Broadband optical vortex beam generation using flat-surface nanostructured gradient index vortex phase masks.

We developed a new kind of compact flat-surface nanostructured gradient index vortex phase mask, for the effective generation of optical vortex beams in broadband infrared wavelength range. A low-cost nanotechnological material method was employed for this work. The binary structure component consists of 17,557 nano-sized rods made of two lead-bismuth-gallium silicate glasses which were developed in-house. Those small rods are spatially arranged in such a way that, according to effective medium theory, the refractive index of this internal structure is constant in the radial direction and linearly changes following azimuthal angle. Numerical results demonstrated that a nanostructured vortex phase mask with a thickness of 19 µm can convert Gaussian beams into fundamental optical vortices over 290 nm wavelength bandwidth from 1275 to 1565 nm. This has been confirmed in experiments using three diode laser sources operating at 1310, 1550, and 1565 nm. The generation of vortex beams is verified through their uniform doughnut-like intensity distributions, clear astigmatic transformation patterns, and spiral as well as fork-like interferograms. This new flat-surface component can be directly mounted to an optical fiber tip for simplifying vortex generator systems as well as easier manipulation of the generated OVB in three-dimensional space.

Transmission of an optical vortex beam in antiresonant fibers generated in an all-fiber system.

We report an experimental study on transmission of orbital angular momentum mode in antiresonant fibers generated with a dedicated all-fiber optical vortex phase mask. The vortex generator can convert Gaussian beam into vortex beams with topological charge l = 1. Generated vortex beam is directly butt-coupled into the antiresonant fiber and propagates over distance of 150 cm. The stability and sensitivity of the transmitted vortex beam on the external perturbations including bending, axial stress, and twisting is investigated. We demonstrate distortion-free vortex propagation for the axial stress force below 0.677 N, a bend radius greater than 10 cm.

Development of gradient index microlenses for the broadband infrared range.

The development of gradient index free-form micro-optic components dedicated to the mid-infrared range is challenging due to the lack of appropriate technology. We propose a method for developing gradient index components for broadband infrared range beyond the transmission window of silicate glass based on nanostructurization using a stack-and-draw fiber drawing technique. A proof-of-concept microlens is developed and verified experimentally in the wavelength range 1.5-4.3 µm. The microlenses are composed of a set of nanorods with a diameter of 940 nm made of a pair of SiO2-PbO-Bi2O3-Ga2O3 based glasses ordered into the preliminary calculated binary pattern. The pattern forms effectively continuous parabolic refractive index distribution for infrared range according to Maxwell-Garnett effective medium model. The development of individual microlenses with a diameter of 118 µm and focal length of 278 µm at the wavelength of 3.75 µm are reported. A large array of 737 microlenses with an individual diameter of 125 µm and focal length of 375 µm is also presented and analyzed.

Integration of alumina-phosphate glass with cobalt-doped magnesium aluminate structure using a hot embossing technique for microlaser development.

In this work, the technique of hot embossing has been applied for the bonding of alumina-phosphate (PAL) glass with cobalt-doped magnesium aluminate (MALO) crystals. The application of the hot embossing technique for bonding of PAL/MALO is a competitive method, as compared to the existing thermobonding techniques. The obtained PAL/MALO interfaces show high quality, similar to what is currently achievable with other, more expensive traditional methods. The interfaces of the bonded samples have been successfully tested for strength and damage thresholds. The damage threshold is estimated to be around 4.5-7.9kW/cm2. Therefore, microlasers can be developed based on the obtained components.

Ultrathin glass fiber microprobe for electroporation of arbitrary selected cell groups.

A new type of ultrathin fiber microprobe for selective electroporation is reported. The microprobe is 10 cm long and has a diameter of 350 µm. This microprobe is a low cost tool, which allows electroporation of an arbitrary selected single cell or groups of cells among population with use of a standard microscope and cell culture plates. The microprobe in its basic form contains two metal microelectrodes made of a silver-copper alloy, running along the fiber, each with a diameter of 23 µm. The probe was tested in vitro on a population of normal and cancer cells. Successful targeted electroporation was observed by means of accumulation of trypan blue (TB) dye marker in the cell. The electroporation phenomenon was also verified with propidium iodide and AnnexinV in fluorescent microscopy.

