Non-reciprocal and non-Newtonian mechanical metamaterials.

Non-Newtonian liquids are characterized by stress and velocity-dependent dynamical response. In elasticity, and in particular, in the field of phononics, reciprocity in the equations acts against obtaining a directional response for passive media. Active stimuli-responsive materials have been conceived to overcome it. Significantly, Milton and Willis have shown theoretically in 2007 that quasi-rigid bodies containing masses at resonance can display a very rich dynamical behavior, hence opening a route toward the design of non-reciprocal and non-Newtonian metamaterials. In this paper, we design a solid structure that displays unidirectional shock resistance, thus going beyond Newton's second law in analogy to non-Newtonian fluids. We design the mechanical metamaterial with finite element analysis and fabricate it using three-dimensional printing at the centimetric scale (with fused deposition modeling) and at the micrometric scale (with two-photon lithography). The non-Newtonian elastic response is measured via dynamical velocity-dependent experiments. Reversing the direction of the impact, we further highlight the intrinsic non-reciprocal response.

Micro-Scale Mechanical Metamaterial with a Controllable Transition in the Poisson's Ratio and Band Gap Formation.

The ability to significantly change the mechanical and wave propagation properties of a structure without rebuilding it is currently one of the main challenges in the field of mechanical metamaterials. This stems from the enormous appeal that such tunable behavior may offer from the perspective of applications ranging from biomedical to protective devices, particularly in the case of micro-scale systems. In this work, a novel micro-scale mechanical metamaterial is proposed that can undergo a transition from one type of configuration to another, with one configuration having a very negative Poisson's ratio, corresponding to strong auxeticity, and the other having a highly positive Poisson's ratio. The formation of phononic band gaps can also be controlled concurrently which can be very useful for the design of vibration dampers and sensors. Finally, it is experimentally shown that the reconfiguration process can be induced and controlled remotely through application of a magnetic field by using appropriately distributed magnetic inclusions.

3D Auxetic Metamaterials with Elastically-Stable Continuous Phase Transition.

In solid state physics, phase transitions can influence material functionality and alter their properties. In mechanical metamaterials, structural-phase transitions can be achieved through instability or buckling of certain structural elements. However, these fast transitions in one mechanical parameter typically affect significantly the remaining parameters, hence, limiting their applications. Here, this limitation is addressed by designing a novel 3D mechanical metamaterial that is capable of undergoing a phase transition from positive to negative Poisson's ratio under compression, without significant degradation of Young's modulus (i.e. the phase transition is elastically-stable). The metamaterial is fabricated by two-photon lithography at the micro-scale and its mechanical behavior is assessed experimentally. For another choice of structural parameters, it is then shown that the auxetic behavior of the considered 3D metamaterial class can be maintained over a wide range of applied compressive strain.

Brillouin Light Scattering Characterisation of Gray Tone 3D Printed Isotropic Materials.

Three-dimensional direct laser writing technology enables one to print polymer microstructures whose size varies from a few hundred nanometers to a few millimeters. It has been shown that, by tuning the laser power during writing, one can adjust continuously the optical and elastic properties with the same base material. This process is referred to as gray-tone lithography. In this paper, we characterize by Brillouin light scattering the complex elastic constant C11 of different reticulated isotropic polymers, at longitudinal phonon frequencies of the order of 16 GHz. We estimate the real part of the C11 constant to vary from 7 to 11 GPa as a function of laser power, whereas its imaginary part varies between 0.25 and 0.6 GPa. The linear elastic properties are further measured at a fixed laser power as a function of temperature, from 20∘C to 80∘C. Overall, we show that our 3D printed samples have a good elastic quality with high Q factors only ten times smaller than fused silica at hypersonic frequencies.

Single-Step-Lithography Micro-Stepper Based on Frictional Contact and Chiral Metamaterial.

Stepper motors and actuators are among the main constituents of control motion devices. They are complex multibody systems with rather large overall volume due to their multifunctional parts and elaborate technological assembly processes. Miniaturization of individual parts is still posing assembly problems. In this paper, a single-step lithography process to fabricate a micro-stepper engine with an accurate micrometric rotation axis and an overall sub-millimeter size is demonstrated. The device is based on the frictional contacts and chiral metamaterials to get rid of the dependence on the accuracy of parts. The functional aspects of fabricated samples are discussed for many rotation cycles and for different frictional surfaces.

Micro-Scale Auxetic Hierarchical Mechanical Metamaterials for Shape Morphing.

