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1.
Materials (Basel) ; 15(9)2022 Apr 19.
Article in English | MEDLINE | ID: mdl-35591305

ABSTRACT

Self-healing materials have the potential to create a paradigm shift in the life cycle design of engineered structures, by changing the relation between material damage and structural failure, affecting structures' lifetime, safety, and reliability. However, the knowledge of self-healing capabilities in metallic materials is still in its infancy compared to other material systems because of challenges in the synthesis of organized and complex structures. This paper presents a study of a metal matrix composite system that was synthesized with an off-eutectic Tin (Sn)-Bismuth (Bi) alloy matrix, reinforced with Nickel-Titanium (NiTi) shape memory alloy (SMA) wires. The ability to close cracks, recover bulk geometry, and regenerate strength upon the application of heat was investigated. NiTi wires were etched and coated in flux before being incorporated into the matrix to prevent disbonding with the matrix. Samples were subjected to large deformations in a three-point bending setup. Subsequent thermo-mechanical testing of the composites confirmed the materials' ability to restore their geometry and recover strength, without using any consumable components. Self-healing was accomplished through a combination of activation of the shape memory effect in the NiTi to recover the samples' original macroscopic geometry, closing cracks, and melting of the eutectic material in the matrix alloy, which resealed the cracks. Subsequent testing indicated a 92% strength recovery.

2.
Sensors (Basel) ; 21(13)2021 Jun 28.
Article in English | MEDLINE | ID: mdl-34203284

ABSTRACT

The use of high-frequency strain waves to perform examinations and note measurements is referred to as ultrasonic testing (UT). UT is commonly used for the detection or evaluation of flaws and characterization of materials, among other applications. A standard ultrasonic inspection system comprises a pulser/receiver, transducer, and display devices. The pulser/receiver produces electrical pulses of high voltage. The transducer generates high-frequency ultrasonic energy after being driven by the pulser. The reflected wave is then converted into an electrical signal by the transducer and is displayed on a screen. The reflected signal strength versus the time plot helps to glean information regarding the features of a defect. In this paper, we discuss the experiments performed in a laboratory setting to determine ultrasound-based biofilm sensor sensitivity in relation to changes in the surrounding environment of temperature, concentration, turbidity, and conductivity of the liquid passing through the system. The effect of the change in frequency of the sensors was also studied. The sensors being developed are small and compact, portable, can be placed on the outer walls of the desired surface, use digital signal processing techniques, and the biofilm presence on the inner walls of the surface can be monitored.


Subject(s)
Water Pipe Smoking , Biofilms , Signal Processing, Computer-Assisted , Transducers , Ultrasonography
3.
Sci Rep ; 9(1): 19805, 2019 12 24.
Article in English | MEDLINE | ID: mdl-31874957

ABSTRACT

The adhesion strength of thin films is critical to the durability of micro and nanofabricated devices. However, current testing methods are imprecise and do not produce quantitative results necessary for design specifications. The most common testing methods involve the manual application and removal of unspecified tape. This overcome many of the challenges of connecting to thin films to test their adhesion properties but different tapes, variation in manual application, and poorly controlled removal of tape can result in wide variation in resultant forces. Furthermore, the most common tests result in a qualitative ranking of film survival, not a measurement with scientific units. This paper presents a study into application and peeling parameters that can cause variation in the peeling force generated by tapes. The results of this study were then used to design a test methodology that would control the key parameters and produced repeatable quantitative measurements. Testing using the resulting method showed significant improvement over more standard methods, producing measured results with reduced variation. The new method was tested on peeling a layer of paint from a PTFE backing and was found to be sensitive enough to register variation in force due to differing peeling mechanisms within a single test.

4.
Sensors (Basel) ; 18(11)2018 Nov 11.
Article in English | MEDLINE | ID: mdl-30423892

ABSTRACT

Ultrasonic systems employing embedded piezoelectric transducers have seen increased interest in recent years. The ability to sense, actuate, and analyze the wave propagation modes in engineering structures has been fundamental to the advancement of ultrasonic structural health monitoring (SHM). This paper presents a study into the sensing and actuation properties of shear-mode (d35) piezoelectric transducers made of lead zirconate titanate (PZT) that are internally embedded in the bondline of laminate structures. The manuscript presents analytical analysis, finite element simulation, and experimental validation building from an individual piezoelectric element to a full laminate structure. The validated model was then used to perform a parametric study into the effects of d35 PZT transducer size on the strength of actuation and sensing output signal. The selectivity of d35 PZT sensors was also investigated by generating multiple wave modes in the laminate structure and inspecting the output signals. The d35 PZT sensors were found to selectively detect only certain modes of the wave propagation providing a fundamental hardware filter that could be employed to simplify signal analysis and processing. The results of this study indicate that d35 PZTs embedded in the bondline have multiple properties that can potentially be employed for ultrasonic SHM.

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