Light field camera based on hexagonal array of flat-surface nanostructured GRIN lenses.

In this paper we present a light field camera system where a flat-surface hexagonal array of nanostructured gradient index lenses was used as a lens matrix. In our approach we use an array of 469 gradient index microlenses with a diameter of 20 µm and 100% fill factor. To develop the single lens and the lenslet array we used a modified stack-and-draw technology. In this technique, variation of refractive index is achieved by using quantized gradient index profiles and rods from different types of glasses. We show experimental results of using this type of lenses for imaging in a system of two kinds of light field cameras. In the first one, the microlens array is located in the focal plane of the main lens. The image is reconstructed, in this case using a Fourier slice photography algorithm. This allowed a partial reconstruction of a 3D scene with spatial and depth resolution of 20 µm and field of view of 500×500×500 µm. In the second configuration, the microlens array is located between a sample and a microscopic objective, thus allowing for superresolution 3D reconstruction of a microscopic image. The scale-invariant feature transform method was used for image reconstruction and obtained a partial 3D reconstruction with a field of view of 150×115×80 µm and a spatial resolution of 2 µm and depth resolution of 10 µm.

Development of large diameter nanostructured GRIN microlenses enhanced with temperature-controlled diffusion.

Nanostructured GRIN components are optical elements which can have an arbitrary refractive index profile while retaining flat-parallel entry and exit facets. A method of their fabrication requires assembly of large quantities of glass rods in order to satisfy subwavelength requirement of the effective medium theory. In this paper, we present a development of gradient index microlenses using a combination of methods: nanostructurization of the preform and controlled diffusion process during lens drawing on a fiber drawing tower. Adding a diffusion process allows us to overcome limits of the effective medium theory related to maximum size of nanorods in the lens structure. We show that nanorods are dissolved during the fiber drawing process in high temperature and glass components are locally quasi-uniformly distributed. To demonstrate feasibility of the proposed approach, we have developed and experimentally verified the performance of a nGRIN microlens with a diameter of 115 µm composed of 115 rods on the diagonal, and length of 200 µm devoted to work for the wavelength over 658 nm.

Inscription of Bragg gratings in nanostructured graded index single-mode fibers.

We report on efficient inscription of fiber Bragg gratings (FBGs) in a new type of single mode fiber with nanostructured core and with an effective parabolic graded index profile, using the standard phase mask method and a 248 nm pulsed laser. A nanostructured core allows to obtain high concentration of GeO2 in subwavelength glass rods and simultaneously to maintain low average germanium dopant level of silica similarly to standard single mode fibers. We showed that in a nanostructured core fiber, a factor of 3 better efficiency in gratings inscription was achieved, although the fiber has 20% lower average concentration of GeO2 with respect to SMF-28. In the nanostructured fiber we obtained a significant improvement in temperature sensitivity, while the strain sensitivity of FBG in nGRIN optical fiber is the same as in case of standard single-mode fiber (SMF-28). We have measured the strain sensitivity of 0.72 × 10-6 1/µÎµ (1.11 pm/µÎµ@1.53µm), and the temperature sensitivity is about 30% higher than for FBG in SMF-28 and equals to 10.2 × 10-6 1/K (15.6 pm/K@1.53µm).

Development of Dispersion-Optimized Photonic Crystal Fibers Based on Heavy Metal Oxide Glasses for Broadband Infrared Supercontinuum Generation with Fiber Lasers.

In this work a photonic crystal fiber made of a heavy metal oxide glass with optimized dispersion profile is proposed for supercontinuum generation in a broad range of wavelengths in the near-infrared, when pumped by a mode-locked fiber-based laser. The fiber is modelled and optimal geometrical parameters are selected to achieve flat and low dispersion in the anomalous regime. Supercontinuum generation in the range of 0.76⁻2.40 µm, within the dynamics of 30 dB, when pumped at 1.56 µm with 400 fs⁻long pulses and an average power 660 mW is possible. The applicability of such fibers is also discussed.