Shape morphing and the possibility of having control over mechanical properties via designed deformations have attracted a lot of attention in the materials community and led to a variety of applications with an emphasis on the space industry. However, current materials normally do not allow to have a full control over the deformation pattern and often fail to replicate such behavior at low scales which is essential in flexible electronics. Thus, in this paper, novel 2D and 3D microscopic hierarchical mechanical metamaterials using mutually-competing substructures within the system that are capable of exhibiting a broad range of the highly unusual auxetic behavior are proposed. Using experiments (3D microprinted polymers) supported by computer simulations, it is shown that such ability can be controlled through geometric design parameters. Finally it is demonstrated that the considered structure can form a composite capable of shape morphing allowing it to deform to a predefined shape.

Near IR stationary wave Fourier transform lambda meter in lithium niobate: multiplexing and improving optical sampling using spatially shifted nanogroove antenna.

Several integrated optics solutions currently exist to develop monolithic, robust, and lightweight high-resolution spectrometers for spatial applications. An interesting option is generating a stationary wave inside a single-mode waveguide, and sampling the interference fringes using dielectric discontinuities on the surface of the waveguide. This allows the recording of the signal on a detector on top of the waveguide, and using dedicated Fourier transform methods to recover the spectrum of the source. All the difficulty is then linked to the length of the interferogram that is sampled. This determines the spectral resolution and the spacing between sampling centers, which are ultimately limited by the pixel pitch, and that will determine the spectral range of the spectrum. In addition, the dielectric discontinuities that will extract the flux from the waveguide have a relatively wide angular emission, resulting in crosstalk between pixels, and reducing the effective sampling step. Finally, the optical sensitivity of these systems is limited since the waveguides are single mode. Therefore, improving the efficiency of stationary wave Fourier transform spectrometers will require reducing the angular divergence of the sampled signal, reducing the sampling step, and increasing the optical input collection capacity. To achieve the two latest conditions, one interesting approach is spatial multiplexing. In this paper, we present the proof of concept of a multiplexed integrated optics Fourier transform spectrometer based on lithium niobate waveguides, using focused ion beam nanogrooves as sampling centers. The spatially shifted position of the antennas between consecutive waveguides will allow us to determine an unknown wavelength with tens of picometer resolution. The extraction efficiency and bandwidth of the antennas will be theoretically studied to optimize their periodicity and match a given pixel pitch. Finally, the ability to develop this concept on an electro-optic material will be of great interest to achieve further active phase modulation and increase the spectral bandwidth.

Bloch surface waves at the telecommunication wavelength with lithium niobate as the top layer for integrated optics.

Lithium niobate (LN)-based devices are widely used in integrated and nonlinear optics. This material is robust and resistive to high temperatures, which makes the LN-based devices stable, but challenging to fabricate. In this work, we report on the design, manufacturing, and characterization of engineered dielectric media with thin-film LN (TFLN) on top for the coupling and propagation of electromagnetic surface waves at telecommunication wavelengths. The designed one-dimensional photonic crystal (1DPhC) sustains Bloch surface waves (BSWs) at the multilayer-air interface at 1550 nm wavelength with a propagation detected over a distance of 3 mm. The working wavelength and improved BSW propagation parameters open the way for exploration of nonlinear properties of BSW-based devices. It is also expected that these novel devices potentially would be able to modify BSW propagation and coupling by external thermal-electrical stimuli due to the improved quality of the TFLN top layer of 1DPhC.

Improving the vertical radiation pattern issued from multiple nano-groove scattering centers acting as an antenna for future integrated optics Fourier transform spectrometers in the near IR.

The stationary wave integrated Fourier transform spectrometer (SWIFTS) is based on the sampling of a stationary wave using nano-scattering centers on the surface of a channel waveguide. Single nano-scale scattering centers above the waveguide surface will radiate the sampled signal with wide angular distribution, which is not compatible with the buried detection area of infrared (IR) detectors, resulting in crosstalk between pixels. An implementation of multiple diffraction nano-grooves (antenna) for each sampling center is proposed as an alternative solution to improve directivity towards the detector pixel by narrowing the scattering angle of the extracted light. Its efficiency is demonstrated from both simulated and measured far-field radiative patterns exhibiting a promising method to be used for the future integrated IR-SWIFTS.

Simple production of membrane-based LiNbO3 micro-modulators with integrated tapers.

We report on free-standing electro-optical LiNbO3 waveguides with integrated tapers made by optical grade dicing. Membranes with a calibrated thickness are produced simultaneously with tapers acting as spot-size converters. Thereby, thicknesses from 450 to 500 µm can simply be achieved together with integrated tapers guaranteeing low insertion losses. These developments open the way to the low-cost production of compact and low-power-consuming electro-optical components. As an example, a 200 µm-long free-standing electro-optical Fabry-Perot is demonstrated with a figure of merit of only 0.19 V·cm in a 4.5 µm-thick membrane.

