Development and validation of a siphoning prototype for surface runoff evaluation.

The degradation of soil and water quality encourages research to assess the effects of rainfall on the losses of soil and chemical elements that result from surface runoff. In seasons of high surface runoff, the collectors must support the total volume drained or allow its correct estimation to avoid misinterpretation of the data. The present investigation aimed to develop and validate a compact and low-cost system to quantify surface runoff, sediments, and chemical elements losses using the bucket-siphon sampler system (BS3) siphoning method. The tests performed within the system used the runoff collected in a Nitisol or solutions constructed at the laboratory through mixing soil (i.e., Nitisol or Cambisol) with tap water. The BS3 method was efficient in estimating the total volume of water runoff and the concentration of sediments and P in the surface runoff. The maximum flow rate supported by the BS3 method, as presented here, is 0.035 L s-1 , which considering a 10-m² plot is equivalent to 12.6 mm h-1 . Due to the craft characteristics of the system, we recommend the calibration of each unit built to obtain a precise ratio between the volume stored and discarded by the siphoning. The prototype developed here is suitable for quantifying runoff volume, sediment, and P losses in field plots and has been manufactured under US$15.00.

Phosphorus accumulation in a southern Brazilian Ultisol amended with pig manure for nine years

This study evaluated P pools after nine years of successive application of either pig slurry (PS) or deep pig litter (DL) in a no-till Ultisol from southern Brazil. The experiment was established in Dec 2002 with the treatments control, application of 90 and 180 kg N ha−1 N as PS and as DL. In Mar 2010, soil samples were taken at six layers up to 30 cm deep. Total organic and inorganic P were assessed by the ignition method, and P compounds classes were evaluated by 31P-NMR spectroscopy. Total soil P increased proportionally with the P amount applied via DL and PS. Only DL application increased soil organic P, mainly at the highest dose and in the uppermost soil layers. The application of high doses of manure to these soils under no-till to meet crop N demands significantly increased P accumulation at the soil surface, especially with DL. This, in turn, increases the risk of contamination of water bodies due to P transfer from soil to rivers via runoff. The ignition method overestimates organic P compared to P-NMR. The highest proportion of organic P estimated by the ignition and P-NMR methods, at surface layers in the control suggests that inorganic P is added to the plots treated, increasing inorganic P and decreasing organic P. Moreover, with no P additions to the control, inorganic soil P is removed by plants, causing an apparent increase in the organic P proportion.(AU)

Phosphorus accumulation in a southern Brazilian Ultisol amended with pig manure for nine years

This study evaluated P pools after nine years of successive application of either pig slurry (PS) or deep pig litter (DL) in a no-till Ultisol from southern Brazil. The experiment was established in Dec 2002 with the treatments control, application of 90 and 180 kg N ha−1 N as PS and as DL. In Mar 2010, soil samples were taken at six layers up to 30 cm deep. Total organic and inorganic P were assessed by the ignition method, and P compounds classes were evaluated by 31P-NMR spectroscopy. Total soil P increased proportionally with the P amount applied via DL and PS. Only DL application increased soil organic P, mainly at the highest dose and in the uppermost soil layers. The application of high doses of manure to these soils under no-till to meet crop N demands significantly increased P accumulation at the soil surface, especially with DL. This, in turn, increases the risk of contamination of water bodies due to P transfer from soil to rivers via runoff. The ignition method overestimates organic P compared to P-NMR. The highest proportion of organic P estimated by the ignition and P-NMR methods, at surface layers in the control suggests that inorganic P is added to the plots treated, increasing inorganic P and decreasing organic P. Moreover, with no P additions to the control, inorganic soil P is removed by plants, causing an apparent increase in the organic P proportion.