Fused silica photonic crystal fiber with heavily germanium doped microinclusion in the core dedicated to couple, guide and control LP02 higher-order mode.

We report on modeling, development, and optical characterization of fused silica photonic crystal fiber with germanium doped microinclusion placed in the middle of the core. The fiber is designed to efficiently couple and guide LP02 mode. It offers high optical density in the center region, large mode separation, low losses, and small dispersion with relatively flat profile for both LP01 and LP02 modes in 1-1.6 µm wavelength range. We demonstrate that by changing geometrical and material parameters of the inclusion partially independent tuning of propagation constants of individual modes is possible, what might be found is a variety of potential applications, e.g., in nonlinear optics. We also show that diffraction-limited propagation of LP02 mode in free space can be exploited in microscopy or lab-on-a-chip systems, where the proposed fiber can be used for light delivery.

Integrating Free-Form Nanostructured GRIN Microlenses with Single-Mode Fibers for Optofluidic Systems.

We present both a theoretical and an experimental study of a novel compact lensed fiber system utilizing a nanostructured GRIN lens. The lens can be integrated with an optical fiber, which ensures a unique and efficient focusing in any high index medium, such as a liquid. We use the effective medium approach to design lenses with arbitrary refractive index. To fabricate lenses, we utilize a discrete array of nano-sized rods made of two types of glasses, and apply a standard stack-and-draw fiber drawing technology. The fabricated nanostructured GRIN lenses have a parabolic refractive index profile with a diameter of a standard fiber, very short working distances (55 µm in the air) and a high numerical aperture (NA = 0.16). As a proof-of-concept of the new micro-lensed fiber system, we demonstrate an experiment on optical trapping of micrometer-sized glass beads. We also show that our method is compatible with optical fiber technology and allows for any shape of the refractive index distribution in 2D. Thanks to that a new functionality could be achieved by replacing the GRIN lens with an axicon lens, vortex type elements, micro-lenses arrays or diffraction elements.

Formation of optical vortices with all-glass nanostructured gradient index masks.

We report the development of microscopic size gradient index vortex masks using the modified stack-and-draw technique. The vortex mask has a form of flat surface all-glass plate. Its functionality is determined by an internal nanostructure composed of two types of soft glass nanorods. The generation of optical vortices with charges 1 and 2 is demonstrated.

High resolution Shack-Hartmann sensor based on array of nanostructured GRIN lenses.

We present a novel method for the development of a micro lenslets hexagonal array. We use gradient index (GRIN) micro lenses where the variation of the refraction index is achieved with a structure of nanorods made of 2 types of glasses. To develop the GRIN micro lens array, we used a modified stack-and-draw technology which was originally applied for the fabrication of photonic crystal fibers. This approach results in a completely flat element that is easy to integrate with other optical components and can be effectively used in high refractive index medium as liquids. As a proof-of-concept of the method we present a hexagonal array of 469 GRIN micro lenses with a diameter of 20 µm each and 100% fill factor. The GRIN lens array is further used to build a Shack-Hartmann detector for measuring wavefront distortion. A 50 lens/mm sampling density is achieved.

Diffractive optics development using a modified stack-and-draw technique.

We present a novel method for the development of diffractive optical elements (DOEs). Unlike standard surface relief DOEs, the phase shift is introduced through a refractive index variation achieved by using different types of glass. For the fabrication of DOEs we use a modified stack-and-draw technique, originally developed for the fabrication of photonic crystal fibers, resulting in a completely flat element that is easy to integrate with other optical components. A proof-of-concept demonstration of the method is presented-a two-dimensional binary optical phase grating in the form of a square chessboard with a pixel size of 5 µm. Two types of glass are used: low refractive index silicate glass NC21 and high refractive index lead-silicate glass F2. The measured diffraction characteristics of the fabricated component are presented and it is shown numerically and experimentally that such a DOE can be used as a fiber interconnector that couples light from a small-core fiber into the several cores of a multicore fiber.

Large elliptical nanostructured gradient-index microlens.

