; (ii) the fractal dimension of the pore structure is negatively correlated with the ESS and EAV of the filling slurry. The UCS of the backfill is positively correlated with the flowability parameter; (iii) the fractal dimension of the pore structure has a certain correlation with some macro parameters of the backfill, i.e. the fractal dimension is negatively correlated with the UCS and positively correlated with the WC and (iv) the linear correlations between the pore fractal dimension and UCS and WC are established. The correlation coefficient between the fractal dimension and UCS has an R 2 value of -0.638, while the corresponding value of the fractal dimension and WC is 0.604. UCS and WC can be predicted by the fractal dimension of pores.

4.
R Soc Open Sci ; 6(12): 191227, 2019 Dec.
Article in English | MEDLINE | ID: mdl-31903208

ABSTRACT

Under different exploitive conditions, the humidity levels of the backfill stopes are not the same. Humidity greatly affects the strength and microscopic characterization of the backfill. Cemented paste backfill (CPB) specimens were cured using 0, 30, 70% and standard curing (20°C, 99%) under four different humidity conditions. At 28 days, nuclear magnetic resonance (NMR) and scanning electron microscopy (SEM) techniques were used to obtain the microscopic features of the CPB specimens. The relationships between the permeability and uniaxial compressive strength (UCS) of the CPB specimens, and the microscopic characteristics of the CPB specimens, were established. The results showed the following: (i) The permeability of the CPB had an exponential functional relationship with its stone powder content. (ii) The stone powder content of CPB and the peak area of the T 2 spectrum are negatively correlated with the UCS. However, there was a T 2 peak area corresponding to the worst UCS with the same stone powder content. (iii) The peak area of the T 2 spectrum showed that the proportion of area of a small pore size was more than 80%, indicating that the pore size was mainly small. The pore diameter of small pores was linearly and inversely proportional to the UCS of the specimens. It can be found that the factors affecting the strength characteristics of CPB include not only the stone powder content, but also the curing conditions of different humidity.

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