Accuracy of methods to estimate potential acidity and lime requirement in soils of west region of Santa Catarina / Exatidão de métodospara estimativa da acidez potencial e necessidade de calcário em solos da região oeste de Santa Catarina

The objective of this study was to compare two methods of evaluation of potencial acidity (H+Al) and two methods to estimate liming requirement (LR) for soils from the west region of Santa Catarina State, Brazil. Fourteen soils were incubated with 7 lime rates for 120 days, obtaining the real values of H+Al at pH 7.0 and LR. These values were used as reference to evaluate the accuracy of two H+Al estimating methods: SMP buffer and calcium acetate at pH 7.0, and to evaluate the accuracy of two LR methods: base saturation (BS) and SMP index. On average, H+Al was underestimated in 6 and 40% by SMP and calcium acetate methods, respectively, especially in soils with high buffer capacity. The LR was underestimated in 20 and 30% by SMP index and BS, respectively. The SMP Index showed a better LR estimative than BS, especially in soils with high buffer capacity.(AU)

O estudo objetivou comparar dois métodos de avaliação de acidez potencial (H+Al) e de estimativa da necessidade de calagem (NC) para solos da região Oeste de Santa Catarina (SC). Quatorze solos foram incubados com 7 doses de calcário durante 120 dias, obtendo-se ao final os valores reais de H+Al a pH 7,0 e a NC dos solos. Esses valores serviram de referência para avaliar a exatidão dos métodos de estimativa do H+Al: tampão SMP e acetato de cálcio a pH 7,0 e a exatidão dos métodos de estimativa da NC: índice SMP e saturação por bases (V%). Em média, o H+Al foi subestimado em 6 e 40% pelos métodos SMP e acetato de cálcio, respectivamente, sendo mais problemático nos solos de maior tamponamento. Já a NC foi subestimada em 20 e 30% pelo Índice SMP e V%, respectivamente. O índice SMP estimou melhor a NC que o método V%, principalmente em solos de maior tamponamento.(AU)

Teor crítico de Enxofre no solo para o estabelecimento de clones de erva-mate no Sul do Brasil / Critical level of available sulphur in the soil during establishment of clones of yerba mate at Southern Brazil

O cultivo da erva-mate (Ilex paraguariensis St. Hil.) apresenta grande importância econômica na região Sul do Brasil. Contudo, a necessidade de fertilização no estabelecimento de plantios de erva-mate ainda é pouco conhecida. O trabalho objetivou avaliar a adubação sulfatada no crescimento inicial de dois clones de erva-mate em um Cambissolo Húmico. O experimento foi implantado em Itaiópolis, SC, testando quatro doses de enxofre (S) (0; 1,2; 2,4 e 3,6 kg de S-SO4 ha-¹) em dois clones femininos de erva-mate (F1 e F2). Avaliou-se a massa verde e a exportação de nutrientes pelas folhas, galhos finos (≤ 7mm), galhos grossos (> 7mm) e erva-mate comercial (folhas + galhos finos) e massa total. O S-SO4 foi avaliado na camada de 0-20 cm do solo 24 meses após a aplicação dos tratamentos e plantio das mudas. A produtividade de galho fino e a massa total foram influenciadas pela dose de S, independentemente do clone, indicando a exigência do nutriente para aumentar o rendimento de massa verde. Ainda, o clone F2 apresentou maior produção de galho grosso em função da dose de S. Assim, sugere-se o teor mínimo de 10 mg dm-3 S-SO4 no solo para um adequado estabelecimento de clones de erva-mate.(AU)

The cultivation of yerba mate (Ilex paraguariensis St. Hil.) has great economic importance in the Southern of Brazil. However, the fertilization requirements in the establishment of yerba mate plantations is still unknown. The objective of this work was to evaluate the needs of sulfate fertilization on the initial growth of two clones of yerba mate in a Humic Cambisol. An experiment was carried out in Itaiópolis, SC and fourdoses of S (0.0; 1.2; 2.4 and 3.6 kg of S-SO4 ²- ha-¹) and two clones (F1 and F2) were tested. The green mass and the export of nutrients were evaluated: leafs, fine twigs, thick twigs and commercial yerba mate (leaf + fine twigs), and total mass. Soil available S-SO4 was evaluated in the 0-20 cm soil layer 24 months after planting. The production of thick twigs increased with application of S, for clone F2. However, the yield of fine twig and total mass were influenced by the dose of S, independent of the clone. Thus, there was a positive response from the application of sulfur to clone F2, indicating that it is demanding on the nutrient, increasing the yield of green mass and the levels of S-SO4 in the soil.(AU)

