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1.
J Food Prot ; 83(5): 754-761, 2020 May 01.
Article in English | MEDLINE | ID: mdl-32294761

ABSTRACT

ABSTRACT: Two different potato chip coatings-aqueous extracts including Zataria multiflora and Allium hirtifolium at concentrations of 1, 3, 5, and 7% and hydrocolloids individually or in combination-were used to decrease acrylamide content, and their effects on the characteristics of the product were then investigated. According to the results, the incorporation of hydrocolloids as the coating was more efficient in the reduction of acrylamide production than with the extracts. Also, the application of each extract and hydrocolloids individually can be considered a more efficient technique for acrylamide reduction than their mixture. In this regard, the economic aspects of the application of hydrocolloids in the coating of fried potato crisps can be evaluated.


Subject(s)
Acrylamide , Food Contamination/prevention & control , Solanum tuberosum , Acrylamide/analysis , Colloids , Food Handling , Solanum tuberosum/chemistry
2.
J Sep Sci ; 37(18): 2559-65, 2014 Sep.
Article in English | MEDLINE | ID: mdl-24958392

ABSTRACT

In this work, multiwalled carbon nanotubes were reacted with N-[3-(triet-hoxysilyl)propyl]isonicotinamide to prepare pyridine-functionalized carbon nanotubes. This novel sorbent was characterized by infrared spectroscopy, thermal and elemental analysis, and scanning electron microscopy. Functionalized carbon nanotubes were applied for the preconcentration and determination of copper ions using flame atomic absorption spectrometry. Various parameters such as sample pH, flow rate, eluent type and concentration, and its volume were optimized. Under optimal experimental conditions, the limit of detection, the relative standard deviation, and the recovery of the method were 0.65 ng/mL, 3.2% and 99.4%, respectively. After validating the method using standard reference materials, the new sorbent was applied for the extraction and determination of trace copper(II) ions in fruit samples.


Subject(s)
Copper/analysis , Fruit/chemistry , Nanotubes, Carbon/chemistry , Adsorption , Ions/analysis , Particle Size , Spectrophotometry, Atomic , Surface Properties
3.
Article in English | MEDLINE | ID: mdl-24827373

ABSTRACT

This paper describes a novel sorbent based on 4-(2-pyridylazo) resorcinol functionalised magnetic nanoparticles and its application for the extraction and pre-concentration of trace amounts of Cu(II) and Pb(II) ions. The nanosorbent was characterised by Fourier transform infrared spectroscopy, X-ray powder diffraction, thermal analysis, elemental analysis and scanning electron microscopy. The effects of various parameters such as pH, sorption time, sorbent dosage, elution time, volume and concentration of eluent were investigated. Following the sorption and elution of analytes, Cu(II) and Pb(II) ions were quantified by flame atomic absorption spectrometry. The limits of detection were 0.07 and 0.7 µg l(-1) for Cu(II) and Pb(II), respectively. The relative standard deviations of the method were less than 7%. The sorption capacity of this new sorbent were 92 and 78 mg g(-1) for Cu(II) and Pb(II), respectively. Finally this nanosorbent was applied to the rapid extraction of trace quantities of Cu(II) and Pb(II) ions in different real samples and satisfactory results were obtained.


Subject(s)
Copper/analysis , Food Contamination/analysis , Lead/analysis , Water Pollutants, Chemical/analysis , Adsorption , Cations, Divalent/analysis , Humans , Limit of Detection , Magnetite Nanoparticles/chemistry , Magnetite Nanoparticles/ultrastructure , Microscopy, Electron, Scanning , Resorcinols , Solid Phase Extraction , Spectrophotometry, Atomic , Spectroscopy, Fourier Transform Infrared , Water Pollution, Chemical/analysis , X-Ray Diffraction
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