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1.
Materials (Basel) ; 16(24)2023 Dec 08.
Article in English | MEDLINE | ID: mdl-38138712

ABSTRACT

Sewage and water networks are crucial infrastructures of modern urban society. The uninterrupted functionality of these networks is paramount, necessitating regular maintenance and rehabilitation. In densely populated urban areas, trenchless methods, particularly those employing cured-in-place pipe technology, have emerged as the most cost-efficient approach for network rehabilitation. Common diagnostic methods for assessing pipe conditions, whether original or retrofitted with-cured-in-place pipes, typically include camera examination or laser scans, and are limited in material characterization. This study introduces three innovative methods for characterizing critical aspects of pipe conditions. The impact-echo method, ground-penetrating radar, and impedance spectroscopy address the challenges posed by polymer liners and offer enhanced accuracy in defect detection. These methods enable the characterization of delamination, identification of caverns behind cured-in-place pipes, and evaluation of overall pipe health. A machine learning algorithm using deep learning on images acquired from impact-echo signals using continuous wavelet transformation is presented to characterize defects. The aim is to compare traditional machine learning and deep learning methods to characterize selected pipe defects. The measurement conducted with ground-penetrating radar is depicted, employing a heuristic algorithm to estimate caverns behind the tested polymer composites. This study also presents results obtained through impedance spectroscopy, employed to characterize the delamination of polymer liners caused by uneven curing. A comparative analysis of these methods is conducted, assessing the accuracy by comparing the known positions of defects with their predicted characteristics based on laboratory measurements.

2.
Materials (Basel) ; 16(9)2023 May 04.
Article in English | MEDLINE | ID: mdl-37176410

ABSTRACT

Two sizes of test samples were selected to investigate the effect of size on the level of degradation. The smaller test specimens had dimensions of 40 × 40 × 160 mm, and the larger ones had dimensions of 100 × 100 × 400 mm. Both sizes of test specimens were always made of the same mortar. In one case, Blast Furnace Cement was chosen as the binder. In the other case, it was an alkali-activated material as a possibly more environmentally economical substitute. Both types of material were deposited in three degrading solutions: magnesium sulphate, ammonium nitrate and acetic acid. The reference set was stored in a water bath. After six months in the degradation solutions, a static elastic modulus was determined for the specimens during this test, and the acoustic emission was measured. Acoustic emission parameters were evaluated: the number of hits, the amplitude magnitude and a slope from the amplitude magnitude versus time (this slope should correspond to the Kaiser effect). For most of the parameters studied, the size effect was more evident for the more degraded specimens, i.e., those placed in aggressive solutions. The approximate location of emerging defects was also determined using linear localisation for smaller specimens where the degradation effect was more significant. In more aggressive environments (acetic acid, ammonium nitrate), the higher resistance of materials based on alkaline-activated slag was more evident, even in the case of larger test bodies. The experiments show that the acoustic emission results agree with the results of the static modulus of elasticity.

3.
Materials (Basel) ; 15(4)2022 Feb 11.
Article in English | MEDLINE | ID: mdl-35207884

ABSTRACT

Alkali-activated systems (AAS) represent an ecologically and economically sustainable inorganic binder as an alternative to ordinary Portland cement (OPC). One of the main benefits of AAS is their durability in aggressive environments, which can be equal or even better than that of OPC. In this paper, the influence of the type of alkaline activator in alkali-activated blast furnace slag (AAS) in terms of resistance to sulfur dioxide corrosion was investigated. The durability testing process was based on the CSN EN ISO 3231 standard and simultaneously compared with mortar samples prepared by using Blastfurnace cement CEM III/A 32.5R. The degradation progress was evaluated by employing several different methods such as observing the compressive strength development, weight change evaluation, non-destructive testing methods like ultrasound or impact echo technique, or visual phenolphthalein technique. Subsequently, fundamental characterization of samples by the XRD method was performed during the degradation test. The obtained results indicate that none of the testing methods used could be prioritized over others to determine the resistance of AAS against the action of sulfur dioxide. For this reason, the durability testing of AAS remains an issue, and the development of specific standards considering the behavior of AAS seems necessary.