Accuracy of methods to estimate potential acidity and lime requirement in soils of west region of Santa Catarina / Exatidão de métodospara estimativa da acidez potencial e necessidade de calcário em solos da região oeste de Santa Catarina

The objective of this study was to compare two methods of evaluation of potencial acidity (H+Al) and two methods to estimate liming requirement (LR) for soils from the west region of Santa Catarina State, Brazil. Fourteen soils were incubated with 7 lime rates for 120 days, obtaining the real values of H+Al at pH 7.0 and LR. These values were used as reference to evaluate the accuracy of two H+Al estimating methods: SMP buffer and calcium acetate at pH 7.0, and to evaluate the accuracy of two LR methods: base saturation (BS) and SMP index. On average, H+Al was underestimated in 6 and 40% by SMP and calcium acetate methods, respectively, especially in soils with high buffer capacity. The LR was underestimated in 20 and 30% by SMP index and BS, respectively. The SMP Index showed a better LR estimative than BS, especially in soils with high buffer capacity.

O estudo objetivou comparar dois métodos de avaliação de acidez potencial (H+Al) e de estimativa da necessidade de calagem (NC) para solos da região Oeste de Santa Catarina (SC). Quatorze solos foram incubados com 7 doses de calcário durante 120 dias, obtendo-se ao final os valores reais de H+Al a pH 7,0 e a NC dos solos. Esses valores serviram de referência para avaliar a exatidão dos métodos de estimativa do H+Al: tampão SMP e acetato de cálcio a pH 7,0 e a exatidão dos métodos de estimativa da NC: índice SMP e saturação por bases (V%). Em média, o H+Al foi subestimado em 6 e 40% pelos métodos SMP e acetato de cálcio, respectivamente, sendo mais problemático nos solos de maior tamponamento. Já a NC foi subestimada em 20 e 30% pelo Índice SMP e V%, respectivamente. O índice SMP estimou melhor a NC que o método V%, principalmente em solos de maior tamponamento.

Teor crítico de Enxofre no solo para o estabelecimento de clones de erva-mate no Sul do Brasil / Critical level of available sulphur in the soil during establishment of clones of yerba mate at Southern Brazil

O cultivo da erva-mate (Ilex paraguariensis St. Hil.) apresenta grande importância econômica na região Sul do Brasil. Contudo, a necessidade de fertilização no estabelecimento de plantios de erva-mate ainda é pouco conhecida. O trabalho objetivou avaliar a adubação sulfatada no crescimento inicial de dois clones de erva-mate em um Cambissolo Húmico. O experimento foi implantado em Itaiópolis, SC, testando quatro doses de enxofre (S) (0; 1,2; 2,4 e 3,6 kg de S-SO4 ha-¹) em dois clones femininos de erva-mate (F1 e F2). Avaliou-se a massa verde e a exportação de nutrientes pelas folhas, galhos finos (≤ 7mm), galhos grossos (> 7mm) e erva-mate comercial (folhas + galhos finos) e massa total. O S-SO4 foi avaliado na camada de 0-20 cm do solo 24 meses após a aplicação dos tratamentos e plantio das mudas. A produtividade de galho fino e a massa total foram influenciadas pela dose de S, independentemente do clone, indicando a exigência do nutriente para aumentar o rendimento de massa verde. Ainda, o clone F2 apresentou maior produção de galho grosso em função da dose de S. Assim, sugere-se o teor mínimo de 10 mg dm-3 S-SO4 no solo para um adequado estabelecimento de clones de erva-mate.

