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Synthesis of 7,8α-dihydro-14α-deoxyecdysteroids.
Savchenko, Rimma G; Urasaeva, Yana R; Galyautdinov, Ilgiz V; Afonkina, Svetlana R; Khalilov, Leonard M; Dolgushin, Fedor M; Odinokov, Victor N.
Steroids ; 76(6): 603-6, 2011 May.
Article in English | MEDLINE | ID: mdl-21356225

ABSTRACT

A Pd-C-catalyzed hydrogenation in methanol and in the presence of sodium methylate is a simple, convenient and high yielding reduction method to convert the 7,14-dien-6-one ecdysteroids to their corresponding 7,8α-dihydro-14α-deoxyecdysteroids.


Subject(s)
Ecdysteroids/chemical synthesis , Catalysis , Crystallography, X-Ray , Ecdysteroids/chemistry , Methanol/chemistry , Molecular Conformation , Oxidation-Reduction , Palladium
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