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Two new 15-deoxycimigenol-type and three new 24-epi-cimigenol-type glycosides from Cimicifuga Rhizome.
Yoshimitsu, Hitoshi; Nishida, Makiko; Sakaguchi, Masahide; Nohara, Toshihiro.
Chem Pharm Bull (Tokyo) ; 54(9): 1322-5, 2006 Sep.
Article in English | MEDLINE | ID: mdl-16946545

ABSTRACT

Two new 15-deoxycimigenol-type (1, 2) and three new 24-epi-cimigenol-type glycosides (3-5) were isolated from Cimicifuga Rhizome, and the structures were elucidated on the basis of spectroscopic data including 2D NMR spectra and chemical evidence. The two new 15-deoxycimigenol-type glycosides were the first cimigenol-type glycosides lacking a hydroxyl group at C-15.


Subject(s)
Cimicifuga/chemistry , Glycosides/chemistry , Glycosides/isolation & purification , Magnetic Resonance Spectroscopy/methods , Magnetic Resonance Spectroscopy/standards , Molecular Conformation , Reference Standards , Sensitivity and Specificity , Stereoisomerism
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