The cultivation of yerba mate (Ilex paraguariensis St. Hil.) has great economic importance in the Southern of Brazil. However, the fertilization requirements in the establishment of yerba mate plantations is still unknown. The objective of this work was to evaluate the needs of sulfate fertilization on the initial growth of two clones of yerba mate in a Humic Cambisol. An experiment was carried out in Itaiópolis, SC and fourdoses of S (0.0; 1.2; 2.4 and 3.6 kg of S-SO4 ²- ha-¹) and two clones (F1 and F2) were tested. The green mass and the export of nutrients were evaluated: leafs, fine twigs, thick twigs and commercial yerba mate (leaf + fine twigs), and total mass. Soil available S-SO4 was evaluated in the 0-20 cm soil layer 24 months after planting. The production of thick twigs increased with application of S, for clone F2. However, the yield of fine twig and total mass were influenced by the dose of S, independent of the clone. Thus, there was a positive response from the application of sulfur to clone F2, indicating that it is demanding on the nutrient, increasing the yield of green mass and the levels of S-SO4 in the soil.

Accuracy of methods to estimate potential acidity and lime requirement in soils of west region of Santa Catarina / Exatidão de métodospara estimativa da acidez potencial e necessidade de calcário em solos da região oeste de Santa Catarina

ABSTRACT: The objective of this study was to compare two methods of evaluation of potencial acidity (H+Al) and two methods to estimate liming requirement (LR) for soils from the west region of Santa Catarina State, Brazil. Fourteen soils were incubated with 7 lime rates for 120 days, obtaining the real values of H+Al at pH 7.0 and LR. These values were used as reference to evaluate the accuracy of two H+Al estimating methods: SMP buffer and calcium acetate at pH 7.0, and to evaluate the accuracy of two LR methods: base saturation (BS) and SMP index. On average, H+Al was underestimated in 6 and 40% by SMP and calcium acetate methods, respectively, especially in soils with high buffer capacity. The LR was underestimated in 20 and 30% by SMP index and BS, respectively. The SMP Index showed a better LR estimative than BS, especially in soils with high buffer capacity.

RESUMO: O estudo objetivou comparar dois métodos de avaliação de acidez potencial (H+Al) e de estimativa da necessidade de calagem (NC) para solos da região Oeste de Santa Catarina (SC). Quatorze solos foram incubados com 7 doses de calcário durante 120 dias, obtendo-se ao final os valores reais de H+Al a pH 7,0 e a NC dos solos. Esses valores serviram de referência para avaliar a exatidão dos métodos de estimativa do H+Al: tampão SMP e acetato de cálcio a pH 7,0 e a exatidão dos métodos de estimativa da NC: índice SMP e saturação por bases (V%). Em média, o H+Al foi subestimado em 6 e 40% pelos métodos SMP e acetato de cálcio, respectivamente, sendo mais problemático nos solos de maior tamponamento. Já a NC foi subestimada em 20 e 30% pelo Índice SMP e V%, respectivamente. O índice SMP estimou melhor a NC que o método V%, principalmente em solos de maior tamponamento.

Phosphorus Concentrations in Sequentially Fractionated Soil Samples as Affected by Digestion Methods.

Sequential fractionation has helped improving our understanding of the lability and bioavailability of P in soil. Nevertheless, there have been no reports on how manipulation of the different fractions prior to analyses affects the total P (TP) concentrations measured. This study investigated the effects of sample digestion, filtration, and acidification on the TP concentrations determined by ICP-OES in 20 soil samples. Total P in extracts were either determined without digestion by ICP-OES, or ICP-OES following block digestion, or autoclave digestion. The effects of sample filtration, and acidification on undigested alkaline extracts prior to ICP-OES were also evaluated. Results showed that, TP concentrations were greatest in the block-digested extracts, though the variability introduced by the block-digestion was the highest. Acidification of NaHCO3 extracts resulted in lower TP concentrations, while acidification of NaOH randomly increased or decreased TP concentrations. The precision observed with ICP-OES of undigested extracts suggests this should be the preferred method for TP determination in sequentially extracted samples. Thus, observations reported in this work would be helpful in appropriate sample handling for P determination, thereby improving the precision of P determination. The results are also useful for literature data comparison and discussion when there are differences in sample treatments.