We demonstrate the feasibility of the development of a gradient-index elliptical microlens with a size of 75×125 µm using nanostructured glass technology. The gradient index is obtained by means of a discrete internal structure composed of two glasses with feature sizes much smaller than the wavelength of the incident light. A modified photonic crystal fiber-drawing technique is used for the lens fabrication. The elliptical shape of the lens is obtained by a novel final drawing stage where the spherically symmetric lens preform is drawn into an elliptical form by collapsing two large air holes placed in the preform during assembly. The effective focal lengths of 160 and 260 µm for the orthogonal axes are obtained experimentally for the fabricated lens, and show good agreement with those predicted by the effective medium theory and the full-wave beam propagation simulations.

Nanostructured gradient index microaxicons made by a modified stack and draw method.

We report the design and fabrication of nanostructured gradient index microaxicons suitable for integration with optical fibers. A structure with the effective refractive index decreasing linearly from the center to the edges (i.e., an axicon) was designed using a combination of a simulated annealing method and the effective medium theory. The design was verified numerically with beam propagation method simulations. The axicons were made by the modified stack and draw method and integrated with optical fibers. The optical properties of the fabricated elements were measured and showed good agreement with the numerical simulations. The fabricated axicons produced an extended line focus at a distance from about 70 to 160 µm from the lens facet with a minimum FWHM diameter of 8 µm at 90 µm. At smaller distances, an interference pattern is observed both in the experiment and in simulations, which is attributed to the uneven effective refractive index profile at the structure.

Optical fibers with gradient index nanostructured core.

We present a new approach for the development of structured optical fibers. It is shown that fibers having an effective gradient index profile with designed refractive index distribution can be developed with internal nanostructuring of the core composed of two glasses. As proof-of-concept, fibers made of two soft glasses with a parabolic gradient index profile are developed. Energy-dispersive X-ray spectroscopy reveals a possibility of selective diffusion of individual chemical ingredients among the sub-wavelength components of the nanostructure. This hints a postulate that core nanostructuring also changes material dispersion of the glasses in the core, potentially opening up unique dispersion shaping possibilities.

Coherent supercontinuum generation up to 2.3 µm in all-solid soft-glass photonic crystal fibers with flat all-normal dispersion.

Supercontinuum spanning over an octave from 900 - 2300 nm is reported in an all-normal dispersion, soft glass photonic crystal fiber. The all-solid microstructured fiber was engineered to achieve a normal dispersion profile flattened to within -50 to -30 ps/nm/km in the wavelength range of 1100 - 2700 nm. Under pumping with 75 fs pulses centered at 1550 nm, the recorded spectral flatness is 7 dB in the 930 - 2170 nm range, and significantly less if cladding modes present in the uncoated photonic crystal fiber are removed. To the best of our knowledge, this is the first report of an octave-spanning, all-normal dispersion supercontinuum generation in a non-silica microstructured fiber, where the spectrum long-wavelength edge is red-shifted to as far as 2300 nm. This is also an important step in moving the concept of ultrafast coherent supercontinuum generation in all-normal dispersion fibers further towards the mid-infrared spectral region.

Broadband infrared supercontinuum generation in hexagonal-lattice tellurite photonic crystal fiber with dispersion optimized for pumping near 1560 nm: reply.

We respond to the comment submitted by Xian Feng on our recent Letter, Opt. Lett.38, 4679 (2013). The comment addressed the attenuation of our oxide tellurite glass labeled TWPN/I/6. We provide the originally measured absorbance spectrum of the glass and correct values of its mid-infrared attenuation.

All-solid microstructured fiber with flat normal chromatic dispersion.

We present a new approach for the development of all-solid microstructured fiber with flat all-normal dispersion in the broadband range of 1550-2500 nm. The use of two soft glasses gives additional degrees of freedom in the design of microstructured fibers. As a result, we have designed and developed a fiber optimized for supercontinuum generation with 1550 nm pulsed lasers in the all-normal dispersion regime within an infrared range, beyond the fused silica glass limit. The measurement of the chromatic dispersion of the manufactured fibers was performed with a white light interferometric method in the spectral range 900-1650 nm. We demonstrate very good agreement between the full vector finite element simulations and the measurement results.