4.
Materials (Basel) ; 14(21)2021 Oct 25.
Article in English | MEDLINE | ID: mdl-34771903

ABSTRACT

This paper presents the results of an experimental program aimed at the assessment of the freeze-thaw (F-T) resistance of concrete based on the evaluation of fracture tests accompanied by acoustic emission measurements. Two concretes of similar mechanical characteristics were manufactured for the experiment. The main difference between the C1 and C2 concrete was in the total number of air voids and in the A300 parameter, where both parameters were higher for C1 by about 35% and 52%, respectively. The evaluation of the fracture characteristics was performed on the basis of experimentally recorded load-deflection and load-crack mouth opening displacement diagrams using two different approaches: linear fracture mechanics completed with the effective crack model and the double-K model. The results show that both approaches gave similar results, especially if the nonlinear behavior before the peak load was considered. According to the results, it can be stated that continuous AE measurement is beneficial for the assessment of the extent of concrete deterioration, and it suitably supplements the fracture test evaluation. A comparison of the results of fracture tests with the resonance method and splitting tensile strength test shows that all testing methods led to the same conclusion, i.e., the C1 concrete was more F-T-resistant than C2. However, the fracture test evaluation provided more detailed information about the internal structure deterioration due to the F-T exposure.

5.
Materials (Basel) ; 14(22)2021 Nov 10.
Article in English | MEDLINE | ID: mdl-34832189

ABSTRACT

This article presents research on the behavior of cement-bonded particleboards under mechanical stress caused by the static load. The composition of the boards was modified using alternative raw materials-dust (DU) forming during the processing of cement-fibre boards and particle mixture (PM) generated in the production of cement-bonded particleboards. The particleboards (1-year-old) were subjected to an adverse environment (100 to 250 frost cycles). Mechanical parameters were tested, and the development of defects during static load of the boards by bending was analyzed using acoustic emission. Particleboards with modified compositions are slightly more resistant to adverse environments. The results of the acoustic emission showed the different types of defects occurring under stress by bending. Standard-composition particleboards showed defects located mainly under the cylindrical stress-test head. The modified boards showed larger location distribution of the occurring defects that were also concentrated further away from the cylindrical stress head. The energy during the occurrence of defects was higher in the modified boards in the location of weight application than in the reference boards.

6.
Materials (Basel) ; 14(16)2021 Aug 04.
Article in English | MEDLINE | ID: mdl-34442875

ABSTRACT

The development of smart materials is a basic prerequisite for the development of new technologies enabling the continuous non-destructive diagnostic analysis of building structures. Within this framework, the piezoresistive behavior of fly ash geopolymer with added carbon black under compression was studied. Prepared cubic specimens were doped with 0.5, 1 and 2% carbon black and embedded with four copper electrodes. In order to obtain a complex characterization during compressive loading, the electrical resistivity, longitudinal strain and acoustic emission were recorded. The samples were tested in two modes: repeated loading under low compressive forces and continuous loading until failure. The results revealed piezoresistivity for all tested mixtures, but the best self-sensing properties were achieved with 0.5% of carbon black admixture. The complex analysis also showed that fly ash geopolymer undergoes permanent deformations and the addition of carbon black changes its character from quasi-brittle to rather ductile. The combination of electrical and acoustic methods enables the monitoring of materials far beyond the working range of a strain gauge.

7.
Materials (Basel) ; 14(5)2021 Mar 05.
Article in English | MEDLINE | ID: mdl-33807866

ABSTRACT

This manuscript deals with a complex analysis of acoustic emission signals that were recorded during freeze-thaw cycles in test specimens produced from air-entrained concrete. An assessment of the resistance of concrete to the effects of freezing and thawing was conducted on the basis of a signal analysis. Since the experiment simulated testing of concrete in a structure, a concrete block with the height of 2.4 m and width of 1.8 m was produced to represent a real structure. When the age of the concrete was two months, samples were obtained from the block by core drilling and were subsequently used to produce test specimens. Testing of freeze-thaw resistance of concrete employed both destructive and non-destructive methods including the measurement of acoustic emission, which took place directly during the freeze-thaw cycles. The recorded acoustic emission signals were then meticulously analysed. The aim of the conducted experiments was to verify whether measurement using the acoustic emission method during Freeze-thaw (F-T) cycles are more sensitive to the degree of damage of concrete than the more commonly employed construction testing methods. The results clearly demonstrate that the acoustic emission method can reveal changes (e.g., minor cracks) in the internal structure of concrete, unlike other commonly used methods. The analysis of the acoustic emission signals using a fast Fourier transform revealed a significant shift of the dominant frequency towards lower values when the concrete was subjected to freeze-thaw cycling.