Fast-beam self-trapping in LiNbO(3) films by pyroelectric effect.

We report light-beam self-trapping triggered by the pyroelectric effect in an isolated ferroelectric thin film. Experiments are performed in an 8-µm-thick congruent undoped LiNbO(3) film bonded onto a silicon wafer. Response time two orders of magnitude faster than in bulk LiNbO(3) is reported. The original underlying physics specific of this arrangement is discussed.

Optical characterization of ultra-short Bragg grating on lithium niobate ridge waveguide.

In this Letter, we report a technique to etch giant aspect ratio nanostructures in lithium niobate. An 8 µm long Bragg grating on a Ti:LiNbO3 ridge waveguide was fabricated by combining optical-grade dicing and focused ion beam milling. The reflectivity was evaluated using an optical coherence tomography system: it is measured to be 53% for the TM wave and 47% for the TE wave. We study by 2D-FDTD the modeled behavior of the electromagnetic field when an angle exists between two consecutive sidewalls of the grating in order to understand the difference between ideal Bragg grating and experimental samples. These simulations allow us to optimize the parameters in order to increase the reflection of the grating up to 80%.

Integrated temperature sensor based on an enhanced pyroelectric photonic crystal.

In this paper, temperature variations are detected thanks to an enhanced nano-optical pyroelectric sensor. Sensing is obtained with the pyroelectric effect of lithium niobate (LN) in which, a suitable air-membrane photonic crystal cavity has been fabricated. The wavelength position of the cavity mode is tuned 11.5 nm for a temperature variation of only 32 °C. These results agree quite well with 3D-FDTD simulations that predict tunability of 12.5 nm for 32 °C. This photonic crystal temperature sensor shows a sensitivity of 0.359 nm/°C for an active length of only ~5.2 µm.

Acoustic resonator based on periodically poled lithium niobate ridge.

The constant improvement of industrial needs to face modern telecommunication challenges leads to the development of novel transducer principles as alternatives to SAW and BAW solutions. The main technological limits of SAW (short-circuit between electrodes) and BAW (precise thickness control) solutions can be overcome by a new kind of transducer based on periodically poled ferroelectric substrate. The approach proposed in this paper exploits a ridge structure combined with a periodically poled transducer (PPT), allowing for the excitation of highly coupled modes unlike previously published results on planar PPTs. High-aspect-ratio ridges showing micrometer dimensions are achieved by dicing PPT plates with a diamond-tipped saw. An adapted metallization is achieved to excite acoustic modes exhibiting electromechanical coupling in excess of 15% with phase velocities up to 10 000 m·s(-1). Theoretical predictions show that these figures may reach values up to 20% and 18 000 m·s(-1), respectively, using an appropriate design.

Acoustic wave filter based on periodically poled lithium niobate.

Solutions for the development of compact RF passive transducers as an alternative to standard surface or bulk acoustic wave devices are receiving increasing interest. This article presents results on the development of an acoustic band-pass filter based on periodically poled ferroelectric domains in lithium niobate. The fabrication of periodically poled transducers (PPTs) operating in the range of 20 to 650 MHz has been achieved on 3-in (76.2-mm) 500-µm-thick wafers. This kind of transducer is able to excite elliptical as well as longitudinal modes, yielding phase velocities of about 3800 and 6500 ms(-1), respectively. A new type of acoustic band-pass filter is proposed, based on the use of PPTs instead of the SAWs excited by classical interdigital transducers. The design and the fabrication of such a filter are presented, as well as experimental measurements of its electrical response and transfer function. The feasibility of such a PPT-based filter is thereby demonstrated and the limitations of this method are discussed.

Optimization of LiNbO3 photonic crystals: toward 3D LiNbO3 micro-components.

We report easy-to-implement techniques to improve the reflectivity of LiNbO3 photonic crystals within the photonic bandgap. Firstly, we show that widening the channel waveguides confines the optical modes in the vertical direction, which leads to the development of the first 2D-PhCs on Ti-indiffused LiNbO3 waveguides. We also report the first optical characterization of PhCs implemented on ridge LiNbO3 waveguides. The reflectivity is measured using a swept-source optical coherence tomography (OCT) system, together with the transmission spectrum. Finally we report 3D-PhCs LiNbO3 fabricated by Focused Ion Beam milling on the side of ridge waveguides.