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J Org Chem ; 72(23): 8972-5, 2007 Nov 09.
Article in English | MEDLINE | ID: mdl-17924694

ABSTRACT

We report a novel, facile, and asymmetric approach for the synthesis of the anti-tumor alkaloid (+)-crispine A via a highly diastereoselective N-acyliminium cyclization reaction as a key synthetic step.


Subject(s)
Alkaloids/chemical synthesis , Antineoplastic Agents/chemical synthesis , Isoquinolines/chemical synthesis , Alkaloids/chemistry , Antineoplastic Agents/chemistry , Isoquinolines/chemistry , Magnetic Resonance Spectroscopy/methods , Magnetic Resonance Spectroscopy/standards , Molecular Conformation , Reference Standards , Stereoisomerism
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