8.
Materials (Basel) ; 14(3)2021 Jan 28.
Article in English | MEDLINE | ID: mdl-33525594

ABSTRACT

The impact-echo diagnostic method is a well-known nondestructive pulse compression test method, which can be relatively easily used for the testing of concrete and reinforced concrete elements. The evaluation of the measurement with this method is based on the analysis of the signal itself in the time and frequency domains. This allows acquisition of information on the velocity of the mechanical wave, the resonant frequency of the specimen or on the presence of internal defects. The ability to interpret these measurements depends on the experience of the diagnostic technician. The advent of classification algorithms in the field of machine learning has brought an increasing number of applications where the entire interpretation phase can be considerably simplified with the help of classification models. However, this automated evaluation procedure must be provided with the information of whether the signal acquired by the test equipment has actually been measured under optimally set conditions. This paper proposes a procedure for the mutual comparison of different measuring setups with a variable tip type, hammer handle and impact force. These three variables were used for a series of measurements which were subsequently compared with each other using multi-criteria evaluation. This offers a tool for the evaluation of measured data and their filtering. As an output of the designed method, each measurement is marked by a score value, which represents how well the acquired signal fit the weight demands for each observed feature of the signal. The method allows the adjustment of selected demands for a specific application by means of set thresholds. This approach enables the understanding of characteristics of the signal in the automated pre-processing of measured data, where computing power is limited. Thus, this solution is potentially suitable for remote long-term observations with sensor arrays or for acoustic emission signals pre-processing.

9.
Materials (Basel) ; 13(16)2020 Aug 17.
Article in English | MEDLINE | ID: mdl-32824609

ABSTRACT

Hybrid systems represent a new sustainable type of cement combining the properties of ordinary Portland cement and alkali-activated materials. In this study, a hybrid system based on blast furnace slag and Portland clinker was investigated. The economic aspects and appropriate waste management resulted in the usage of technological waste from water glass production (WG-waste) as an alkaline activator. Although the Portland clinker content was very low, the incorporation of this by-product significantly improved the mechanical properties. Nevertheless, the high amount of alkalis in combination with possible reactive aggregates raises concerns about the risk of alkali-silica reaction (ASR). The results obtained from expansion measurement, the uranyl acetate fluorescence method, and microstructure characterization revealed that the undesirable effects of alkali-silica reaction in mortars based on the hydration of hybrid cement are minimal.

10.
Materials (Basel) ; 13(14)2020 Jul 08.
Article in English | MEDLINE | ID: mdl-32650453

ABSTRACT

The cured-in-place pipe (CIPP) method is currently the most frequently used approach for the renovation of piping without digging; this technology is suitable for pipes made from all types of material. The authors of this paper examined how chemical substances and increased temperature change samples of CIPP with vinyl-ester resin taken from a simulated installation. Changes were observed at several levels: visually via a digital optical microscope, through changes of short-term bending properties and by observation of the activity of the sample structure by means of acoustic emission (AE). Interdependencies among the observed parameters were examined, specifically, the cumulative number of hits (cnt)/deflection and flexural properties/mechanic wave velocity. The test results prove that after three weeks of immersion in a simulated aggressive environment that mirrors what may happen to CIPP in real conditions, short-term mechanical properties change. This is also proven by the results of the AE measurements. For clarity, the results include images from a digital optical microscope. In addition, this paper proves that CIPP samples have good resistance to the action of organic and inorganic acids and to increased temperatures. After three weeks of exposure to a temperature of 100 °C the CIPP flexural properties of the samples had even improved.

11.
Materials (Basel) ; 13(14)2020 Jul 17.
Article in English | MEDLINE | ID: mdl-32709159

ABSTRACT

The paper describes an experiment focusing on the way the material system influences the bond strength of large-format tiles installed on concrete substrate during mechanical loading under conditions that correspond to real-life application. This involves a controllable mechanical load applied over an area of a test model while observing its condition using non-destructive methods (ultrasonic pulse velocity test, acoustic emission method, strain measurement, and acoustic tracing). The model consisted of a concrete slab onto which were mounted four different systems with large-format tiles with the dimensions of 3 m × 1 m. The combinations differed in the thickness of the tile, the adhesive, and whether or not a fabric membrane was included in the adhesive bed. The experiment showed that the loading caused no damage to the ceramic tile. All the detected failures took place in the adhesive layer or in the concrete slab.

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