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1.
Micromachines (Basel) ; 14(12)2023 Dec 10.
Article in English | MEDLINE | ID: mdl-38138390

ABSTRACT

This work aimed to numerically investigate the dynamic and thermal behavior of a fully developed, laminar, gaseous flow in a microchannel featuring a rhombic cross-section. Due to new fabrication techniques, microducts with rhombic cross-sections have recently received more attention. The momentum and energy balance equations were solved by using a commercial CDF code and assuming the slip and the H2 boundary conditions. The temperature jump between the wall and the adjacent fluid was also taken into account. The accuracy of the numerical results was checked by using the data available in the literature in terms of velocity profiles in the slip flow regime and the Nusselt number in the continuum flow regime. To also investigate the geometry effects on the fluid behavior, several values of the side angle of the rhombus were considered. The numerical results revealed that the rarefaction degree and geometrical properties significantly affected the Nusselt number.

2.
Micromachines (Basel) ; 13(8)2022 Jul 31.
Article in English | MEDLINE | ID: mdl-36014158

ABSTRACT

This paper aims to contribute to the analysis of a heat sink designed for the active cooling of small flat surfaces. The heat transfer device investigated here consists of a flat square substrate and a cover, separated by parallel channels with a rectangular cross-section. The cold air flowing in the channels is sucked from the environment, and the bottom of the substrate adheres closely to the hot surface of the device to be cooled. The thermal problem is tackled by considering two different conditions: the first one assuming one long side of the channel is heated and the three other sides are adiabatic (version 1L) and the second one assuming high conductivity of the walls (version 4), in both the H1 and H2 boundary conditions. Moreover, to investigate the effect of the number of channels on the performance of the heat sink, the number of channels is changed between 1 and 20. The results, presented in terms of the f Re product, Nusselt number, maximum surface temperature, and thermal resistance, reveal that both the thermal boundary conditions and the number of channels significantly affect the performance of the investigated heat transfer device.

3.
J Chromatogr A ; 1627: 461421, 2020 Sep 13.
Article in English | MEDLINE | ID: mdl-32823116

ABSTRACT

Herein we present an efficient, column-switching method that relies on a custom-made T-union passive diffusion micromixer to assist water dilution and promote trap solute focusing of a high sample volume dissolved in pure organic solvent using a 0.075 mm i.d. nano-LC column. This method allows injecting 20 µL (or higher) of sample volume, speeding up the analysis time, with a 400-fold increase of the limits of quantitation for selected compounds. Five pesticides in different media were used as model compounds, and the analyses were carried out with a triple quadrupole mass spectrometer equipped with a Liquid Electron Ionization (LEI) LC-MS interface working in multiple reaction monitoring (MRM) mode. The system microfluidics were investigated using COMSOL modeling software. Robustness of the entire system was evaluated using a post-extraction addition soil extracts with limits of detection values spanning from 0.10 to 0.45 µg/L. Reproducible results in terms of peak area, peak shape, and retention times were achieved in soil matrix. Repeatability test on peak area variations were lower than 10%.


Subject(s)
Chromatography, Reverse-Phase/methods , Electrons , Microfluidics/methods , Nanoparticles/chemistry , Tandem Mass Spectrometry/methods , Water/chemistry , Acetonitriles/chemistry , Diffusion , Limit of Detection , Pesticides/analysis , Reproducibility of Results , Solvents/chemistry
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