ABSTRACT
BACKGROUND: The present study was aimed to evaluate the effect of pre-heating of bulk -fill resin composites on monomer elution from them. MATERIAL AND METHODS: Three different types of resin composites were used including Tetric N-Ceram Bulk Fill, X-tra Fill and X-tra Base. 10 cylindrical samples were prepared from each resin composites. Before light curing, 5 samples were pre-heated until reaching 68ËC, then 5 other samples were polymerized at room temperature. After 24 hours, release of UDMA, TEGDMA and BIS-GMA monomers were measured by High-Performance Liquid Chromatography analysis. Data analysis was performed by two-way ANOVA test, Games-Howell and Sidak post hoc tests. RESULTS: Pre-heating did not have any statistically significant effect on the mean values of UDMA, TEGDMA and Bis-GMA elution (p>0.05). The greatest amount of released Bis-GMA and UDMA was obtained from Tetric N-Ceram Bulk-fill composite. The greatest amount of released TEGDMA was obtained from X-tra Fill composite. X-tra Base composite showed the lowest amount of monomer release (P<0.001). CONCLUSIONS: Pre-heating did not have any effect on monomer release from bulk-fill resin composites. Moreover, the amount and the type of monomers released from various bulk-fill resin composites were not similar. Key words:Bulk fill composite resin, elution, HPLC, residual monomer, temperature.
ABSTRACT
Background. Due to the effect of pre-heating on the degree of conversion of composite resins and the possible effect on cytotoxicity, the effect of pre-heating of bulk-fill composite resins was investigated on cytotoxicity in this study. Methods. In this study, three different types of composite resin were used, including Tetric N-Ceram Bulk-Fil, Xtrafil, and Xtrabase. From each composite resin, 10 cylindrical samples (5 mm in diameter and 4 mm in height) were prepared, with five samples preheated to 68°C, and the other five samples polymerized at room temperature (25°C). Twenty-four hours after polymerization, cytotoxicity was assessed by MTT assay on human fibroblasts. Statistical analysis of data was carried out with two-way ANOVA and Sidak Post-Hoc. The significance level of the test was determined at 0.05. Results. There was no statistically significant difference between the mean percentage of cytotoxicity in terms of pre-heating (P>0.05), but the cytotoxicity of the studied composite resins was significantly different (P<0.001). The cytotoxicity of Tetric N-Ceram Bulk-fil composite resin was higher than that of the two other composite resins. Conclusion. Pre-heating of bulk-fill composite resin did not affect their cytotoxicity. In addition, the cytotoxicity of different bulk-fill composite resins was not the same.
ABSTRACT
Introduction: Relining fiber posts using composite resins helps the posts adapt to the anatomical space of the root canals. The aim of this study was to evaluate the effect of composite resin type on the push-out bond strength of anatomical fiber posts to intra canal dentin. Methods and Materials: Forty-eight bovine upper incisors were prepared for post space after root canal therapy and randomly divided in to six groups. Five different types of composite resin (GrandioSO, GrandioSO Heavy Flow, X-tra Fil, X-tra base and everX Posterior) were used for relining the prepared fiber posts. In the control group, the prepared post was cemented into the post space without relining. Cervical, middle and apical cross-sections were achieved from each root and push-out test was conducted at a crosshead speed of 0.5 mm/min. One sample from each group was scanned using a micro-CT scanner which provided views from the apical, middle and coronal thirds. Data were analyzed using Kolmogorov-Smirnov test, repeated measures ANOVA and post hoc tests using SPSS 17 (P<0.05). Results: Statistical analysis showed significant differences in terms of mean push-out bond strengths between different composite resin types and cross-sections (P<0.001). The mean push-out bond strength of the samples relined with Grandio SO composite resin (15.48±2.32) and X-tra Fil Bulk-fill composite resin (14.09±1.98) were significantly higher than that of other groups (P<0.05). The unrelined group had a mean push-out bond strength (5.94±1.45) which was significantly lower than that in other groups (P<0.05). In addition, there was a relationship between cross-sections and composite resin types (P<0.05). Conclusion: This in vitro study showed that the composite resins used for relining can affect the push-out bond strength to intra canal dentin based on their physical and mechanical properties.
ABSTRACT
INTRODUCTION: The aim of the present experimental study was to evaluate the push-out bond strength of Dorifill, Epiphany and MTA-Fillapex sealers to root canal dentin in presence and absence of smear layer (SL). METHODS AND MATERIALS: Sixty human single-rooted teeth were selected and divided into six groups (n=10). The canal irrigation protocol in groups 1, 3 and 5 consisted of 2.5% NaOCl during instrumentation and normal saline at the end of preparation plus a 5-min irrigation with 17% ethylenediaminetetraacetic acid (EDTA). In the remaining groups, normal saline was used for canal irrigation. The root canals were filled with Epiphany/Resilon (groups 1 and 2), Dorifill/gutta-percha (groups 3 and 4) and MTA-Fillapex/gutta-percha (groups 5 and 6). After two weeks of storage in 95% relative humidity at 37(º)C, 2 mm-thick dentin disks were prepared from coronal third of each root. The push-out bond strength test was carried out using a universal testing machine. Data were analyzed with the two-way ANOVA and post hoc Tukey's tests. Statistical significance was defined at 0.05. RESULTS: The highest (3.06±0.38 MPa) and lowest (1.16±0.32 MPa) push-out bond strength values were recorded in Epiphany/Resilon-NaOCl/EDTA and Dorifill/gutta-percha/normal saline groups, respectively. There were significant differences in the bond strength of sealers (P<0.05). In addition, elimination of the SL significantly increased the bond strength of all sealers (P<0.05). CONCLUSION: The Epiphany/Resilon group exhibited the highest push-out bond strength in the presence and absence of the SL. Elimination of the SL resulted in a significant increase in the bond strength of all the sealers to dentin.
