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1.
Ultramicroscopy ; 259: 113923, 2024 May.
Article in English | MEDLINE | ID: mdl-38324944

ABSTRACT

M-subshell X-ray production cross sections were indirectly measured for Ir and Bi targets irradiated with monoenergetic electron beams. The projectile energy range ran from 2.2 to 28 keV, impinging on Ir and Bi pure bulk targets in a scanning electron microscope. The resulting X-ray emission spectra were acquired with an energy dispersive spectrometer, and processed afterwards by means of a robust parameter optimization procedure developed previously. X-ray production cross sections were finally obtained through an approach involving an analytical prediction for the emission spectra, which relies on the ionization depth distribution function. The values obtained by this approach were compared with empirical and theoretical predictions, appealing to different relaxation data taken from the literature.

2.
Ultramicroscopy ; 232: 113401, 2022 Jan.
Article in English | MEDLINE | ID: mdl-34634763

ABSTRACT

The cadmium L x-ray spectrum induced by electron impact was analyzed in detail. The measurements were performed on a bulk pure sample using a commercial wavelength dispersive spectrometer, and the spectrum was processed with a parameter optimization method previously developed. This procedure permitted the determination of characteristic energies, relative transition probabilities and natural linewidths for this element. The results obtained here were compared to the data found in the literature, when available. Spectral structures related to satellite and radiative Auger Effect emissions were also analyzed, assessing energy shifts and relative intensities. Some of these parameters were determined for the first time, even in overlapping peaks and weak transitions, which was possible due to the robustness of the spectral processing method used.

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